JP2012528825A5 - - Google Patents
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- Publication number
- JP2012528825A5 JP2012528825A5 JP2012513596A JP2012513596A JP2012528825A5 JP 2012528825 A5 JP2012528825 A5 JP 2012528825A5 JP 2012513596 A JP2012513596 A JP 2012513596A JP 2012513596 A JP2012513596 A JP 2012513596A JP 2012528825 A5 JP2012528825 A5 JP 2012528825A5
- Authority
- JP
- Japan
- Prior art keywords
- group
- alcohol
- ion
- alkoxyaryl
- substituted
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 claims 12
- -1 biaryl alcohol Chemical compound 0.000 claims 7
- 238000005868 electrolysis reaction Methods 0.000 claims 3
- 239000003115 supporting electrolyte Substances 0.000 claims 3
- PETRWTHZSKVLRE-UHFFFAOYSA-N 2-Methoxy-4-methylphenol Chemical compound COC1=CC(C)=CC=C1O PETRWTHZSKVLRE-UHFFFAOYSA-N 0.000 claims 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 2
- DTQVDTLACAAQTR-UHFFFAOYSA-N Trifluoroacetic acid Chemical compound OC(=O)C(F)(F)F DTQVDTLACAAQTR-UHFFFAOYSA-N 0.000 claims 2
- 125000003158 alcohol group Chemical group 0.000 claims 2
- 238000006471 dimerization reaction Methods 0.000 claims 2
- 150000002500 ions Chemical class 0.000 claims 2
- 229940085991 phosphate ion Drugs 0.000 claims 2
- 125000000027 (C1-C10) alkoxy group Chemical group 0.000 claims 1
- BYEAHWXPCBROCE-UHFFFAOYSA-N 1,1,1,3,3,3-hexafluoropropan-2-ol Chemical compound FC(F)(F)C(O)C(F)(F)F BYEAHWXPCBROCE-UHFFFAOYSA-N 0.000 claims 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000001298 alcohols Chemical class 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 1
- 125000003545 alkoxy group Chemical group 0.000 claims 1
- 125000005910 alkyl carbonate group Chemical group 0.000 claims 1
- 150000008051 alkyl sulfates Chemical class 0.000 claims 1
- 125000002947 alkylene group Chemical group 0.000 claims 1
- 150000003863 ammonium salts Chemical class 0.000 claims 1
- 150000001491 aromatic compounds Chemical group 0.000 claims 1
- 125000000732 arylene group Chemical group 0.000 claims 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 1
- 229910052796 boron Inorganic materials 0.000 claims 1
- 125000003917 carbamoyl group Chemical group [H]N([H])C(*)=O 0.000 claims 1
- 239000003575 carbonaceous material Substances 0.000 claims 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims 1
- 238000006356 dehydrogenation reaction Methods 0.000 claims 1
- 229910003460 diamond Inorganic materials 0.000 claims 1
- 239000010432 diamond Substances 0.000 claims 1
- 229910002804 graphite Inorganic materials 0.000 claims 1
- 239000010439 graphite Substances 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-M hydrogensulfate Chemical compound OS([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-M 0.000 claims 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 125000002560 nitrile group Chemical group 0.000 claims 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- VLTRZXGMWDSKGL-UHFFFAOYSA-M perchlorate Chemical compound [O-]Cl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-M 0.000 claims 1
- CTYRPMDGLDAWRQ-UHFFFAOYSA-N phenyl hydrogen sulfate Chemical compound OS(=O)(=O)OC1=CC=CC=C1 CTYRPMDGLDAWRQ-UHFFFAOYSA-N 0.000 claims 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 125000001424 substituent group Chemical group 0.000 claims 1
