JP2017008172A - 表面保護フィルム - Google Patents
表面保護フィルム Download PDFInfo
- Publication number
- JP2017008172A JP2017008172A JP2015123731A JP2015123731A JP2017008172A JP 2017008172 A JP2017008172 A JP 2017008172A JP 2015123731 A JP2015123731 A JP 2015123731A JP 2015123731 A JP2015123731 A JP 2015123731A JP 2017008172 A JP2017008172 A JP 2017008172A
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- Prior art keywords
- weight
- cation
- protective film
- surface protective
- bis
- Prior art date
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- SSDSCDGVMJFTEQ-UHFFFAOYSA-N octadecyl 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 SSDSCDGVMJFTEQ-UHFFFAOYSA-N 0.000 description 1
- BMOMBHKAYGMGCR-UHFFFAOYSA-N octadecyl 3-oxobutanoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CC(C)=O BMOMBHKAYGMGCR-UHFFFAOYSA-N 0.000 description 1
- NKBWPOSQERPBFI-UHFFFAOYSA-N octadecyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCCCCCCCCCCCCCCCC NKBWPOSQERPBFI-UHFFFAOYSA-N 0.000 description 1
- OEIJHBUUFURJLI-UHFFFAOYSA-N octane-1,8-diol Chemical compound OCCCCCCCCO OEIJHBUUFURJLI-UHFFFAOYSA-N 0.000 description 1
- QTDSLDJPJJBBLE-PFONDFGASA-N octyl (z)-octadec-9-enoate Chemical compound CCCCCCCCOC(=O)CCCCCCC\C=C/CCCCCCCC QTDSLDJPJJBBLE-PFONDFGASA-N 0.000 description 1
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- IKYDDBGYKFPTGF-UHFFFAOYSA-N octyl 3-oxobutanoate Chemical compound CCCCCCCCOC(=O)CC(C)=O IKYDDBGYKFPTGF-UHFFFAOYSA-N 0.000 description 1
- 229940073665 octyldodecyl myristate Drugs 0.000 description 1
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- 125000006353 oxyethylene group Chemical group 0.000 description 1
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- 125000002080 perylenyl group Chemical group C1(=CC=C2C=CC=C3C4=CC=CC5=CC=CC(C1=C23)=C45)* 0.000 description 1
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- 125000000472 sulfonyl group Chemical group *S(*)(=O)=O 0.000 description 1
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- DZLFLBLQUQXARW-UHFFFAOYSA-N tetrabutylammonium Chemical compound CCCC[N+](CCCC)(CCCC)CCCC DZLFLBLQUQXARW-UHFFFAOYSA-N 0.000 description 1
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- DZKXJUASMGQEMA-UHFFFAOYSA-N tetradecyl tetradecanoate Chemical compound CCCCCCCCCCCCCCOC(=O)CCCCCCCCCCCCC DZKXJUASMGQEMA-UHFFFAOYSA-N 0.000 description 1
