JP2015535017A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2015535017A5 JP2015535017A5 JP2015540108A JP2015540108A JP2015535017A5 JP 2015535017 A5 JP2015535017 A5 JP 2015535017A5 JP 2015540108 A JP2015540108 A JP 2015540108A JP 2015540108 A JP2015540108 A JP 2015540108A JP 2015535017 A5 JP2015535017 A5 JP 2015535017A5
- Authority
- JP
- Japan
- Prior art keywords
- mixture
- branched
- pfpe
- chain
- linear
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 claims description 23
- 238000000034 method Methods 0.000 claims description 18
- 229910052801 chlorine Inorganic materials 0.000 claims description 10
- 229910052731 fluorine Inorganic materials 0.000 claims description 10
- 125000000524 functional group Chemical group 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 5
- 239000000460 chlorine Substances 0.000 claims description 5
- 125000001309 chloro group Chemical group Cl* 0.000 claims description 5
- 125000001153 fluoro group Chemical group F* 0.000 claims description 5
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 5
- 150000001732 carboxylic acid derivatives Chemical group 0.000 claims 10
- 239000007790 solid phase Substances 0.000 claims 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical group OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 6
- 239000007791 liquid phase Substances 0.000 claims 5
- 239000000725 suspension Substances 0.000 claims 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 3
- 239000003960 organic solvent Substances 0.000 claims 3
- 229920000642 polymer Polymers 0.000 claims 3
- 238000004587 chromatography analysis Methods 0.000 claims 2
- 239000007787 solid Substances 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- BOSAWIQFTJIYIS-UHFFFAOYSA-N 1,1,1-trichloro-2,2,2-trifluoroethane Chemical compound FC(F)(F)C(Cl)(Cl)Cl BOSAWIQFTJIYIS-UHFFFAOYSA-N 0.000 claims 1
- SJBBXFLOLUTGCW-UHFFFAOYSA-N 1,3-bis(trifluoromethyl)benzene Chemical group FC(F)(F)C1=CC=CC(C(F)(F)F)=C1 SJBBXFLOLUTGCW-UHFFFAOYSA-N 0.000 claims 1
- DFUYAWQUODQGFF-UHFFFAOYSA-N 1-ethoxy-1,1,2,2,3,3,4,4,4-nonafluorobutane Chemical compound CCOC(F)(F)C(F)(F)C(F)(F)C(F)(F)F DFUYAWQUODQGFF-UHFFFAOYSA-N 0.000 claims 1
- 241000255925 Diptera Species 0.000 claims 1
- 230000005526 G1 to G0 transition Effects 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- 239000003849 aromatic solvent Substances 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- 125000003709 fluoroalkyl group Chemical group 0.000 claims 1
- 239000000499 gel Substances 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000000746 purification Methods 0.000 claims 1
- 239000000741 silica gel Substances 0.000 claims 1
- 229910002027 silica gel Inorganic materials 0.000 claims 1
- 150000004760 silicates Chemical class 0.000 claims 1
- 239000000377 silicon dioxide Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 150000007942 carboxylates Chemical class 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 238000007306 functionalization reaction Methods 0.000 description 2
