JP2015501276A5 - - Google Patents
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- Publication number
- JP2015501276A5 JP2015501276A5 JP2014535857A JP2014535857A JP2015501276A5 JP 2015501276 A5 JP2015501276 A5 JP 2015501276A5 JP 2014535857 A JP2014535857 A JP 2014535857A JP 2014535857 A JP2014535857 A JP 2014535857A JP 2015501276 A5 JP2015501276 A5 JP 2015501276A5
- Authority
- JP
- Japan
- Prior art keywords
- ium
- formula
- reaction mixture
- methylpiperidin
- diyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 27
- 239000011541 reaction mixture Substances 0.000 claims 10
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 6
- 239000002808 molecular sieve Substances 0.000 claims 4
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims 4
- PAMIQIKDUOTOBW-UHFFFAOYSA-N 1-methylpiperidine Chemical compound CN1CCCCC1 PAMIQIKDUOTOBW-UHFFFAOYSA-N 0.000 claims 3
- 239000003513 alkali Substances 0.000 claims 3
- 150000001342 alkaline earth metals Chemical class 0.000 claims 3
- 239000013078 crystal Substances 0.000 claims 3
- ZPALNACUHMMGIU-UHFFFAOYSA-N 1-[4-(1-methylpiperidin-1-ium-1-yl)butyl]-1-azoniabicyclo[2.2.2]octan-3-ol Chemical compound C1CC(C(O)C2)CC[N+]12CCCC[N+]1(C)CCCCC1 ZPALNACUHMMGIU-UHFFFAOYSA-N 0.000 claims 2
- ZENRZVVLGKAAGY-UHFFFAOYSA-N 1-methyl-1-[4-(1-methylpiperidin-1-ium-1-yl)butyl]piperidin-1-ium Chemical compound C1CCCC[N+]1(C)CCCC[N+]1(C)CCCCC1 ZENRZVVLGKAAGY-UHFFFAOYSA-N 0.000 claims 2
- SHVYPTOWNDGXEG-UHFFFAOYSA-N 1-methyl-1-[6-(1-methylpiperidin-1-ium-1-yl)hexyl]piperidin-1-ium Chemical compound C1CCCC[N+]1(C)CCCCCC[N+]1(C)CCCCC1 SHVYPTOWNDGXEG-UHFFFAOYSA-N 0.000 claims 2
- PAMIQIKDUOTOBW-UHFFFAOYSA-O 1-methylpiperidin-1-ium Chemical compound C[NH+]1CCCCC1 PAMIQIKDUOTOBW-UHFFFAOYSA-O 0.000 claims 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 2
- 229910052782 aluminium Inorganic materials 0.000 claims 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 2
- 125000004432 carbon atom Chemical group C* 0.000 claims 2
- 238000002425 crystallisation Methods 0.000 claims 2
- 230000008025 crystallization Effects 0.000 claims 2
- 239000000203 mixture Substances 0.000 claims 2
- 229910052700 potassium Inorganic materials 0.000 claims 2
- 239000011591 potassium Substances 0.000 claims 2
- SBYHFKPVCBCYGV-UHFFFAOYSA-N quinuclidine Chemical group C1CC2CCN1CC2 SBYHFKPVCBCYGV-UHFFFAOYSA-N 0.000 claims 2
- 229910052710 silicon Inorganic materials 0.000 claims 2
- 239000010703 silicon Substances 0.000 claims 2
- LPSCAAJINWAJSC-UHFFFAOYSA-N 1-[5-(1-methylpiperidin-1-ium-1-yl)pentyl]-1-azoniabicyclo[2.2.2]octan-3-ol Chemical compound C1CC(C(O)C2)CC[N+]12CCCCC[N+]1(C)CCCCC1 LPSCAAJINWAJSC-UHFFFAOYSA-N 0.000 claims 1
- RYGUIMZKXUZJHP-UHFFFAOYSA-N 1-methyl-1-[5-(1-methylpiperidin-1-ium-1-yl)pentyl]piperidin-1-ium Chemical compound C1CCCC[N+]1(C)CCCCC[N+]1(C)CCCCC1 RYGUIMZKXUZJHP-UHFFFAOYSA-N 0.000 claims 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims 1
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- 238000002441 X-ray diffraction Methods 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 150000008064 anhydrides Chemical class 0.000 claims 1