- CBXCPBUEXACCNR-UHFFFAOYSA-N tetraethylammonium Chemical compound CC[N+](CC)(CC)CC CBXCPBUEXACCNR-UHFFFAOYSA-N 0.000 description 1
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- DTIFFPXSSXFQCJ-UHFFFAOYSA-N tetrahexylazanium Chemical compound CCCCCC[N+](CCCCCC)(CCCCCC)CCCCCC DTIFFPXSSXFQCJ-UHFFFAOYSA-N 0.000 description 1
- QEMXHQIAXOOASZ-UHFFFAOYSA-N tetramethylammonium Chemical compound C[N+](C)(C)C QEMXHQIAXOOASZ-UHFFFAOYSA-N 0.000 description 1
- GJSGYPDDPQRWPK-UHFFFAOYSA-N tetrapentylammonium Chemical compound CCCCC[N+](CCCCC)(CCCCC)CCCCC GJSGYPDDPQRWPK-UHFFFAOYSA-N 0.000 description 1
- KSBAEPSJVUENNK-UHFFFAOYSA-L tin(ii) 2-ethylhexanoate Chemical compound [Sn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O KSBAEPSJVUENNK-UHFFFAOYSA-L 0.000 description 1
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- RUELTTOHQODFPA-UHFFFAOYSA-N toluene 2,6-diisocyanate Chemical compound CC1=C(N=C=O)C=CC=C1N=C=O RUELTTOHQODFPA-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 239000012780 transparent material Substances 0.000 description 1
- GFVKHYGXCQWRON-UHFFFAOYSA-N tributyl(ethyl)azanium Chemical compound CCCC[N+](CC)(CCCC)CCCC GFVKHYGXCQWRON-UHFFFAOYSA-N 0.000 description 1
- NXFZDTAAMQLJEC-UHFFFAOYSA-M tributyl-(2,2,2-trichloroacetyl)oxytin(1-) Chemical compound CCCC[Sn-](CCCC)(CCCC)OC(=O)C(Cl)(Cl)Cl NXFZDTAAMQLJEC-UHFFFAOYSA-M 0.000 description 1
- PWBHRVGYSMBMIO-UHFFFAOYSA-M tributylstannanylium;acetate Chemical compound CCCC[Sn](CCCC)(CCCC)OC(C)=O PWBHRVGYSMBMIO-UHFFFAOYSA-M 0.000 description 1
- MEJYOZOPFBOWNM-UHFFFAOYSA-N triethyl(heptyl)azanium Chemical compound CCCCCCC[N+](CC)(CC)CC MEJYOZOPFBOWNM-UHFFFAOYSA-N 0.000 description 1
- WGYXSYLSCVXFDU-UHFFFAOYSA-N triethyl(propyl)azanium Chemical compound CCC[N+](CC)(CC)CC WGYXSYLSCVXFDU-UHFFFAOYSA-N 0.000 description 1
- IQZRBOPLVCXUST-UHFFFAOYSA-M trifluoromethanesulfonate;trimethyl(oxiran-2-ylmethyl)azanium Chemical compound C[N+](C)(C)CC1CO1.[O-]S(=O)(=O)C(F)(F)F IQZRBOPLVCXUST-UHFFFAOYSA-M 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
- NRZWQKGABZFFKE-UHFFFAOYSA-N trimethylsulfonium Chemical compound C[S+](C)C NRZWQKGABZFFKE-UHFFFAOYSA-N 0.000 description 1