- 239000002243 precursor Substances 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12191288.5 | 2012-11-05 | ||
| EP12191288 | 2012-11-05 | ||
| PCT/EP2013/072679 WO2014067981A1 (en) | 2012-11-05 | 2013-10-30 | Process for the purification of (per)fluoropolyethers with carboxylate end groups |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015535017A JP2015535017A (ja) | 2015-12-07 |
| JP2015535017A5 true JP2015535017A5 (cg-RX-API-DMAC7.html) | 2018-12-13 |
| JP6530715B2 JP6530715B2 (ja) | 2019-06-12 |
Family
ID=47143687
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015540108A Active JP6530715B2 (ja) | 2012-11-05 | 2013-10-30 | カルボキシレート末端基を有する（パー）フルオロポリエーテルの精製方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US9370733B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP2914358B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JP6530715B2 (cg-RX-API-DMAC7.html) |
| CN (1) | CN104768623B (cg-RX-API-DMAC7.html) |
| WO (1) | WO2014067981A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012157714A1 (ja) * | 2011-05-18 | 2012-11-22 | 旭硝子株式会社 | 含フッ素共重合体およびイオン交換膜 |
| JP5862661B2 (ja) * | 2011-05-18 | 2016-02-16 | 旭硝子株式会社 | 含フッ素共重合体の製造方法およびイオン交換膜の製造方法 |
| JP5668888B1 (ja) * | 2013-08-23 | 2015-02-12 | ダイキン工業株式会社 | パーフルオロ（ポリ）エーテル基含有カルボン酸化合物の分離方法 |
| JP6513053B2 (ja) * | 2016-06-13 | 2019-05-15 | 信越化学工業株式会社 | 片末端カルボキシル基含有パーフルオロポリエーテル化合物を含む組成物の製造方法 |
| WO2019163712A1 (ja) * | 2018-02-21 | 2019-08-29 | ダイキン工業株式会社 | （ポリ）エーテル基含有モノカルボン酸化合物の製造方法 |
| JP7493307B2 (ja) | 2018-06-08 | 2024-05-31 | 信越化学工業株式会社 | パーフルオロポリエーテル化合物の分離精製方法 |
| CN116209710A (zh) * | 2020-09-16 | 2023-06-02 | Ａｇｃ株式会社 | 分离方法 |
| CN113866314B (zh) * | 2021-10-09 | 2022-09-09 | 上海睿易环境科技有限公司 | 一种测定土壤和沉积物中九氟丁基乙基醚含量的方法 |
| CN116874765A (zh) * | 2022-06-23 | 2023-10-13 | 浙江大学 | 液液萃取分离单羧酸盐端基全氟聚醚和双羧酸盐端基全氟聚醚的方法 |
| CN116870528B (zh) * | 2022-06-23 | 2025-11-07 | 浙江大学 | 离子络合萃取分离惰性全氟聚醚和活性全氟聚醚羧酸盐 |
| WO2024147355A1 (ja) * | 2023-01-06 | 2024-07-11 | ダイキン工業株式会社 | フルオロポリエーテル基含有カルボン酸の製造方法 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1104482A (en) | 1964-04-09 | 1968-02-28 | Montedison Spa | Perfluoro-olefin derivatives |
| US3442942A (en) | 1964-04-09 | 1969-05-06 | Montedison Spa | Fluorinated oxygen containing acyl fluorides |
| AU579374B2 (en) | 1984-05-23 | 1988-11-24 | Ausimont S.R.L. | Process for preparing perfluoropolyethers with neutral and functional end-groups, having a regulated molecular weight |
| IT1229845B (it) | 1989-04-20 | 1991-09-13 | Ausimont Srl | Procedimento per la preparazione di perfluoropolieteri perossidici. |
| IT1251965B (it) | 1991-10-21 | 1995-05-27 | Ausimont Spa | Procedimento per separare tra loro le specie non funzionali, monofunzionali e bifunzionali presenti nei perfluoropoliossialchileni. |
| IT1251964B (it) | 1991-10-21 | 1995-05-27 | Ausimont Spa | Procedimento per separare tra loro specie non funzionali, monofunzionali e bifunzionali presenti nei perfluoropoliossialchileni. |
| US5919614A (en) | 1994-10-19 | 1999-07-06 | Lifecell Corporation | Composition comprising three platelet lesion inhibitors for platelet storage |
| IT1282628B1 (it) | 1996-02-14 | 1998-03-31 | Ausimont Spa | Processo per la preparazione di perfluoropolieteri perossidici |
| IT1283646B1 (it) * | 1996-08-02 | 1998-04-23 | Ausimont Spa | Processo di preparazione di perfluoropolieteri |
| IT1290462B1 (it) | 1997-04-08 | 1998-12-03 | Ausimont Spa | Polimeri idrogenati modificati |
| ITMI20041370A1 (it) | 2004-07-09 | 2004-10-09 | Solvay Solexis Spa | Separazione di perfluioropolirteri -pepe-bifunzionali a termninazione-ch20h dalle loro miscele con pepe monofunzionali-ch2oh |
| ITMI20060681A1 (it) | 2006-04-06 | 2007-10-07 | Solvay Solexis Spa | Processo per preparare perfluoropolieteri mono-carbossilici ad elevata purezza |
| US8664353B2 (en) * | 2009-05-15 | 2014-03-04 | Solvay Solexis S.P.A. | Process for the purification of polyol PFPE derivatives |
| JP5235026B2 (ja) | 2010-09-28 | 2013-07-10 | 信越化学工業株式会社 | フルオロオキシアルキレン基含有ポリマー組成物および該組成物を含む表面処理剤並びに該表面処理剤で表面処理された物品 |
-
2013
- 2013-10-30 JP JP2015540108A patent/JP6530715B2/ja active Active
- 2013-10-30 EP EP13783931.2A patent/EP2914358B1/en active Active
- 2013-10-30 CN CN201380057794.9A patent/CN104768623B/zh active Active
- 2013-10-30 WO PCT/EP2013/072679 patent/WO2014067981A1/en not_active Ceased
- 2013-10-30 US US14/440,821 patent/US9370733B2/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2015535017A5 (cg-RX-API-DMAC7.html) | ||
| JP6530715B2 (ja) | カルボキシレート末端基を有する（パー）フルオロポリエーテルの精製方法 | |
| CN107709296B (zh) | 富勒烯衍生物和润滑剂 | |
| Raffa et al. | Amphiphilic copolymers based on PEG‐acrylate as surface active water viscosifiers: towards new potential systems for enhanced oil recovery | |
| JPWO2021100836A5 (cg-RX-API-DMAC7.html) | ||
| CN103193919B (zh) | 端硅烷基液体氟聚合物的制备方法及固化方法 | |
| JP6119656B2 (ja) | フルオロポリエーテル基含有ポリマー | |
| JP2014148600A5 (cg-RX-API-DMAC7.html) | ||
| JP2013189641A5 (cg-RX-API-DMAC7.html) | ||
| JP2014516210A5 (cg-RX-API-DMAC7.html) | ||
| JP2004525238A5 (cg-RX-API-DMAC7.html) | ||
| JP6636949B2 (ja) | 銀ナノワイヤーの製造方法、該方法で得られた銀ナノワイヤー及び該銀ナノワイヤーを含有するインク | |
| KR102311165B1 (ko) | 편말단 카르복실기 함유 퍼플루오로폴리에테르 화합물을 포함하는 조성물의 제조방법 | |
| CN105939990A (zh) | 富勒烯衍生物、氟树脂组合物和润滑剂 | |
| JP2012021100A (ja) | イオン性高分岐ポリマー及び炭素ナノ材料分散剤 | |
| CN102985506B (zh) | 不燃性溶剂和表面处理剂 | |
| JP6355109B2 (ja) | 含フッ素ニトリルオキシド化合物 | |
| JP6130288B2 (ja) | アリル基変性フルオロオキシアルキレン基含有ポリマー及びその製造方法 | |
| Gnanasekaran et al. | Influence of moieties on morphology, thermal, and dielectric properties in polyamide‐polyhedral oligomeric silsequioxanes nanocomposites | |
| Salavagione et al. | Poly (vinyl chloride)/multiwalled carbon nanotube nanocomposites: Effect of the tacticity distribution on the polymer/nanofiller interface | |
| ITMI20050384A1 (it) | Processo per preparare perfluoropolieteri perossidici | |
| WO2021095870A1 (ja) | 半導体型単層カーボンナノチューブ分散液の製造方法 | |
| WO2024111519A1 (ja) | ポリオルガノシロキサン | |
| CN108329465B (zh) | 含氟环氧寡聚物基苯乙烯单体及其制备方法和应用 | |
| JP6513053B2 (ja) | 片末端カルボキシル基含有パーフルオロポリエーテル化合物を含む組成物の製造方法 |