JP2015529608A5 - - Google Patents
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- Publication number
- JP2015529608A5 JP2015529608A5 JP2015515625A JP2015515625A JP2015529608A5 JP 2015529608 A5 JP2015529608 A5 JP 2015529608A5 JP 2015515625 A JP2015515625 A JP 2015515625A JP 2015515625 A JP2015515625 A JP 2015515625A JP 2015529608 A5 JP2015529608 A5 JP 2015529608A5
- Authority
- JP
- Japan
- Prior art keywords
- zeolitic material
- mixture
- range
- cha
- absorption band
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 32
- 239000000463 material Substances 0.000 claims 22
- 239000000203 mixture Substances 0.000 claims 21
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 7
- 238000010521 absorption reaction Methods 0.000 claims 7
- 150000001875 compounds Chemical class 0.000 claims 6
- -1 tetraalkylammonium cations Chemical class 0.000 claims 5
- 238000002835 absorbance Methods 0.000 claims 4
- 238000002425 crystallisation Methods 0.000 claims 4
- 230000008025 crystallization Effects 0.000 claims 4
- 239000010457 zeolite Substances 0.000 claims 4
- 229910052676 chabazite Inorganic materials 0.000 claims 3
- 238000005004 MAS NMR spectroscopy Methods 0.000 claims 2
- 229910052782 aluminium Inorganic materials 0.000 claims 2
- 229910052796 boron Inorganic materials 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- 239000013078 crystal Substances 0.000 claims 2
- 125000000753 cycloalkyl group Chemical group 0.000 claims 2
- 229910052733 gallium Inorganic materials 0.000 claims 2
- 229910052732 germanium Inorganic materials 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 229910052738 indium Inorganic materials 0.000 claims 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims 2
- 229910052710 silicon Inorganic materials 0.000 claims 2
- 235000012239 silicon dioxide Nutrition 0.000 claims 2
- 239000000377 silicon dioxide Substances 0.000 claims 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims 2
- 238000006467 substitution reaction Methods 0.000 claims 2
- 229910052718 tin Inorganic materials 0.000 claims 2
- 229910052719 titanium Inorganic materials 0.000 claims 2
- 229910052726 zirconium Inorganic materials 0.000 claims 2
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 claims 1
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 claims 1
- 101100008649 Caenorhabditis elegans daf-5 gene Proteins 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- 229910018557 Si O Inorganic materials 0.000 claims 1
- 239000004115 Sodium Silicate Substances 0.000 claims 1
- 238000002441 X-ray diffraction Methods 0.000 claims 1
- 229910021536 Zeolite Inorganic materials 0.000 claims 1
- 239000003463 adsorbent Substances 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims 1
- 150000004645 aluminates Chemical class 0.000 claims 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- YOUGRGFIHBUKRS-UHFFFAOYSA-N benzyl(trimethyl)azanium Chemical compound C[N+](C)(C)CC1=CC=CC=C1 YOUGRGFIHBUKRS-UHFFFAOYSA-N 0.000 claims 1
- UNYSKUBLZGJSLV-UHFFFAOYSA-L calcium;1,3,5,2,4,6$l^{2}-trioxadisilaluminane 2,4-dioxide;dihydroxide;hexahydrate Chemical compound O.O.O.O.O.O.[OH-].[OH-].[Ca+2].O=[Si]1O[Al]O[Si](=O)O1.O=[Si]1O[Al]O[Si](=O)O1 UNYSKUBLZGJSLV-UHFFFAOYSA-L 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 239000008119 colloidal silica Substances 0.000 claims 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- 229910021485 fumed silica Inorganic materials 0.000 claims 1
- 238000002329 infrared spectrum Methods 0.000 claims 1
- 230000010354 integration Effects 0.000 claims 1
- 238000005342 ion exchange Methods 0.000 claims 1
- 150000002500 ions Chemical class 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 150000002739 metals Chemical class 0.000 claims 1
- 239000002808 molecular sieve Substances 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 235000019353 potassium silicate Nutrition 0.000 claims 1
- 238000000634 powder X-ray diffraction Methods 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 229910002027 silica gel Inorganic materials 0.000 claims 1
- 239000000741 silica gel Substances 0.000 claims 1