- LAGQNGWYNLUQRI-UHFFFAOYSA-N trioctylmethylammonium bis(trifluoromethylsulfonyl)imide Chemical compound FC(F)(F)S(=O)(=O)[N-]S(=O)(=O)C(F)(F)F.CCCCCCCC[N+](C)(CCCCCCCC)CCCCCCCC LAGQNGWYNLUQRI-UHFFFAOYSA-N 0.000 description 1
- 150000004072 triols Chemical class 0.000 description 1
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- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
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- 239000008096 xylene Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 150000003752 zinc compounds Chemical class 0.000 description 1
- IFNXAMCERSVZCV-UHFFFAOYSA-L zinc;2-ethylhexanoate Chemical compound [Zn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O IFNXAMCERSVZCV-UHFFFAOYSA-L 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- 150000003755 zirconium compounds Chemical class 0.000 description 1
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- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
- G02B1/14—Protective coatings, e.g. hard coatings
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- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/04—Homopolymers or copolymers of esters
- C09J133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09J133/08—Homopolymers or copolymers of acrylic acid esters
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- C09J175/04—Polyurethanes
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- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/22—Plastics; Metallised plastics
- C09J7/25—Plastics; Metallised plastics based on macromolecular compounds obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds
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- C09J7/00—Adhesives in the form of films or foils
- C09J7/30—Adhesives in the form of films or foils characterised by the adhesive composition
- C09J7/38—Pressure-sensitive adhesives [PSA]
- C09J7/381—Pressure-sensitive adhesives [PSA] based on macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
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- C09J2203/00—Applications of adhesives in processes or use of adhesives in the form of films or foils
- C09J2203/318—Applications of adhesives in processes or use of adhesives in the form of films or foils for the production of liquid crystal displays
