JP2013529587A5 - - Google Patents

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Publication number

JP2013529587A5

JP2013529587A5 JP2013514836A JP2013514836A JP2013529587A5 JP 2013529587 A5 JP2013529587 A5 JP 2013529587A5 JP 2013514836 A JP2013514836 A JP 2013514836A JP 2013514836 A JP2013514836 A JP 2013514836A JP 2013529587 A5 JP2013529587 A5 JP 2013529587A5

Authority

JP

Japan

Prior art keywords

zeolitic material

lev

mixture

framework structure

molar ratio

Prior art date

2011-06-17

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Granted

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• 238000000034 method Methods 0.000 claims 32
• 239000000463 material Substances 0.000 claims 24
• 239000000203 mixture Substances 0.000 claims 19
• 239000010457 zeolite Substances 0.000 claims 8
• 239000013078 crystal Substances 0.000 claims 7
• 238000002425 crystallisation Methods 0.000 claims 7
• 230000008025 crystallization Effects 0.000 claims 7
• 150000001340 alkali metals Chemical class 0.000 claims 3
• 239000002904 solvent Substances 0.000 claims 3
• 238000006467 substitution reaction Methods 0.000 claims 3
• VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 2
• 229910021536 Zeolite Inorganic materials 0.000 claims 2
• 229910052783 alkali metal Inorganic materials 0.000 claims 2
• 239000003054 catalyst Substances 0.000 claims 2
• HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 2
• 238000010438 heat treatment Methods 0.000 claims 2
• 238000002441 X-ray diffraction Methods 0.000 claims 1
• 239000003463 adsorbent Substances 0.000 claims 1
• AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims 1
• 229910052782 aluminium Inorganic materials 0.000 claims 1
• 229910052796 boron Inorganic materials 0.000 claims 1
• 238000001354 calcination Methods 0.000 claims 1
• UNYSKUBLZGJSLV-UHFFFAOYSA-L calcium;1,3,5,2,4,6$l^{2}-trioxadisilaluminane 2,4-dioxide;dihydroxide;hexahydrate Chemical compound O.O.O.O.O.O.[OH-].[OH-].[Ca+2].O=[Si]1O[Al]O[Si](=O)O1.O=[Si]1O[Al]O[Si](=O)O1 UNYSKUBLZGJSLV-UHFFFAOYSA-L 0.000 claims 1
• 125000002091 cationic group Chemical group 0.000 claims 1
• 150000001768 cations Chemical group 0.000 claims 1
• 229910052676 chabazite Inorganic materials 0.000 claims 1
• 238000001035 drying Methods 0.000 claims 1
• 238000010304 firing Methods 0.000 claims 1
• 229910052733 gallium Inorganic materials 0.000 claims 1
• 229910052732 germanium Inorganic materials 0.000 claims 1
• 229910052738 indium Inorganic materials 0.000 claims 1
• 238000005342 ion exchange Methods 0.000 claims 1
• 238000004519 manufacturing process Methods 0.000 claims 1
• 239000002808 molecular sieve Substances 0.000 claims 1
• 239000002798 polar solvent Substances 0.000 claims 1
• 238000000634 powder X-ray diffraction Methods 0.000 claims 1
• 229910052710 silicon Inorganic materials 0.000 claims 1
• 239000000377 silicon dioxide Substances 0.000 claims 1
• URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims 1
• 238000003756 stirring Methods 0.000 claims 1
• 229910052718 tin Inorganic materials 0.000 claims 1
• 229910052719 titanium Inorganic materials 0.000 claims 1
• 238000005406 washing Methods 0.000 claims 1
• 229910052726 zirconium Inorganic materials 0.000 claims 1