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Inorganic materials [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims 1
- 235000019795 sodium metasilicate Nutrition 0.000 claims 1
- 229910052911 sodium silicate Inorganic materials 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12170709 | 2012-06-04 | ||
| EP12170709.5 | 2012-06-04 | ||
| PCT/IB2013/054569 WO2013182974A1 (en) | 2012-06-04 | 2013-06-03 | Cha type zeolitic materials and methods for their preparation using cycloalkylammonium compounds |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015529608A JP2015529608A (ja) | 2015-10-08 |
| JP2015529608A5 true JP2015529608A5 (cg-RX-API-DMAC7.html) | 2016-07-21 |
| JP6227634B2 JP6227634B2 (ja) | 2017-11-08 |
Family
ID=49711486
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015515625A Active JP6227634B2 (ja) | 2012-06-04 | 2013-06-03 | Ｃｈａ型ゼオライト材料、及びシクロアルキルアンモニウム化合物を用いるそれらの製造方法 |
Country Status (11)
| Country | Link |
|---|---|
| EP (1) | EP2855354B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JP6227634B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR102108057B1 (cg-RX-API-DMAC7.html) |
| CN (2) | CN104520235A (cg-RX-API-DMAC7.html) |
| BR (1) | BR112014030263B1 (cg-RX-API-DMAC7.html) |
| CA (1) | CA2875700C (cg-RX-API-DMAC7.html) |
| MX (1) | MX363327B (cg-RX-API-DMAC7.html) |
| PL (1) | PL2855354T3 (cg-RX-API-DMAC7.html) |
| RU (1) | RU2627399C2 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2013182974A1 (cg-RX-API-DMAC7.html) |
| ZA (1) | ZA201409466B (cg-RX-API-DMAC7.html) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015185625A2 (en) * | 2014-06-05 | 2015-12-10 | Basf Se | Cha type zeolitic materials and methods for their preparation using combinations of cycloalkyl- and tetraalkylammonium compounds |
| JP6451743B2 (ja) * | 2014-10-31 | 2019-01-16 | 東亞合成株式会社 | 揮発性有機物質用消臭剤及びこれを用いた消臭性加工品、並びに揮発性有機物質用消臭剤及び消臭性加工品の製造方法 |
| ES2574500B1 (es) * | 2014-12-17 | 2017-03-31 | Consejo Superior De Investigaciones Científicas (Csic) | Síntesis de la zeolita con la estructura cristalina CHA, procedimiento de síntesis y su uso en aplicaciones catalíticas |
| KR102659804B1 (ko) * | 2015-12-09 | 2024-04-23 | 바스프 코포레이션 | Cha-형 제올라이트 물질 및 사이클로알킬- 및 에틸트라이메틸암모늄 화합물의 조합을 사용하는 이의 제조 방법 |
| WO2017204212A1 (ja) * | 2016-05-23 | 2017-11-30 | 東ソー株式会社 | Ｃｈａ型ゼオライト及びその製造方法 |
| WO2018064273A1 (en) * | 2016-09-30 | 2018-04-05 | Johnson Matthey Public Limited Company | A novel zeolite synthesis with a fluoride source |
| JP2020502020A (ja) | 2016-12-21 | 2020-01-23 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | 無溶媒ゼオライト転換によってゼオライト材料を製造する方法 |
| BR112019021877A2 (pt) | 2017-05-15 | 2020-05-26 | Basf Corporation | Processo para preparar um material zeolítico, material zeolítico e uso de um material zeolítico |
| JP7229175B2 (ja) | 2017-05-15 | 2023-02-27 | ビーエーエスエフ コーポレーション | 金属ｍを含み、フレームワークタイプａｅｉを有するゼオライト系材料を製造する方法 |
| MY190284A (en) * | 2017-10-11 | 2022-04-12 | Tosoh Corp | Metal-containing cha-type zeolite and method for producing the same |
| US11897778B2 (en) | 2017-11-22 | 2024-02-13 | Basf Se | Zeolite synthesis in a reactor with controlled velocity profile |
| CN110240179B (zh) * | 2018-03-09 | 2021-05-07 | 国家能源投资集团有限责任公司 | Sapo-34分子筛及其制备方法和应用 |
| US20210138441A1 (en) * | 2018-05-14 | 2021-05-13 | Umicore Ag & Co. Kg | Stable CHA Zeolites |
| EP3793727B1 (en) * | 2018-05-14 | 2022-06-22 | UMICORE AG & Co. KG | Stable small-pore zeolites |
| EP3830032A1 (en) * | 2018-08-02 | 2021-06-09 | Basf Se | Process for a continuous synthesis of zeolitic materials using seed crystals loaded with organotemplate |
| US11667536B2 (en) | 2018-08-24 | 2023-06-06 | Umicore Ag & Co. Kg | Method for the preparation of a molecular sieve of the CHA-type |
| US11219885B2 (en) * | 2018-11-30 | 2022-01-11 | Johnson Matthey Public Limited Company | JMZ-1, a CHA-containing zeolite and methods of preparation |
| JP7572009B2 (ja) | 2018-12-19 | 2024-10-23 | ビーエーエスエフ ソシエタス・ヨーロピア | Ｃｈａ型ゼオライト材料、及びシクロアルキルアンモニウム化合物とヒドロキシアルキルアンモニウム化合物との組み合わせを使用するその製造方法 |
| WO2020156506A1 (en) * | 2019-01-31 | 2020-08-06 | Basf Se | A zeolitic material having framework type cha |