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- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/30—Additional features of adhesives in the form of films or foils characterized by the chemical, physicochemical or physical properties of the adhesive or the carrier
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Abstract
Description
ポリエステル樹脂を主成分とする基材層と粘着剤層を有する表面保護フィルムであって、
該基材層が、黒色顔料を含む着色基材層であり、
該表面保護フィルムの全光線透過率が5%以下であり、
該表面保護フィルムのガラスに対する、剥離速度0.3m/分、剥離角度90度でのきっかけ剥離力が1N/25mm以下であり、
該表面保護フィルムのガラスに対する、剥離速度0.3m/分、剥離角度180度での剥離力が0.1N/25mm以下であり、
該表面保護フィルムのガラスに対する濡れ速度が0.05cm2/秒以上である。
本発明の表面保護フィルムは、ポリエステル樹脂を主成分とする基材層と粘着剤層を有する。
(a)全光線透過率が5%以下であり、
(b)ガラスに対する、剥離速度0.3m/分、剥離角度90度でのきっかけ剥離力が1N/25mm以下であること、
(c)ガラスに対する、剥離速度0.3m/分、剥離角度180度での剥離力が0.1N/25mm以下であること、
(d)ガラスに対する濡れ速度が0.05cm2/秒以上であること、
という要件を全て満たすことにより、被着体からの剥離のきっかけが容易に得られ、且つ、軽く剥離ができ、さらに、傷や異物混入の検出率が高くなる。
基材層はポリエステル樹脂を主成分とする。具体的には、基材層中のポリエステル樹脂の含有割合は、好ましくは50重量%〜99.99重量%であり、より好ましくは70重量%〜99.95重量%であり、さらに好ましくは90重量%〜99.9重量%であり、特に好ましくは92重量%〜99.7重量%であり、最も好ましくは95重量%〜99.5重量%である。基材層中のポリエステル樹脂の含有割合を上記範囲内に調整することによって、被着体からの剥離のきっかけが容易に得られ、且つ、軽く剥離ができ、さらに、傷や異物混入の検出率がより高い表面保護フィルムを提供することができる。
粘着剤層は、好ましくは、ウレタン系粘着剤およびアクリル系粘着剤から選ばれる少なくとも1種の粘着剤を含む。粘着剤層が、ウレタン系粘着剤およびアクリル系粘着剤から選ばれる少なくとも1種の粘着剤を含むことにより、きっかけ剥離力が軽く、180度ピール剥離力が軽く、濡れ速度が速い粘着剤層とすることができ、本発明で採用する特定の基材層と組み合わせることにより、被着体からの剥離のきっかけが容易に得られ、且つ、軽く剥離ができ、さらに、傷や異物混入の検出率がより高い表面保護フィルムを提供することができる。
ウレタン系粘着剤はポリウレタン系樹脂を含む。
スルホニル)イミド、トリエチルペンチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、トリエチルヘプチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、N,N−ジプロピル−N−メチル−N−エチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、N,N−ジプロピル−N−メチル−N−ペンチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、N,N−ジプロピル−N−ブチル−N−ヘキシルアンモニウムビス(トリフルオロメタンスルホニル)イミド、N,N−ジプロピルーN,N−ジヘキシルアンモニウムビス(トリフルオロメタンスルホニル)イミド、N,N−ジブチル−N−メチル−N−ペンチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、N,N−ジブチル−N−メチル−N−へキシルアンモニウムビス(トリフルオロメタンスルホニル)イミド、トリオクチルメチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、N−メチル−N−エチル−N−プロピル−N−ペンチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、1−ブチルピリジニウム(トリフルオロメタンスルホニル)トリフルオロアセトアミド、1−ブチル−3−メチルピリジニウム(トリフルオロメタンスルホニル)トリフルオロアセトアミド,1−エチル−3−メチルイミダゾリウム(トリフルオロメタンスルホニル)トリフルオロアセトアミド、テトラヘキシルアンモニウムビス(トリフルオロメタンスルホニル)イミド、ジアリルジメチルアンモニウムトリフルオロメタンスルホネート、ジアリルジメチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、ジアリルジメチルアンモニウムビス(ペンタフルオロエタンスルホニル)イミド、N,N−ジエチル−N−メチル−N−(2−メトキシエチル)アンモニウムトリフルオロメタンスルホネート、N,N−ジエチル−N−メチル−N−(2−メトキシエチル)アンモニウムビス(トリフルオロメタンスルホニル)イミド、N,N−ジエチル−N−メチル−N−(2−メトキシエチル)アンモニウムビス(ペンタフルオロエタンスルホニル)イミド、グリシジルトリメチルアンモニウムトリフルオロメタンスルホネート、グリシジルトリメチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、グリシジルトリメチルアンモニウムビス(ペンタフルオロエタンスルホニル)イミド、ジアリルジメチルアンモニウムビス(トリフルオロメタンスルホニル)イミド、ジアリルジメチルビス(ペンタフルオロエタンタンスルホニル)イミド、リチウムビス(トリフルオロメタンスルホニル)イミド、リチウムビス(フルオロスルホニル)イミドなどが挙げられる。
アクリル系粘着剤はアクリル系ポリマーを含む。
A={(Y−X)×f×5.611}/M
A:酸価
Y:サンプル溶液の滴定量(ml)
X:混合溶媒50gのみの溶液の滴定量(ml)
f:滴定溶液のファクター
M:ポリマーサンプルの重量(g)
測定条件は下記の通りである。
サンプル溶液:ポリマーサンプル約0.5gを混合溶媒(トルエン/2−プロパノール/蒸留水=50/49.5/0.5、重量比)50gに溶解してサンプル溶液とした。
滴定溶液:0.1N、2−プロパノール性水酸化カリウム溶液(和光純薬工業社製、石油製品中和価試験用)
電極:ガラス電極;GE−101、比較電極;RE−201
測定モード:石油製品中和価試験1
本発明の表面保護フィルムは、任意の適切な方法により製造することができる。
(1)粘着剤層の形成材料の溶液や熱溶融液を基材層上に塗布する方法、
(2)(1)に準じ、セパレーター上に塗布、形成した粘着剤層を基材層上に移着する方法、
(3)粘着剤層の形成材料を基材層上に押出して形成塗布する方法、
(4)基材層と粘着剤層を二層または多層にて押出しする方法、
(5)基材層上に粘着剤層を単層ラミネートする方法またはラミネート層とともに粘着剤層を二層ラミネートする方法、
(6)粘着剤層とフィルムやラミネート層等の基材層形成材料とを二層または多層ラミネートする方法、
などの、任意の適切な方法によって準備することができる。
本発明の表面保護フィルムは、被着体からの剥離のきっかけが容易に得られ、且つ、軽く剥離ができ、さらに、傷や異物混入の検出率が高いので、光学部材や電子部材の表面保護に好適に用いることができる。すなわち、本発明の光学部材は、本発明の表面保護フィルムが貼着されたものである。本発明の電子部材は、本発明の表面保護フィルムが貼着されたものである。
重量平均分子量は、ゲルパーミエーションクロマトグラフ(GPC)法により測定して得られたものをいう。より具体的には、例えば、GPC測定装置として、商品名「HLC−8220GPC」(東ソー(株)製)を用いて、下記の条件にて測定し、標準ポリスチレン換算値により算出することができる。
(分子量測定条件)
・サンプル濃度:0.2重量%(テトラヒドロフラン溶液)
・サンプル注入量:10μL
・サンプルカラム:TSKguardcolumn SuperHZ−H(1本)+TSKgel SuperHZM−H(2本)
・リファレンスカラム;TSKgel SuperH−RC(1本)
・溶離液:テトラヒドロフラン(THF)
・流量:0.6mL/min
・検出器:示差屈折計(RI)
・カラム温度(測定温度):40℃
JIS K7361「プラスチック−透明材料の全光線透過率の試験方法」に規定の方法に準じ、ヘイズメーター(村上色彩技術研究所製、HM−150型)を用いて、全光線透過率を測定した。
25mm幅にカットしてセパレーターを剥離した表面保護フィルムの粘着剤層側をガラス板(松浪硝子工業株式会社製、商品名:マイクロスライドガラスS)の表面に2kgのローラーを用いて貼り合わせた後、23℃、50%RHの条件で20分間放置し、剥離角度90度、剥離速度0.3m/分の条件で剥離し、表面保護フィルムが剥がれ始める時点の最大の力を読み取り、きっかけ剥離力とした。
25mm幅にカットしてセパレーターを剥離した表面保護フィルムの粘着剤層側をガラス板(松浪硝子工業株式会社製、商品名:マイクロスライドガラスS)の表面に2kgのローラーを用いて貼り合わせた後、23℃、50%RHの条件で20分間放置し、剥離角度180度、剥離速度0.3m/分の条件で剥離し、表面保護フィルムの剥離力を測定した。
(1)試験片(表面保護フィルムを2.5cm×15.0cmに切断したもの)の粘着剤層面の一部を被着体(ガラス板(松浪硝子工業株式会社製、商品名:マイクロスライドガラスS))に接触させた状態で、角度を20度〜30度となるように手で保持した。
(2)次に、試験片から手を離し、試験片の粘着剤層面がガラス板と接触して接触部から一方向に濡れ広がる様子をビデオカメラで記録した。なお、上記(1)において、試験片の粘着剤層面の一部を被着体のガラス板に接触させた部分以外から濡れ広がる状態となった場合には、測定・記録は行わなかった。
(3)試験片が全て濡れ広がるまでの時間を記録し、濡れ速度(cm2/秒)=測定面積(25cm2)/記録した秒数(秒)で算出し、濡れ速度(cm2/秒)とした。