- 229910052796 boron Inorganic materials 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- 239000011651 chromium Substances 0.000 claims 1
- 238000005336 cracking Methods 0.000 claims 1
- 125000002993 cycloalkylene group Chemical group 0.000 claims 1
- 229910052733 gallium Inorganic materials 0.000 claims 1
- 229910052732 germanium Inorganic materials 0.000 claims 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims 1
- 150000002892 organic cations Chemical class 0.000 claims 1
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 claims 1
- -1 polymethylene group Polymers 0.000 claims 1
- 239000011148 porous material Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 230000002194 synthesizing effect Effects 0.000 claims 1
- 229910052718 tin Inorganic materials 0.000 claims 1
- 239000011135 tin Substances 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- 239000010936 titanium Substances 0.000 claims 1
- 229910052720 vanadium Inorganic materials 0.000 claims 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161546335P | 2011-10-12 | 2011-10-12 | |
| US61/546,335 | 2011-10-12 | ||
| PCT/US2012/059678 WO2013055871A1 (en) | 2011-10-12 | 2012-10-11 | Synthesis of mse-framework type molecular sieves |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015501276A JP2015501276A (ja) | 2015-01-15 |
| JP2015501276A5 true JP2015501276A5 (enExample) | 2015-07-09 |
| JP5906320B2 JP5906320B2 (ja) | 2016-04-20 |
Family
ID=47116413
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014535857A Active JP5906320B2 (ja) | 2011-10-12 | 2012-10-11 | Ｍｓｅフレームワーク型モレキュラーシーブの合成 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US8916130B2 (enExample) |
| EP (1) | EP2766303B1 (enExample) |
| JP (1) | JP5906320B2 (enExample) |
| KR (1) | KR101996105B1 (enExample) |
| CN (1) | CN103874656B (enExample) |
| CA (1) | CA2849923C (enExample) |
| SG (1) | SG11201400503WA (enExample) |
| WO (1) | WO2013055871A1 (enExample) |
| ZA (1) | ZA201402691B (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104781191B (zh) | 2012-11-16 | 2017-12-12 | 埃克森美孚研究工程公司 | Mse骨架型分子筛的合成 |
| JP6422488B2 (ja) * | 2013-06-10 | 2018-11-14 | エクソンモービル ケミカル パテンツ インコーポレイテッド | モレキュラーシーブの製造方法 |
| US9187334B2 (en) * | 2013-10-11 | 2015-11-17 | Chevron U.S.A. Inc. | Molecular sieve SSZ-96 |
| US20160102590A1 (en) | 2014-10-14 | 2016-04-14 | Exxonmobil Research And Engineering Company | Methods of making porous crystalline materials and their use in hydrocarbon sorption |
| US9868643B2 (en) | 2016-05-20 | 2018-01-16 | Chevron U.S.A. Inc. | Synthesis of zeolite SSZ-16 |
| US10272420B2 (en) * | 2016-10-06 | 2019-04-30 | Uop Llc | Composition of matter and structure of zeolite UZM-55 |
| US10611645B2 (en) | 2016-10-06 | 2020-04-07 | Uop Llc | Zeolite having a one-dimensional channel system, 10-membered rings and 12-membered rings |
| WO2018071113A1 (en) * | 2016-10-11 | 2018-04-19 | Chevron U.S.A. Inc. | Synthesis of molecular sieve ssz-83 |
| JP7440530B2 (ja) | 2019-03-18 | 2024-02-28 | エクソンモービル テクノロジー アンド エンジニアリング カンパニー | メソ多孔性触媒化合物及びその使用 |
| FR3101341B1 (fr) * | 2019-09-26 | 2021-10-15 | Ifp Energies Now | Procede de preparation d’une zeolithe izm-2 en presence d’un structurant organique azote sous forme hydroxyde et d’un chlorure de metal alcalin, en milieu fluore ou non |