| JP2022523138A (ja) * | 2019-03-14 | 2022-04-21 | ジョンソン、マッセイ、パブリック、リミテッド、カンパニー | Ｃｈａ含有モレキュラーシーブであるｊｍｚ－１ｓ及びその調製方法 |
| GB2584775B (en) | 2019-03-28 | 2022-08-10 | Johnson Matthey Plc | Molecular sieve intergrowths of cha and aft having an "sfw-GME tail", methods of preparation and use |
| WO2020225409A1 (en) | 2019-05-09 | 2020-11-12 | Basf Se | Process for a continuous synthesis of a cha zeolitic material from an emulsion |
| CN110975924B (zh) * | 2019-11-19 | 2021-12-07 | 上海应用技术大学 | 环己烯催化氧化制环己酮反应催化剂及制备方法和应用 |
| CN111871450A (zh) * | 2020-08-10 | 2020-11-03 | 中触媒新材料股份有限公司 | 一种cha结构分子筛及其尾气脱硝催化剂的制备方法与应用 |
| CN111871452A (zh) * | 2020-08-10 | 2020-11-03 | 中触媒新材料股份有限公司 | 一种用于柴油车尾气净化cha型分子筛、催化剂及制备方法与应用 |
| US20230211327A1 (en) | 2020-08-28 | 2023-07-06 | Tosoh Corporation | Cha-type zeolite and method for producing the same |
| EP4015454A1 (en) * | 2020-12-21 | 2022-06-22 | Tosoh Corporation | Cha-type zeolite and manufacturing method thereof |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6709644B2 (en) | 2001-08-30 | 2004-03-23 | Chevron U.S.A. Inc. | Small crystallite zeolite CHA |
| JP4508654B2 (ja) * | 2002-03-15 | 2010-07-21 | エクソンモービル・ケミカル・パテンツ・インク | 高シリカシャバサイト、その合成及びオキシジェネート類のオレフィン類への変換におけるその使用 |
| US6793901B2 (en) * | 2002-06-12 | 2004-09-21 | Exxonmobil Chemical Patents, Inc. | Synthesis of molecular sieves having the CHA framework type |
| US7247287B2 (en) * | 2003-06-11 | 2007-07-24 | Exxonmobil Chemical Patents Inc. | Synthesis of aluminophosphates and silicoaluminophosphates |
| US7094389B2 (en) * | 2003-12-23 | 2006-08-22 | Exxonmobil Chemical Patents Inc. | Chabazite-containing molecular sieve, its synthesis and its use in the conversion of oxygenates to olefins |
| US7090814B2 (en) * | 2004-11-10 | 2006-08-15 | Exxonmobil Chemical Patents Inc. | Method of synthesizing silicoaluminophosphate molecular sieves |
| US8048402B2 (en) * | 2005-08-18 | 2011-11-01 | Exxonmobil Chemical Patents Inc. | Synthesis of molecular sieves having the chabazite framework type and their use in the conversion of oxygenates to olefins |
| US7754187B2 (en) * | 2005-10-31 | 2010-07-13 | Exxonmobil Chemical Patents Inc. | Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins |
| WO2007053239A1 (en) * | 2005-10-31 | 2007-05-10 | Exxonmobil Chemical Patents Inc. | Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins |
| CN101489674B (zh) * | 2006-06-09 | 2011-12-14 | 埃克森美孚化学专利公司 | Cha型分子筛的处理及其在含氧物转化成烯烃中的用途 |
| CN101528342B (zh) * | 2006-09-25 | 2012-09-26 | 雪佛龙美国公司 | 使用结构导向剂和n，n，n-三烷基苄基季铵阳离子制备分子筛 |
| US8007764B2 (en) * | 2006-12-27 | 2011-08-30 | Chevron U.S.A. Inc. | Preparation of molecular sieve SSZ-13 |
| US8715618B2 (en) * | 2008-05-21 | 2014-05-06 | Basf Se | Process for the direct synthesis of Cu containing zeolites having CHA structure |
| US8182780B2 (en) * | 2008-07-25 | 2012-05-22 | Exxonmobil Chemical Patents Inc. | Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins |
| US8242041B2 (en) * | 2009-01-12 | 2012-08-14 | Exxonmobil Chemical Patents Inc. | Oxygenate conversion catalyst system and processes for making and using same |
| US8409546B2 (en) * | 2009-11-24 | 2013-04-02 | Basf Se | Process for the preparation of zeolites having B-CHA structure |
-
2013
- 2013-06-03 CN CN201380041292.7A patent/CN104520235A/zh active Pending
- 2013-06-03 WO PCT/IB2013/054569 patent/WO2013182974A1/en not_active Ceased
- 2013-06-03 PL PL13800386T patent/PL2855354T3/pl unknown
- 2013-06-03 KR KR1020147037062A patent/KR102108057B1/ko active Active
- 2013-06-03 CN CN201710994745.8A patent/CN107673366A/zh active Pending
- 2013-06-03 RU RU2014153662A patent/RU2627399C2/ru active
- 2013-06-03 JP JP2015515625A patent/JP6227634B2/ja active Active
- 2013-06-03 BR BR112014030263-4A patent/BR112014030263B1/pt active IP Right Grant
- 2013-06-03 MX MX2014014893A patent/MX363327B/es unknown
- 2013-06-03 CA CA2875700A patent/CA2875700C/en active Active
- 2013-06-03 EP EP13800386.8A patent/EP2855354B1/en active Active
-
2014
- 2014-12-22 ZA ZA2014/09466A patent/ZA201409466B/en unknown
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