(4)なお、測定は独立して3回行い、その平均値を採用した。また、測定は、クラス10000のクリーンルーム(温度23℃、湿度50%RH)の環境下で行った。
ガラス板(松浪硝子工業株式会社製、商品名:マイクロスライドガラスS)にガラス切で約2mmの長さの傷をつけ、傷をつけた面と反対の面に表面保護フィルムを貼り、反射法、目視にて、その傷が容易に確認できれば○、確認が困難であれば×とした。
酢酸エチルを染み込ませたウェスで表面保護フィルムの粘着剤層とは反対側の面を3回擦り、ウェスに色移りが確認されなかった場合は○、確認された場合は×とした。
カーボンブラックが1%未満の量で練り込まれたポリエチレンテレフタレートフィルム(東レ株式会社製、ルミラーX30、厚み=50μm)を、着色基材(A)とした。
透明なポリエチレンテレフタレートフィルム(東レ株式会社製、ルミラーS10、厚み=38μm)を、透明基材(B)とした。
透明なポリエチレンテレフタレートフィルム(東レ株式会社製、ルミラーS10、厚み=38μm)の片方の表面に、グラビア印刷法によって、黒色インクを5回以上塗工したものを、着色基材(C)とした。
ポリオールとして、プレミノールS3011(旭硝子株式会社製、Mn=10000):85重量部、サンニックスGP3000(三洋化成工業製、Mn=3000):13重量部、サンニックスGP1000(三洋化成工業製、Mn=1000)2重量部を用い、多官能イソシアネート化合物として多官能脂環族系イソシアネート化合物であるコロネートHX(日本ポリウレタン工業株式会社):18重量部、触媒(日本化学産業株式会社製、商品名:ナーセム第2鉄):0.08重量部、劣化防止剤としてIrganox1010(BASF製):0.5重量部、濡れ性添加剤としてミリスチン酸イソプロピル(花王製、商品名:エキセパールIPM):30重量部、希釈溶剤として酢酸エチル:210重量部を配合し、ディスパーで撹拌し、ウレタン系粘着剤組成物を得た。
得られたウレタン系粘着剤組成物を、製造例1で得られた着色基材(A)にアプリケータで乾燥後の厚みが10μmとなるよう塗布し、乾燥温度130℃、乾燥時間2分の条件でキュアーして乾燥した。このようにして、着色基材(A)上にウレタン系粘着剤(A)からなる粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、表面保護フィルム(1)を得た。
結果を表1に示した。
ポリオールとして、プレミノールS3011(旭硝子株式会社製、Mn=10000):85重量部、サンニックスGP3000(三洋化成工業製、Mn=3000):13重量部、サンニックスGP1000(三洋化成工業製、Mn=1000)2重量部を用い、多官能イソシアネート化合物として多官能脂環族系イソシアネート化合物であるコロネートHX(日本ポリウレタン工業株式会社):18重量部、触媒(日本化学産業株式会社製、商品名:ナーセム第2鉄):0.08重量部、劣化防止剤としてIrganox1010(BASF製):0.5重量部、濡れ性添加剤としてミリスチン酸イソプロピル(花王製、商品名:エキセパールIPM):30重量部、帯電防止剤として1−エチル−3−メチルイミダゾリウムビス(フルオロスルホニル)イミド(第一工業製薬性、商品名:エレクセルAS110):1.25重量部、変性シリコーン(信越化学工業製、商品名:KF−6004):0.01重量部、希釈溶剤として酢酸エチル:210重量部を配合し、ディスパーで撹拌し、ウレタン系粘着剤組成物を得た。
得られたウレタン系粘着剤組成物を、製造例1で得られた着色基材(A)にアプリケータで乾燥後の厚みが10μmとなるよう塗布し、乾燥温度130℃、乾燥時間2分の条件でキュアーして乾燥した。このようにして、着色基材(A)上にウレタン系粘着剤(B)からなる粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、表面保護フィルム(2)を得た。
結果を表1に示した。
攪拌羽根、温度計、窒素ガス導入管、冷却器を備えた四つ口フラスコに、2−エチルヘキシルアクリレート200重量部、2−ヒドロキシエチルアクリレート8重量部、重合開始剤として2,2´−アゾビスイソブチロニトリル0.4重量部、溶剤として酢酸エチル312重量部を仕込み、緩やかに撹拌しながら窒素ガスを導入し、フラスコ内の液温を65℃付近に保って6時間重合反応を行い、アクリル系ポリマー溶液(40重量%)を調製した。上記アクリル系ポリマーの重量平均分子量は54万、ガラス転移温度(Tg)は−68℃、酸価は0.0であった。
上記アクリル系ポリマー溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液中の固形分100重量部に対して、架橋剤としてヘキサメチレンジイソシアネートのイソシアヌレート体(日本ポリウレタン工業社製、商品名:コロネートHX):4重量部、架橋触媒としてジラウリン酸ジブチルスズ(東京ファインケミカル社製、商品名:エンビライザーOL−1、0.5重量%酢酸エチル溶液):0.015重量部、架橋遅延剤としてアセチルアセトンを全溶剤量に対して3重量部を加えて混合撹拌を行い、アクリル系粘着剤組成物を得た。
