JP2014515792A5 - - Google Patents
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- JP2014515792A5 JP2014515792A5 JP2014508399A JP2014508399A JP2014515792A5 JP 2014515792 A5 JP2014515792 A5 JP 2014515792A5 JP 2014508399 A JP2014508399 A JP 2014508399A JP 2014508399 A JP2014508399 A JP 2014508399A JP 2014515792 A5 JP2014515792 A5 JP 2014515792A5
- Authority
- JP
- Japan
- Prior art keywords
- molten
- titanium
- powder
- titanium alloy
- molten pool
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 62
- 239000000843 powder Substances 0.000 claims description 43
- 229910001069 Ti alloy Inorganic materials 0.000 claims description 37
- 229910045601 alloy Inorganic materials 0.000 claims description 35
- 239000000956 alloy Substances 0.000 claims description 35
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 32
- 239000002245 particle Substances 0.000 claims description 26
- 239000010936 titanium Substances 0.000 claims description 23
- 229910052719 titanium Inorganic materials 0.000 claims description 22
- 150000003839 salts Chemical class 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 18
- 229910052786 argon Inorganic materials 0.000 claims description 16
- 239000011261 inert gas Substances 0.000 claims description 15
- 239000011777 magnesium Substances 0.000 claims description 15
- 238000005275 alloying Methods 0.000 claims description 13
- 238000010438 heat treatment Methods 0.000 claims description 13
- 229910000883 Ti6Al4V Inorganic materials 0.000 claims description 12
- 238000003672 processing method Methods 0.000 claims description 12
- 238000004519 manufacturing process Methods 0.000 claims description 11
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 9
- 238000002844 melting Methods 0.000 claims description 9
- 230000008018 melting Effects 0.000 claims description 9
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 8
- 238000001704 evaporation Methods 0.000 claims description 8
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 7
- 229910052749 magnesium Inorganic materials 0.000 claims description 7
- 230000008569 process Effects 0.000 claims description 7
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims description 7
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- 239000003792 electrolyte Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 239000002184 metal Substances 0.000 claims description 6
- 229910052720 vanadium Inorganic materials 0.000 claims description 6
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 4
- 238000005507 spraying Methods 0.000 claims description 4
- 239000000155 melt Substances 0.000 claims description 3
- 230000006698 induction Effects 0.000 claims description 2
- 230000035515 penetration Effects 0.000 claims 3
- 238000003181 co-melting Methods 0.000 claims 2
- 239000012768 molten material Substances 0.000 claims 1
- 239000007921 spray Substances 0.000 claims 1
- 239000010419 fine particle Substances 0.000 description 9
- 239000007789 gas Substances 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 239000000758 substrate Substances 0.000 description 4
- 238000007664 blowing Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 238000001878 scanning electron micrograph Methods 0.000 description 3
- 229910020361 KCl—LiCl Inorganic materials 0.000 description 2
- 230000005674 electromagnetic induction Effects 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 2
- 238000007738 vacuum evaporation Methods 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- QYEXBYZXHDUPRC-UHFFFAOYSA-N B#[Ti]#B Chemical compound B#[Ti]#B QYEXBYZXHDUPRC-UHFFFAOYSA-N 0.000 description 1
