JP2014513053A - フッ化ジオールの製造方法 - Google Patents

フッ化ジオールの製造方法 Download PDF

Info

Publication number
JP2014513053A
JP2014513053A JP2013554595A JP2013554595A JP2014513053A JP 2014513053 A JP2014513053 A JP 2014513053A JP 2013554595 A JP2013554595 A JP 2013554595A JP 2013554595 A JP2013554595 A JP 2013554595A JP 2014513053 A JP2014513053 A JP 2014513053A
Authority
JP
Japan
Prior art keywords
diol compound
producing
fluorinated diol
compound according
fluorinated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2013554595A
Other languages
English (en)
Japanese (ja)
Other versions
JP2014513053A5 (enExample
Inventor
マゼル・ポール・ジュニア
パブリ・ネヴィル
スウィンソン・ジョエル
Original Assignee
ヘイロウカーボン プロダクツ コーポレイション
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ヘイロウカーボン プロダクツ コーポレイション filed Critical ヘイロウカーボン プロダクツ コーポレイション
Publication of JP2014513053A publication Critical patent/JP2014513053A/ja
Publication of JP2014513053A5 publication Critical patent/JP2014513053A5/ja
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/143—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones
    • C07C29/145—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/143—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/44—Palladium
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
    • C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/34—Halogenated alcohols
    • C07C31/38—Halogenated alcohols containing only fluorine as halogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/72—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2013554595A 2011-02-16 2012-02-16 フッ化ジオールの製造方法 Pending JP2014513053A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161443297P 2011-02-16 2011-02-16
US61/443,297 2011-02-16
PCT/US2012/025396 WO2012112751A1 (en) 2011-02-16 2012-02-16 Process for preparing fluorinated diols

Publications (2)

Publication Number Publication Date
JP2014513053A true JP2014513053A (ja) 2014-05-29
JP2014513053A5 JP2014513053A5 (enExample) 2016-04-14

Family

ID=46672940

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2013554595A Pending JP2014513053A (ja) 2011-02-16 2012-02-16 フッ化ジオールの製造方法

Country Status (8)

Country Link
US (1) US8729316B2 (enExample)
EP (1) EP2678303A4 (enExample)
JP (1) JP2014513053A (enExample)
KR (1) KR20130143113A (enExample)
CN (1) CN103429560B (enExample)
BR (1) BR112013021431A2 (enExample)
CA (1) CA2827453C (enExample)
WO (1) WO2012112751A1 (enExample)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6488769B2 (ja) 2014-03-18 2019-03-27 セントラル硝子株式会社 含フッ素ヒドロキシアルデヒド、含フッ素プロパンジオールおよび含フッ素アルコール単量体の製造方法
CN103980405B (zh) * 2014-05-17 2016-01-20 北京化工大学 端羟基液体氟聚合物的制备及固化方法
CN113045381B (zh) * 2019-12-26 2023-06-02 中蓝晨光化工研究设计院有限公司 一种含氟二元醇的制备方法

Citations (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3365504A (en) * 1965-10-22 1968-01-23 Air Reduction Vapor phase production of propargyl alcohol under anhydrous conditions
US3394204A (en) * 1965-10-23 1968-07-23 Blaga Aurel 2-methyl-3, 3, 3, trichloro-1, 2-propanediol and unsaturated polyesters prepared therefrom
US3440285A (en) * 1966-04-01 1969-04-22 Allied Chem Aldehydes and alcohols prepared therefrom
US3468964A (en) * 1965-08-03 1969-09-23 Du Pont Hydrogenation process
US3662071A (en) * 1966-05-17 1972-05-09 Du Pont Pharmaceutical composition comprising certain 1,3-substituted glycols
US3702872A (en) * 1970-07-27 1972-11-14 Baxter Laboratories Inc Production of hexafluoropropanol
JPS4821925B1 (enExample) * 1968-12-27 1973-07-02
JPS5781424A (en) * 1980-11-11 1982-05-21 Central Glass Co Ltd Preparation of 1,1,1,3,3,3-hexafluoropropane-2-ol
US4336408A (en) * 1977-11-25 1982-06-22 Thiokol Corporation 2-Hydroxymethyl-1,3-propanediol preparation
US5166370A (en) * 1991-04-12 1992-11-24 Arco Chemical Technology, L.P. Preparation of tetrahydrofuran using a supported transition metal
JP2003510246A (ja) * 1998-09-04 2003-03-18 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ３−ヒドロキシプロパナールの接触水素化による１，３−プロパンジオールの二段階製造法
CN1475472A (zh) * 2003-06-30 2004-02-18 华东理工大学 1，3－丙二醇的制备方法
JP2004182622A (ja) * 2002-12-02 2004-07-02 Asahi Kasei Chemicals Corp １，３−プロパンジオールの製造方法
JP2005206587A (ja) * 2003-12-26 2005-08-04 Central Glass Co Ltd １，１−ビス（トリフルオロメチル）−１，３−ジオール類アクリル酸系エステルの製造方法
JP2005239710A (ja) * 2004-01-27 2005-09-08 Central Glass Co Ltd 含フッ素２，４−ジオール類およびその誘導体の製造方法
JP2007520561A (ja) * 2004-02-04 2007-07-26 ヘイロウカーボン プロダクツ コーポレイション １，１，１，３，３，３−ヘキサフルオロイソプロパノールの精製
WO2008151102A2 (en) * 2007-06-04 2008-12-11 Shell Oil Company Hydrogenation process