得られたアクリル系粘着剤組成物を、製造例1で得られた着色基材(A)にアプリケータで乾燥後の厚みが10μmとなるよう塗布し、乾燥温度130℃、乾燥時間2分の条件でキュアーして乾燥した。このようにして、着色基材(A)上にアクリル系粘着剤(A)からなる粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、表面保護フィルム(3)を得た。
結果を表1に示した。
攪拌羽根、温度計、窒素ガス導入管、冷却器を備えた四つ口フラスコに、2−エチルヘキシルアクリレート200重量部、2−ヒドロキシエチルアクリレート8重量部、重合開始剤として2,2´−アゾビスイソブチロニトリル0.4重量部、溶剤として酢酸エチル312重量部を仕込み、緩やかに撹拌しながら窒素ガスを導入し、フラスコ内の液温を65℃付近に保って6時間重合反応を行い、アクリル系ポリマー溶液(40重量%)を調製した。上記アクリル系ポリマーの重量平均分子量は54万、ガラス転移温度(Tg)は−68℃、酸価は0.0であった。
上記アクリル系ポリマー溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液中の固形分100重量部に対して、架橋剤としてヘキサメチレンジイソシアネートのイソシアヌレート体(日本ポリウレタン工業社製、商品名:コロネートHX):5重量部、アニオン系界面活性剤であるポリオキシエチレンノニルプロペニルフェニルエーテル硫酸アンモニウム(第一工業製薬社製、商品名:アクアロンHS−10):0.3重量部、架橋触媒としてジラウリン酸ジブチルスズ(東京ファインケミカル社製、商品名:エンビライザーOL−1、0.5重量%酢酸エチル溶液):0.015重量部、架橋遅延剤としてアセチルアセトンを全溶剤量に対して3重量部を加えて混合撹拌を行い、アクリル系粘着剤組成物を得た。
得られたアクリル系粘着剤組成物を、製造例1で得られた着色基材(A)にアプリケータで乾燥後の厚みが10μmとなるよう塗布し、乾燥温度130℃、乾燥時間2分の条件でキュアーして乾燥した。このようにして、着色基材(A)上にアクリル系粘着剤(B)からなる粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、表面保護フィルム(4)を得た。
結果を表1に示した。
ポリオールとして、プレミノールS3011(旭硝子株式会社製、Mn=10000):85重量部、サンニックスGP3000(三洋化成工業製、Mn=3000):13重量部、サンニックスGP1000(三洋化成工業製、Mn=1000)2重量部を用い、多官能イソシアネート化合物として多官能脂環族系イソシアネート化合物であるコロネートHX(日本ポリウレタン工業株式会社):18重量部、触媒(日本化学産業株式会社製、商品名:ナーセム第2鉄):0.08重量部、劣化防止剤としてIrganox1010(BASF製):0.5重量部、濡れ性添加剤としてミリスチン酸イソプロピル(花王製、商品名:エキセパールIPM):30重量部、希釈溶剤として酢酸エチル:210重量部を配合し、ディスパーで撹拌し、ウレタン系粘着剤組成物を得た。
得られたウレタン系粘着剤組成物を、製造例2で得られた透明基材(B)にアプリケータで乾燥後の厚みが10μmとなるよう塗布し、乾燥温度130℃、乾燥時間2分の条件でキュアーして乾燥した。このようにして、透明基材(B)上にウレタン系粘着剤(A)からなる粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、表面保護フィルム(C1)を得た。
結果を表1に示した。
攪拌羽根、温度計、窒素ガス導入管、冷却器を備えた四つ口フラスコに、ブチルアクリレート190重量部、アクリル酸5重量部、重合開始剤として2,2´−アゾビスイソブチロニトリル0.4重量部、溶剤として酢酸エチル312重量部を仕込み、緩やかに撹拌しながら窒素ガスを導入し、フラスコ内の液温を65℃付近に保って6時間重合反応を行い、アクリル系ポリマー溶液(40重量%)を調製した。上記アクリル系ポリマーの重量平均分子量は54万、ガラス転移温度(Tg)は−68℃、酸価は0.0であった。
上記アクリル系ポリマー溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液中の固形分100重量部に対して、架橋剤として1,3−ビス(N,N−グリシジルアミノメチル)シクロヘキサン(三菱瓦斯化学製、商品名:TETRAD−C):6重量部を加えて混合撹拌を行い、アクリル系粘着剤組成物を得た。
得られたアクリル系粘着剤組成物を、製造例1で得られた着色基材(A)にアプリケータで乾燥後の厚みが10μmとなるよう塗布し、乾燥温度130℃、乾燥時間2分の条件でキュアーして乾燥した。このようにして、着色基材(A)上にアクリル系粘着剤(C)からなる粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、表面保護フィルム(C2)を得た。
結果を表1に示した。