| JP2022068871A (ja) * | 2020-10-22 | 2022-05-10 | 東ソー株式会社 | 炭化水素吸着剤及び炭化水素の吸着方法 |
| US20250206623A1 (en) * | 2022-03-29 | 2025-06-26 | Sagami Chemical Research Institute | Cyclohexylenediaminium salt, use thereof, and mse-type zeolite obtained therefrom |
Family Cites Families (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3354078A (en) | 1965-02-04 | 1967-11-21 | Mobil Oil Corp | Catalytic conversion with a crystalline aluminosilicate activated with a metallic halide |
| US4391785A (en) | 1981-12-21 | 1983-07-05 | Mobil Oil Corporation | Preparation of ZSM-12 type zeolites |
| US4508837A (en) | 1982-09-28 | 1985-04-02 | Chevron Research Company | Zeolite SSZ-16 |
| US4481177A (en) | 1982-12-09 | 1984-11-06 | Mobil Oil Corporation | Synthesis of zeolite ZSM-22 with a heterocyclic organic compound |
| US4557919A (en) | 1983-04-12 | 1985-12-10 | Teijin Petrochemical Industries Ltd. | Production of crystalline zeolites |
| US4508337A (en) | 1984-03-23 | 1985-04-02 | Gillespie Jr C Earl | Basketball goal height reducing frame |
| US4689207A (en) | 1985-03-06 | 1987-08-25 | Chevron Research Company | Process for the preparation of crystalline microporous organosilicates using magadiite as a silica source |
| US5187132A (en) | 1991-05-14 | 1993-02-16 | Chevron Research And Technology Company | Preparation of borosilicate zeolites |
| US5225179A (en) * | 1992-08-27 | 1993-07-06 | Chevron Research And Technology Company | Method of making molecular sieves |
| US5591421A (en) * | 1994-07-11 | 1997-01-07 | Chevron U.S.A. Inc. | Zeolite SSZ-41 |
| FR2752567B1 (fr) | 1996-08-23 | 1998-10-16 | Inst Francais Du Petrole | Zeolithe nu-88, son procede de preparation et ses applications catalytiques |
| AU5614498A (en) | 1996-12-31 | 1998-07-31 | Chevron U.S.A. Inc. | A process for preparing zeolites using substituted-piperidinium cations |
| US6049018A (en) * | 1999-01-21 | 2000-04-11 | Mobil Corporation | Synthetic porous crystalline MCM-68, its synthesis and use |
| ES2155797B1 (es) | 1999-07-29 | 2001-12-01 | Univ Valencia Politecnica | Zeolita itq-10 |
| US7198711B1 (en) | 2000-01-21 | 2007-04-03 | Exxonmobil Research And Engineering Company | Catalytic cracking processing using an MCM-68 catalyst |
| JP2004010537A (ja) | 2002-06-06 | 2004-01-15 | Mitsubishi Chemicals Corp | 水熱合成用テンプレート、ケイ素含有層状化合物の製造方法及びケイ素含有層状化合物 |
| ES2247921B1 (es) | 2004-04-07 | 2007-06-16 | Universidad Politecnica De Valencia | Un material amorfo microporoso, procedimiento de preparacion y su uso en la conversion catalitica de compuestos organicos. |
| ES2263369B1 (es) | 2005-02-02 | 2007-12-16 | Universidad Politecnica De Valencia | Material cristalino microporoso de naturaleza zeolitica, zeolita itq-32, procedimiento de preparacion y uso. |
| US8562941B2 (en) * | 2005-12-20 | 2013-10-22 | Exxonmobil Research And Engineering Company | Perturbed synthesis of materials |
| WO2007079038A2 (en) | 2005-12-28 | 2007-07-12 | Chevron U.S.A Inc. | Molecular sieve ssz-74 composition of matter and synthesis thereof |
| FR2918050B1 (fr) | 2007-06-29 | 2011-05-06 | Inst Francais Du Petrole | Solide cristallise izm-2 et son procede de preparation |
