JP2015529608A5 - - Google Patents
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- Publication number
- JP2015529608A5 JP2015529608A5 JP2015515625A JP2015515625A JP2015529608A5 JP 2015529608 A5 JP2015529608 A5 JP 2015529608A5 JP 2015515625 A JP2015515625 A JP 2015515625A JP 2015515625 A JP2015515625 A JP 2015515625A JP 2015529608 A5 JP2015529608 A5 JP 2015529608A5
- Authority
- JP
- Japan
- Prior art keywords
- zeolitic material
- mixture
- range
- cha
- absorption band
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 32
- 239000000463 material Substances 0.000 claims 22
- 239000000203 mixture Substances 0.000 claims 21
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 7
- 238000010521 absorption reaction Methods 0.000 claims 7
- 150000001875 compounds Chemical class 0.000 claims 6
- -1 tetraalkylammonium cations Chemical class 0.000 claims 5
- 238000002835 absorbance Methods 0.000 claims 4
- 238000002425 crystallisation Methods 0.000 claims 4
- 230000008025 crystallization Effects 0.000 claims 4
- 239000010457 zeolite Substances 0.000 claims 4
- 229910052676 chabazite Inorganic materials 0.000 claims 3
- 238000005004 MAS NMR spectroscopy Methods 0.000 claims 2
- 229910052782 aluminium Inorganic materials 0.000 claims 2
- 229910052796 boron Inorganic materials 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- 239000013078 crystal Substances 0.000 claims 2
- 125000000753 cycloalkyl group Chemical group 0.000 claims 2
- 229910052733 gallium Inorganic materials 0.000 claims 2
- 229910052732 germanium Inorganic materials 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 229910052738 indium Inorganic materials 0.000 claims 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims 2
- 229910052710 silicon Inorganic materials 0.000 claims 2
- 235000012239 silicon dioxide Nutrition 0.000 claims 2
- 239000000377 silicon dioxide Substances 0.000 claims 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims 2
- 238000006467 substitution reaction Methods 0.000 claims 2
- 229910052718 tin Inorganic materials 0.000 claims 2
- 229910052719 titanium Inorganic materials 0.000 claims 2
- 229910052726 zirconium Inorganic materials 0.000 claims 2
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 claims 1
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 claims 1
- 101100008649 Caenorhabditis elegans daf-5 gene Proteins 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- 229910018557 Si O Inorganic materials 0.000 claims 1
- 239000004115 Sodium Silicate Substances 0.000 claims 1
- 238000002441 X-ray diffraction Methods 0.000 claims 1
- 229910021536 Zeolite Inorganic materials 0.000 claims 1
- 239000003463 adsorbent Substances 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims 1
- 150000004645 aluminates Chemical class 0.000 claims 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- YOUGRGFIHBUKRS-UHFFFAOYSA-N benzyl(trimethyl)azanium Chemical compound C[N+](C)(C)CC1=CC=CC=C1 YOUGRGFIHBUKRS-UHFFFAOYSA-N 0.000 claims 1
- UNYSKUBLZGJSLV-UHFFFAOYSA-L calcium;1,3,5,2,4,6$l^{2}-trioxadisilaluminane 2,4-dioxide;dihydroxide;hexahydrate Chemical compound O.O.O.O.O.O.[OH-].[OH-].[Ca+2].O=[Si]1O[Al]O[Si](=O)O1.O=[Si]1O[Al]O[Si](=O)O1 UNYSKUBLZGJSLV-UHFFFAOYSA-L 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 239000008119 colloidal silica Substances 0.000 claims 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- 229910021485 fumed silica Inorganic materials 0.000 claims 1
- 238000002329 infrared spectrum Methods 0.000 claims 1
- 230000010354 integration Effects 0.000 claims 1
- 238000005342 ion exchange Methods 0.000 claims 1
- 150000002500 ions Chemical class 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 150000002739 metals Chemical class 0.000 claims 1
- 239000002808 molecular sieve Substances 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 235000019353 potassium silicate Nutrition 0.000 claims 1
- 238000000634 powder X-ray diffraction Methods 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 229910002027 silica gel Inorganic materials 0.000 claims 1