- 229910052580 B4C Inorganic materials 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229910033181 TiB2 Inorganic materials 0.000 description 1
- NRTOMJZYCJJWKI-UHFFFAOYSA-N Titanium nitride Chemical compound [Ti]#N NRTOMJZYCJJWKI-UHFFFAOYSA-N 0.000 description 1
- 229910000756 V alloy Inorganic materials 0.000 description 1
- 229910002065 alloy metal Inorganic materials 0.000 description 1
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000010894 electron beam technology Methods 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 229910000449 hafnium oxide Inorganic materials 0.000 description 1
- WIHZLLGSGQNAGK-UHFFFAOYSA-N hafnium(4+);oxygen(2-) Chemical compound [O-2].[O-2].[Hf+4] WIHZLLGSGQNAGK-UHFFFAOYSA-N 0.000 description 1
- HCQWRNRRURULEY-UHFFFAOYSA-L lithium;potassium;dichloride Chemical compound [Li+].[Cl-].[Cl-].[K+] HCQWRNRRURULEY-UHFFFAOYSA-L 0.000 description 1
- 239000011812 mixed powder Substances 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 210000003625 skull Anatomy 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161517871P | 2011-04-27 | 2011-04-27 | |
| US61/517,871 | 2011-04-27 | ||
| PCT/US2012/033652 WO2012148714A1 (en) | 2011-04-27 | 2012-04-13 | Low cost processing to produce spherical titanium and titanium alloy powder |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2014515792A JP2014515792A (ja) | 2014-07-03 |
| JP2014515792A5 true JP2014515792A5 (https=) | 2017-01-12 |
Family
ID=47066869
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014508399A Pending JP2014515792A (ja) | 2011-04-27 | 2012-04-13 | 球状チタンおよび球状チタン合金粉末を生成する低コスト処理法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US8911529B2 (https=) |
| EP (1) | EP2701869B1 (https=) |
| JP (1) | JP2014515792A (https=) |
| KR (1) | KR20140027335A (https=) |
| CN (1) | CN103608141A (https=) |
| AU (1) | AU2012250152B2 (https=) |
| CA (1) | CA2834328A1 (https=) |
| PL (1) | PL2701869T3 (https=) |
| WO (1) | WO2012148714A1 (https=) |
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| KR102322229B1 (ko) | 2014-05-13 | 2021-11-05 | 더 유니버시티 오브 유타 리서치 파운데이션 | 실질적으로 구형인 금속 분말의 제조 |
| JP6665118B2 (ja) * | 2014-06-16 | 2020-03-13 | コモンウェルス サイエンティフィック アンド インダストリアル リサーチ オーガナイゼーション | 粉末生成物の製造方法 |
| CN104209526B (zh) * | 2014-08-26 | 2016-09-28 | 苏州智研新材料科技有限公司 | 一种微细球形钛合金粉体的制备方法 |
| EP3227038A4 (en) | 2014-12-02 | 2018-08-22 | University of Utah Research Foundation | Molten salt de-oxygenation of metal powders |
| US10987735B2 (en) | 2015-12-16 | 2021-04-27 | 6K Inc. | Spheroidal titanium metallic powders with custom microstructures |
| CA3009630C (en) * | 2015-12-16 | 2023-08-01 | Amastan Technologies Llc | Spheroidal dehydrogenated metals and metal alloy particles |
| CN105537602A (zh) * | 2015-12-25 | 2016-05-04 | 中国科学院重庆绿色智能技术研究院 | 一种3d打印用球形超高温合金粉末的快速规模化制备方法 |
| CN105562700A (zh) * | 2015-12-31 | 2016-05-11 | 龙岩紫荆创新研究院 | 一种用于3d打印的球形钛粉的等离子体制备方法 |
| CN105568055B (zh) * | 2016-01-06 | 2017-08-15 | 龙岩紫荆创新研究院 | 一种钛基合金球形粉末的等离子体制备方法 |
| CN105642879B (zh) * | 2016-01-14 | 2017-08-25 | 鞍山东大激光科技有限公司 | 用于激光3d打印的球形tc4钛合金粉末及其制备方法 |
| CN105903973A (zh) * | 2016-04-27 | 2016-08-31 | 龙岩紫荆创新研究院 | 一种球形钒粉的等离子体制备方法 |
| CN110199039B (zh) | 2016-10-21 | 2022-10-04 | 通用电气公司 | 通过还原四氯化钛制造钛合金材料 |
| AU2017390111B2 (en) | 2016-10-21 | 2021-12-09 | General Electric Company | Producing titanium alloy materials through reduction of titanium tetrahalide |
| CN106493377B (zh) * | 2016-12-29 | 2018-05-11 | 哈尔滨三地增材制造材料有限公司 | 环形排布对撞式气流雾化钛合金粉末制取设备及制取方法 |