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7297811B2 (en) 2003-12-04 2007-11-20 International Business Machines Corporation Precursors to fluoroalkanol-containing olefin monomers and associated methods of synthesis and use
US7495135B2 (en) 2003-12-04 2009-02-24 International Business Machines Corporation Precursors to fluoroalkanol-containing olefin monomers, and associated methods of synthesis and use
US7067691B2 (en) 2003-12-26 2006-06-27 Central Glass Co., Ltd. Process for producing α-substituted acrylic acid esters
US7205443B2 (en) 2004-01-27 2007-04-17 Central Glass Company, Limited Processes for producing fluorine-containing 2,4-diols and their derivatives

Patent Citations (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3468964A (en) * 1965-08-03 1969-09-23 Du Pont Hydrogenation process
US3365504A (en) * 1965-10-22 1968-01-23 Air Reduction Vapor phase production of propargyl alcohol under anhydrous conditions
US3394204A (en) * 1965-10-23 1968-07-23 Blaga Aurel 2-methyl-3, 3, 3, trichloro-1, 2-propanediol and unsaturated polyesters prepared therefrom
US3440285A (en) * 1966-04-01 1969-04-22 Allied Chem Aldehydes and alcohols prepared therefrom
US3662071A (en) * 1966-05-17 1972-05-09 Du Pont Pharmaceutical composition comprising certain 1,3-substituted glycols
JPS4821925B1 (enExample) * 1968-12-27 1973-07-02
US3702872A (en) * 1970-07-27 1972-11-14 Baxter Laboratories Inc Production of hexafluoropropanol
US4336408A (en) * 1977-11-25 1982-06-22 Thiokol Corporation 2-Hydroxymethyl-1,3-propanediol preparation
JPS5781424A (en) * 1980-11-11 1982-05-21 Central Glass Co Ltd Preparation of 1,1,1,3,3,3-hexafluoropropane-2-ol
US5166370A (en) * 1991-04-12 1992-11-24 Arco Chemical Technology, L.P. Preparation of tetrahydrofuran using a supported transition metal
JP2003510246A (ja) * 1998-09-04 2003-03-18 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ３−ヒドロキシプロパナールの接触水素化による１，３−プロパンジオールの二段階製造法
JP2004182622A (ja) * 2002-12-02 2004-07-02 Asahi Kasei Chemicals Corp １，３−プロパンジオールの製造方法
CN1475472A (zh) * 2003-06-30 2004-02-18 华东理工大学 1，3－丙二醇的制备方法
JP2005206587A (ja) * 2003-12-26 2005-08-04 Central Glass Co Ltd １，１−ビス（トリフルオロメチル）−１，３−ジオール類アクリル酸系エステルの製造方法
JP2005239710A (ja) * 2004-01-27 2005-09-08 Central Glass Co Ltd 含フッ素２，４−ジオール類およびその誘導体の製造方法
JP2007520561A (ja) * 2004-02-04 2007-07-26 ヘイロウカーボン プロダクツ コーポレイション １，１，１，３，３，３−ヘキサフルオロイソプロパノールの精製
WO2008151102A2 (en) * 2007-06-04 2008-12-11 Shell Oil Company Hydrogenation process

Also Published As

Publication number Publication date
WO2012112751A1 (en) 2012-08-23
CA2827453C (en) 2015-07-07
CN103429560A (zh) 2013-12-04
KR20130143113A (ko) 2013-12-30
US20130338404A1 (en) 2013-12-19
CN103429560B (zh) 2015-09-09
CA2827453A1 (en) 2012-08-23
EP2678303A1 (en) 2014-01-01
EP2678303A4 (en) 2014-07-23
BR112013021431A2 (pt) 2016-10-25
US8729316B2 (en) 2014-05-20

Similar Documents

Publication Publication Date Title
JP5149796B2 (ja) プロセス
CA2654117C (en) Processes for converting glycerol to amino alcohols
US10000460B2 (en) Chelate-controlled diastereoselective hydrogenation with heterogeneous catalyst
JP2014513053A (ja) フッ化ジオールの製造方法
JPWO2019240009A1 (ja) １，３−ブチレングリコールの製造方法
TW201200494A (en) Process for preparing neopentyl glycol
CN102256918B (zh) 生产二醇型化合物的催化方法
CN105308010B (zh) 制备烯丙醇的方法以及由该方法制备的烯丙醇
JP2014513053A5 (enExample)
JP4979230B2 (ja) テトラヒドロピラン化合物の製造方法及び該製造方法で製造されるテトラヒドロピラン化合物
Seifert et al. Acid-catalyzed aldol-Meerwein–Ponndorf–Verley-etherification reactions—access to defined configured quaternary stereogenic centers
JP7177156B2 (ja) ２，３－ブタンジオールの連続製造方法
CN112074500B (zh) α,β-二羟基羰基化合物脱水并裂解为乳酸和其他产物
JP4552031B2 (ja) シトラール水素化物の製造方法
CN110520403B (zh) α,α-二氟乙醛半缩醛的制造方法
JP5478097B2 (ja) ２−アルキル−２−シクロアルケン−１−オンの製造方法
RU2529033C1 (ru) СПОСОБ ГИДРИРОВАНИЯ α, β-НЕНАСЫЩЕННЫХ КЕТОНОВ
WO2002034703A2 (en) Method of making fluorinated alcohols
JP7175915B2 (ja) 環状エーテルの製造方法
CN113646289A (zh) 卤代环烷烃化合物的制造方法
RU2283301C2 (ru) Способ получения фторированного бензонитрила
JP5742716B2 (ja) シクロヘキシルアルキルケトン類の製造方法
CN113045394A (zh) 一种合成α-碘代-β酮基缩醛类化合物的方法
JP4296275B2 (ja) 超臨界二酸化炭素中での水素化反応によるシトラールからの不飽和アルコールの合成方法
JP2023143030A (ja) １，３－シクロペンタンジオールの製造方法

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20150114

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20150827

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20150901

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20151127

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20151224

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20160128

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20160224

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20160722