- 239000000741 silica gel Substances 0.000 claims 1
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Inorganic materials [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims 1
- 235000019795 sodium metasilicate Nutrition 0.000 claims 1
- 229910052911 sodium silicate Inorganic materials 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12170709 | 2012-06-04 | ||
| EP12170709.5 | 2012-06-04 | ||
| PCT/IB2013/054569 WO2013182974A1 (en) | 2012-06-04 | 2013-06-03 | Cha type zeolitic materials and methods for their preparation using cycloalkylammonium compounds |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015529608A JP2015529608A (ja) | 2015-10-08 |
| JP2015529608A5 true JP2015529608A5 (OSRAM) | 2016-07-21 |
| JP6227634B2 JP6227634B2 (ja) | 2017-11-08 |
Family
ID=49711486
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015515625A Active JP6227634B2 (ja) | 2012-06-04 | 2013-06-03 | Ｃｈａ型ゼオライト材料、及びシクロアルキルアンモニウム化合物を用いるそれらの製造方法 |
Country Status (11)
| Country | Link |
|---|---|
| EP (1) | EP2855354B1 (OSRAM) |
| JP (1) | JP6227634B2 (OSRAM) |
| KR (1) | KR102108057B1 (OSRAM) |
| CN (2) | CN107673366A (OSRAM) |
| BR (1) | BR112014030263B1 (OSRAM) |
| CA (1) | CA2875700C (OSRAM) |
| MX (1) | MX363327B (OSRAM) |
| PL (1) | PL2855354T3 (OSRAM) |
| RU (1) | RU2627399C2 (OSRAM) |
| WO (1) | WO2013182974A1 (OSRAM) |
| ZA (1) | ZA201409466B (OSRAM) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6698555B2 (ja) * | 2014-06-05 | 2020-05-27 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | Ｃｈａ型ゼオライト材料、並びに、シクロアルキル−及びテトラアルキルアンモニウム化合物を使用するそれらの製造方法 |
| CN107073155B (zh) * | 2014-10-31 | 2020-07-28 | 东亚合成株式会社 | 消臭剂及使用其的消臭性加工品、以及消臭剂及消臭性加工品的制造方法 |
| ES2574500B1 (es) * | 2014-12-17 | 2017-03-31 | Consejo Superior De Investigaciones Científicas (Csic) | Síntesis de la zeolita con la estructura cristalina CHA, procedimiento de síntesis y su uso en aplicaciones catalíticas |
| US10913660B2 (en) | 2015-12-09 | 2021-02-09 | Basf Corporation | CHA type zeolitic materials and methods for their preparation using combinations of cycloalkyl and ethyltrimethylammonium compounds |
| US10953390B2 (en) | 2016-05-23 | 2021-03-23 | Tosoh Corporation | CHA-type zeolite and method for producing the same |
| KR102594931B1 (ko) * | 2016-09-30 | 2023-10-30 | 존슨 맛쎄이 퍼블릭 리미티드 컴파니 | 플루오라이드 공급원을 사용한 신규한 제올라이트 합성 |
| KR20190100946A (ko) | 2016-12-21 | 2019-08-29 | 바스프 에스이 | 무용매 제올라이트간 전환을 통한 제올라이트계 물질의 제조 방법 |
| KR102581566B1 (ko) | 2017-05-15 | 2023-09-25 | 바스프 코포레이션 | 금속 m을 포함하고 골격 유형 aei를 갖는 제올라이트 물질을 제조하는 방법 |
| BR112019021877A2 (pt) | 2017-05-15 | 2020-05-26 | Basf Corporation | Processo para preparar um material zeolítico, material zeolítico e uso de um material zeolítico |
| MY190284A (en) * | 2017-10-11 | 2022-04-12 | Tosoh Corp | Metal-containing cha-type zeolite and method for producing the same |
| WO2019101854A1 (en) | 2017-11-22 | 2019-05-31 | Basf Se | Zeolite synthesis in a reactor with controlled velocity profile |
| CN110240179B (zh) * | 2018-03-09 | 2021-05-07 | 国家能源投资集团有限责任公司 | Sapo-34分子筛及其制备方法和应用 |
| US20210138441A1 (en) * | 2018-05-14 | 2021-05-13 | Umicore Ag & Co. Kg | Stable CHA Zeolites |
| KR102746625B1 (ko) * | 2018-05-14 | 2024-12-30 | 우미코레 아게 운트 코 카게 | 안정한 소형 공극 제올라이트 |
| WO2020025799A1 (en) * | 2018-08-02 | 2020-02-06 | Basf Se | Process for a continuous synthesis of zeolitic materials using seed crystals loaded with organotemplate |
| CN112654582A (zh) | 2018-08-24 | 2021-04-13 | 优米科尔股份公司及两合公司 | Cha型分子筛的制备方法 |
| US11219885B2 (en) * | 2018-11-30 | 2022-01-11 | Johnson Matthey Public Limited Company | JMZ-1, a CHA-containing zeolite and methods of preparation |
| EP3898513A1 (en) | 2018-12-19 | 2021-10-27 | Basf Se | Cha type zeolitic materials and methods for their preparation |
| WO2020156506A1 (en) * | 2019-01-31 | 2020-08-06 | Basf Se | A zeolitic material having framework type cha |