| GB201701292D0 (en) * | 2017-01-26 | 2017-03-15 | Univ Ulster | Method and apparatus for producing nanoscale materials |
| KR102112602B1 (ko) | 2018-06-12 | 2020-05-19 | 한국과학기술연구원 | 메탈 3d 프린터용 금속분말 제조 장치 |
| CN112654444A (zh) | 2018-06-19 | 2021-04-13 | 6K有限公司 | 由原材料制造球化粉末的方法 |
| KR102247338B1 (ko) | 2018-12-14 | 2021-05-04 | 재단법인 포항산업과학연구원 | 입상 물질 제조 방법 및 제조 장치 |
| US11066308B2 (en) | 2019-02-05 | 2021-07-20 | United Technologies Corporation | Preparation of metal diboride and boron-doped powders |
| CN111590084B (zh) * | 2019-02-21 | 2022-02-22 | 刘丽 | 一种金属粉体材料的制备方法 |
| CN109750320B (zh) * | 2019-03-04 | 2019-12-13 | 海安县鹰球粉末冶金有限公司 | 雾化电解联合制备金属合金粉末的方法 |
| SG11202111576QA (en) | 2019-04-30 | 2021-11-29 | 6K Inc | Mechanically alloyed powder feedstock |
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| CN114641462A (zh) | 2019-11-18 | 2022-06-17 | 6K有限公司 | 用于球形粉末的独特原料及制造方法 |
| US11590568B2 (en) | 2019-12-19 | 2023-02-28 | 6K Inc. | Process for producing spheroidized powder from feedstock materials |
| CN113510246A (zh) * | 2020-03-25 | 2021-10-19 | 中国科学院过程工程研究所 | 一种Ti-6Al-4V合金粉的制备方法及由其制得的Ti-6Al-4V合金粉 |
| CA3180426A1 (en) | 2020-06-25 | 2021-12-30 | Richard K. Holman | Microcomposite alloy structure |
| AU2021349358A1 (en) | 2020-09-24 | 2023-02-09 | 6K Inc. | Systems, devices, and methods for starting plasma |
| CA3196653A1 (en) | 2020-10-30 | 2022-05-05 | Sunil Bhalchandra BADWE | Systems and methods for synthesis of spheroidized metal powders |
| CN112091229B (zh) * | 2020-11-09 | 2021-02-12 | 西安赛隆金属材料有限责任公司 | 一种细化金属粉末粒径的装置及方法 |
| AU2022206483A1 (en) | 2021-01-11 | 2023-08-31 | 6K Inc. | Methods and systems for reclamation of li-ion cathode materials using microwave plasma processing |
| WO2022212291A1 (en) | 2021-03-31 | 2022-10-06 | 6K Inc. | Systems and methods for additive manufacturing of metal nitride ceramics |
| WO2023229928A1 (en) | 2022-05-23 | 2023-11-30 | 6K Inc. | Microwave plasma apparatus and methods for processing materials using an interior liner |
| US12040162B2 (en) | 2022-06-09 | 2024-07-16 | 6K Inc. | Plasma apparatus and methods for processing feed material utilizing an upstream swirl module and composite gas flows |
| WO2024044498A1 (en) | 2022-08-25 | 2024-02-29 | 6K Inc. | Plasma apparatus and methods for processing feed material utilizing a powder ingress preventor (pip) |
| US12195338B2 (en) | 2022-12-15 | 2025-01-14 | 6K Inc. | Systems, methods, and device for pyrolysis of methane in a microwave plasma for hydrogen and structured carbon powder production |
| EP4725624A1 (en) | 2024-10-14 | 2026-04-15 | Amazemet Spolka Z Ograniczona Odpowiedzialnoscia | Method of atomization of powdered feedstock and device for atomization of powdered feedstock |
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| CN101716686B (zh) * | 2010-01-05 | 2011-02-16 | 北京科技大学 | 一种微细球形钛粉的短流程制备方法 |
-
2012
- 2012-04-13 CA CA2834328A patent/CA2834328A1/en not_active Abandoned
- 2012-04-13 AU AU2012250152A patent/AU2012250152B2/en not_active Ceased
- 2012-04-13 KR KR1020137031306A patent/KR20140027335A/ko not_active Withdrawn
- 2012-04-13 WO PCT/US2012/033652 patent/WO2012148714A1/en not_active Ceased
- 2012-04-13 JP JP2014508399A patent/JP2014515792A/ja active Pending
- 2012-04-13 CN CN201280020807.0A patent/CN103608141A/zh active Pending
- 2012-04-13 PL PL12777501T patent/PL2701869T3/pl unknown
- 2012-04-13 US US13/447,022 patent/US8911529B2/en not_active Expired - Fee Related
- 2012-04-13 EP EP12777501.3A patent/EP2701869B1/en not_active Not-in-force
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