ポリオールとして、プレミノールS3011(旭硝子株式会社製、Mn=10000):85重量部、サンニックスGP3000(三洋化成工業製、Mn=3000):13重量部、サンニックスGP1000(三洋化成工業製、Mn=1000)2重量部を用い、多官能イソシアネート化合物として多官能脂環族系イソシアネート化合物であるコロネートHX(日本ポリウレタン工業株式会社):18重量部、触媒(日本化学産業株式会社製、商品名:ナーセム第2鉄):0.08重量部、劣化防止剤としてIrganox1010(BASF製):0.5重量部、濡れ性添加剤としてミリスチン酸イソプロピル(花王製、商品名:エキセパールIPM):30重量部、希釈溶剤として酢酸エチル:210重量部を配合し、ディスパーで撹拌し、ウレタン系粘着剤組成物を得た。
得られたウレタン系粘着剤組成物を、製造例3で得られた着色基材(C)にアプリケータで乾燥後の厚みが10μmとなるよう塗布し、乾燥温度130℃、乾燥時間2分の条件でキュアーして乾燥した。このようにして、着色基材(C)上にウレタン系粘着剤(A)からなる粘着剤層を作製した。次いで、粘着剤層の表面に、一方の面にシリコーン処理を施した厚さ25μmのポリエステル樹脂からなる基材のシリコーン処理面を貼合せて、表面保護フィルム(C3)を得た。
結果を表1に示した。
実施例1で得られた表面保護フィルム(1)のセパレーターを剥離し、粘着剤層側を光学部材である偏光板(日東電工株式会社製、商品名「TEG1465DUHC」)に貼着し、表面保護フィルムが貼着された光学部材を得た。
実施例2で得られた表面保護フィルム(2)のセパレーターを剥離し、粘着剤層側を、光学部材である偏光板(日東電工株式会社製、商品名「TEG1465DUHC」)に貼着し、表面保護フィルムが貼着された光学部材を得た。
実施例3で得られた表面保護フィルム(3)のセパレーターを剥離し、粘着剤層側を、光学部材である偏光板(日東電工株式会社製、商品名「TEG1465DUHC」)に貼着し、表面保護フィルムが貼着された光学部材を得た。
実施例4で得られた表面保護フィルム(4)のセパレーターを剥離し、粘着剤層側を、光学部材である偏光板(日東電工株式会社製、商品名「TEG1465DUHC」)に貼着し、表面保護フィルムが貼着された光学部材を得た。
実施例1で得られた表面保護フィルム(1)のセパレーターを剥離し、粘着剤層側を、電子部材である導電性フィルム(日東電工株式会社製、商品名「エレクリスタV270L−TFMP」)に貼着し、表面保護フィルムが貼着された電子部材を得た。
実施例2で得られた表面保護フィルム(2)のセパレーターを剥離し、粘着剤層側を、電子部材である導電性フィルム(日東電工株式会社製、商品名「エレクリスタV270L−TFMP」)に貼着し、表面保護フィルムが貼着された電子部材を得た。
実施例3で得られた表面保護フィルム(3)のセパレーターを剥離し、粘着剤層側を、電子部材である導電性フィルム(日東電工株式会社製、商品名「エレクリスタV270L−TFMP」)に貼着し、表面保護フィルムが貼着された電子部材を得た。
実施例4で得られた表面保護フィルム(4)のセパレーターを剥離し、粘着剤層側を、電子部材である導電性フィルム(日東電工株式会社製、商品名「エレクリスタV270L−TFMP」)に貼着し、表面保護フィルムが貼着された電子部材を得た。
2 粘着剤層
3 セパレーター
10 表面保護フィルム
Claims (4)
- ポリエステル樹脂を主成分とする基材層と粘着剤層を有する表面保護フィルムであって、
該基材層が、黒色顔料を含む着色基材層であり、
該表面保護フィルムの全光線透過率が5%以下であり、
該表面保護フィルムのガラスに対する、剥離速度0.3m/分、剥離角度90度でのきっかけ剥離力が1N/25mm以下であり、
該表面保護フィルムのガラスに対する、剥離速度0.3m/分、剥離角度180度での剥離力が0.1N/25mm以下であり、
該表面保護フィルムのガラスに対する濡れ速度が0.05cm2/秒以上である、
表面保護フィルム。 - 前記粘着剤層が、ウレタン系粘着剤およびアクリル系粘着剤から選ばれる少なくとも1種の粘着剤を含む、請求項1に記載の表面保護フィルム。
- 請求項1または2に記載の表面保護フィルムが貼着された光学部材。
- 請求項1または2に記載の表面保護フィルムが貼着された電子部材。
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JP2018123221A (ja) * | 2017-01-31 | 2018-08-09 | 日東電工株式会社 | 表面保護フィルム、及び、光学部材 |
JP2019188822A (ja) * | 2019-07-24 | 2019-10-31 | Agc株式会社 | 保護フィルム付きガラス積層体 |
JP2019194330A (ja) * | 2019-05-29 | 2019-11-07 | 日東電工株式会社 | 表面保護フィルム |
WO2020170820A1 (ja) * | 2019-02-21 | 2020-08-27 | 日東電工株式会社 | 保護シートおよびガラスユニットの製造方法 |
JP2021500617A (ja) * | 2017-10-23 | 2021-01-07 | エルジー・ケム・リミテッド | 光学フィルム、光学フィルムの製造方法および有機発光電子装置の製造方法 |
JP2021041711A (ja) * | 2019-07-24 | 2021-03-18 | Agc株式会社 | 表示装置 |
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