| GB2589156B (en) * | 2019-03-14 | 2022-06-01 | Johnson Matthey Plc | JMZ-1S, a CHA-containing molecular sieve and methods of preparation |
| EP3947284A1 (en) * | 2019-03-28 | 2022-02-09 | Johnson Matthey Public Limited Company | Molecular sieve intergrowths ofcha |
| WO2020225409A1 (en) | 2019-05-09 | 2020-11-12 | Basf Se | Process for a continuous synthesis of a cha zeolitic material from an emulsion |
| CN110975924B (zh) * | 2019-11-19 | 2021-12-07 | 上海应用技术大学 | 环己烯催化氧化制环己酮反应催化剂及制备方法和应用 |
| CN111871452A (zh) * | 2020-08-10 | 2020-11-03 | 中触媒新材料股份有限公司 | 一种用于柴油车尾气净化cha型分子筛、催化剂及制备方法与应用 |
| CN111871450A (zh) * | 2020-08-10 | 2020-11-03 | 中触媒新材料股份有限公司 | 一种cha结构分子筛及其尾气脱硝催化剂的制备方法与应用 |
| CN116096479A (zh) | 2020-08-28 | 2023-05-09 | 东曹株式会社 | 一种cha型沸石及其制备方法 |
| EP4015454A1 (en) * | 2020-12-21 | 2022-06-22 | Tosoh Corporation | Cha-type zeolite and manufacturing method thereof |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6709644B2 (en) | 2001-08-30 | 2004-03-23 | Chevron U.S.A. Inc. | Small crystallite zeolite CHA |
| WO2003078324A1 (en) * | 2002-03-15 | 2003-09-25 | Exxonmobil Chemical Patents Inc. | High silica chabazite, its synthesis and its use in the conversion of oxygenates to olefins |
| US6793901B2 (en) * | 2002-06-12 | 2004-09-21 | Exxonmobil Chemical Patents, Inc. | Synthesis of molecular sieves having the CHA framework type |
| US7247287B2 (en) * | 2003-06-11 | 2007-07-24 | Exxonmobil Chemical Patents Inc. | Synthesis of aluminophosphates and silicoaluminophosphates |
| CA2548315C (en) * | 2003-12-23 | 2009-07-14 | Exxonmobil Chemical Patents Inc. | Chabazite-containing molecular sieve, its synthesis and its use in the conversion of oxygenates to olefins |
| US7090814B2 (en) * | 2004-11-10 | 2006-08-15 | Exxonmobil Chemical Patents Inc. | Method of synthesizing silicoaluminophosphate molecular sieves |
| US8048402B2 (en) * | 2005-08-18 | 2011-11-01 | Exxonmobil Chemical Patents Inc. | Synthesis of molecular sieves having the chabazite framework type and their use in the conversion of oxygenates to olefins |
| WO2007053239A1 (en) * | 2005-10-31 | 2007-05-10 | Exxonmobil Chemical Patents Inc. | Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins |
| US7754187B2 (en) * | 2005-10-31 | 2010-07-13 | Exxonmobil Chemical Patents Inc. | Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins |
| CN101489674B (zh) * | 2006-06-09 | 2011-12-14 | 埃克森美孚化学专利公司 | Cha型分子筛的处理及其在含氧物转化成烯烃中的用途 |
| JP5662021B2 (ja) * | 2006-09-25 | 2015-01-28 | シェブロン ユー．エス．エー． インコーポレイテッド | 構造指向剤およびｎ，ｎ，ｎ−トリアルキルベンジル４級アンモニウムカチオンを用いたモレキュラーシーブの調製 |
| US8007764B2 (en) * | 2006-12-27 | 2011-08-30 | Chevron U.S.A. Inc. | Preparation of molecular sieve SSZ-13 |
| CN102099293B (zh) * | 2008-05-21 | 2014-03-26 | 巴斯夫欧洲公司 | 直接合成具有CHA结构的含Cu沸石的方法 |
| US8268277B2 (en) * | 2008-07-25 | 2012-09-18 | Exxonmobil Chemical Patents Inc. | Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins |
| US8242041B2 (en) * | 2009-01-12 | 2012-08-14 | Exxonmobil Chemical Patents Inc. | Oxygenate conversion catalyst system and processes for making and using same |
| US8409546B2 (en) * | 2009-11-24 | 2013-04-02 | Basf Se | Process for the preparation of zeolites having B-CHA structure |
-
2013
- 2013-06-03 PL PL13800386T patent/PL2855354T3/pl unknown
- 2013-06-03 CN CN201710994745.8A patent/CN107673366A/zh active Pending
- 2013-06-03 BR BR112014030263-4A patent/BR112014030263B1/pt active IP Right Grant
- 2013-06-03 KR KR1020147037062A patent/KR102108057B1/ko active Active
- 2013-06-03 JP JP2015515625A patent/JP6227634B2/ja active Active
- 2013-06-03 CA CA2875700A patent/CA2875700C/en active Active
- 2013-06-03 WO PCT/IB2013/054569 patent/WO2013182974A1/en not_active Ceased
- 2013-06-03 EP EP13800386.8A patent/EP2855354B1/en active Active
- 2013-06-03 RU RU2014153662A patent/RU2627399C2/ru active
- 2013-06-03 CN CN201380041292.7A patent/CN104520235A/zh active Pending
- 2013-06-03 MX MX2014014893A patent/MX363327B/es unknown
-
2014
- 2014-12-22 ZA ZA2014/09466A patent/ZA201409466B/en unknown
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