| FR2924110B1 (fr) * | 2007-11-26 | 2010-02-26 | Inst Francais Du Petrole | Solide cristallise izm-3 et son procede de preparation |
| US8025863B2 (en) | 2008-06-20 | 2011-09-27 | Exxonmobil Research And Engineering Company | Synthesis and use of MSE-framework type molecular sieves |
| FR2934793B1 (fr) | 2008-08-08 | 2010-11-19 | Inst Francais Du Petrole | Catalyseur comprenant une zeolithe izm-2 et au moins un metal et son utilisation en transformation d'hydrocarbures |
| FR2934795B1 (fr) | 2008-08-08 | 2010-11-26 | Inst Francais Du Petrole | Catalyseur comprenant au moins une zeolithe izm-2 et son utilisation pour la transformation de charges hydrocarbonees |
| FR2934794B1 (fr) | 2008-08-08 | 2010-10-22 | Inst Francais Du Petrole | Procede de production de distillats moyens par hydrocraquage de charges issues du procede fischer-trospch en presence d'un catalyseur comprenant un solide izm-2 |
| FR2934796B1 (fr) | 2008-08-08 | 2010-09-03 | Inst Francais Du Petrole | Catalyseur a base de zeolithe izm-2 et procede d'hydroconversion/hydrocraquage de charges hydrocarbonees |
| JP2010159245A (ja) * | 2008-09-19 | 2010-07-22 | Sumitomo Chemical Co Ltd | 酸化化合物の製造方法 |
| US7922997B2 (en) | 2008-09-30 | 2011-04-12 | Uop Llc | UZM-35 aluminosilicate zeolite, method of preparation and processes using UZM-35 |
| FR2936791B1 (fr) | 2008-10-07 | 2011-05-06 | Inst Francais Du Petrole | Procede de preparation d'une zeolithe de type structural mfi |
| FR2936790B1 (fr) | 2008-10-07 | 2010-09-24 | Inst Francais Du Petrole | Procede de preparation d'une zeolithe de type structural mtw |
| US7648694B2 (en) | 2008-10-10 | 2010-01-19 | Chevron U.S.A. Inc. | Method for preparing SSZ-26/33 zeolites using novel structure directing agents |
| WO2010065319A2 (en) | 2008-11-25 | 2010-06-10 | Chevron U.S.A. Inc. | Processes using molecular sieve ssz-83 |
| US7998457B2 (en) | 2008-11-25 | 2011-08-16 | Chevron U.S.A. Inc. | Molecular sieve SSZ-83 |
| US8075871B2 (en) | 2008-11-25 | 2011-12-13 | Chevron U.S.A. Inc. | Method for making molecular sieve SSZ-83 |
| CA2744237C (en) * | 2008-11-25 | 2012-06-26 | Chevron U.S.A. Inc. | Molecular sieve ssz-83 |
| JP5953377B2 (ja) * | 2011-10-12 | 2016-07-20 | エクソンモービル リサーチ アンド エンジニアリング カンパニーＥｘｘｏｎ Ｒｅｓｅａｒｃｈ Ａｎｄ Ｅｎｇｉｎｅｅｒｉｎｇ Ｃｏｍｐａｎｙ | Ｍｓｅフレームワークタイプのモレキュラーシーブの合成 |
-
2012
- 2012-10-11 KR KR1020147012734A patent/KR101996105B1/ko not_active Expired - Fee Related
- 2012-10-11 CN CN201280050096.1A patent/CN103874656B/zh not_active Expired - Fee Related
- 2012-10-11 EP EP12780352.6A patent/EP2766303B1/en not_active Not-in-force
- 2012-10-11 JP JP2014535857A patent/JP5906320B2/ja active Active
- 2012-10-11 US US13/649,283 patent/US8916130B2/en not_active Expired - Fee Related
- 2012-10-11 CA CA2849923A patent/CA2849923C/en not_active Expired - Fee Related
- 2012-10-11 WO PCT/US2012/059678 patent/WO2013055871A1/en not_active Ceased
- 2012-10-11 SG SG11201400503WA patent/SG11201400503WA/en unknown
-
2014
- 2014-04-11 ZA ZA2014/02691A patent/ZA201402691B/en unknown
- 2014-11-14 US US14/541,777 patent/US9035058B2/en not_active Expired - Fee Related
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