- 229910052717 sulfur Inorganic materials 0.000 claims 1
- 239000011593 sulfur Substances 0.000 claims 1
- 0 *c(c(*)c1*)c(*)c(O)c1O Chemical compound *c(c(*)c1*)c(*)c(O)c1O 0.000 description 2
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09162076.5 | 2009-06-05 | ||
| EP09162076 | 2009-06-05 | ||
| PCT/EP2010/057619 WO2010139687A1 (de) | 2009-06-05 | 2010-06-01 | Verfahren zur herstellung von unsymmetrischen biarylalkoholen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2012528825A JP2012528825A (ja) | 2012-11-15 |
| JP2012528825A5 true JP2012528825A5 (enExample) | 2013-07-18 |
Family
ID=42358670
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012513596A Pending JP2012528825A (ja) | 2009-06-05 | 2010-06-01 | 非対称性ビアリールアルコールを製造する方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US8747645B2 (enExample) |
| EP (1) | EP2438215A1 (enExample) |
| JP (1) | JP2012528825A (enExample) |
| CN (1) | CN102459707A (enExample) |
| WO (1) | WO2010139687A1 (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102459706B (zh) * | 2009-06-05 | 2015-02-11 | 巴斯夫欧洲公司 | 芳烃的阳极交叉脱氢二聚方法 |
| DE102013203865A1 (de) * | 2013-03-07 | 2014-09-11 | Evonik Industries Ag | Elektrochemische Kupplung zweier Phenole, welche sich in ihrem Oxidationspotential unterscheiden |
| DE102013211744A1 (de) | 2013-06-21 | 2014-12-24 | Evonik Industries Ag | Elektrochemisches Verfahren zur Herstellung von symmetrischen Biphenolen unter Verwendung einer Glaskohlenstoffanode |
| DE102013211745A1 (de) | 2013-06-21 | 2014-12-24 | Evonik Industries Ag | Elektrochemisches Verfahren zur Herstellung von symmetrischen Biphenolen unter Verwendung von Essigsäure als Elektrolyt |
| DE102014209976A1 (de) | 2014-05-26 | 2015-11-26 | Evonik Degussa Gmbh | Verfahren zur Herstellung von 2,2'-Biphenolen unter Verwendung von Selendioxid und halogeniertem Lösungsmittel |
| DE102014209967A1 (de) | 2014-05-26 | 2015-12-17 | Evonik Degussa Gmbh | Verfahren zur Herstellung von 2,2'-Biphenolen unter Verwendung von Selendioxid |
| US9950979B2 (en) | 2014-05-26 | 2018-04-24 | Evonik Degussa Gmbh | Method for producing asymmetrical biphenols using selenium dioxide |
| SG10201601501QA (en) | 2015-03-05 | 2016-10-28 | Evonik Degussa Gmbh | Preparation of 2,2`-biaryls in the presence of molybdenum(v) chloride |
| EP3095776A1 (de) | 2015-05-20 | 2016-11-23 | Evonik Degussa GmbH | Kupplung von einem Phenol und einem Aren unter Verwendung von Selendioxid |
| DE102015216000A1 (de) * | 2015-08-21 | 2017-02-23 | Evonik Degussa Gmbh | Verfahren zur Herstellung von symmetrischen Pincerliganden aus der Gruppe der m-Terphenylverbindungen |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3992435A (en) * | 1975-04-07 | 1976-11-16 | Standard Oil Company (Indiana) | Process for electrolytic synthesis of polyalkylbiphenylpolycarboxylic acid compounds |
| US4101391A (en) * | 1976-01-05 | 1978-07-18 | Monsanto Company | Electrolytic oxidative methyl-methyl coupling of cresol salts |
| JPH0243388A (ja) * | 1988-08-03 | 1990-02-13 | Mitsubishi Kasei Corp | ４，４’−ジヒドロキシビフェニル類の製造法 |
| EP0663378B1 (de) * | 1993-12-11 | 1999-03-31 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von 2,2'-Dimethyl-1,1'-binaphtyl und 2,7'-Dimethyl-1,1'-binaphtyl |
| DE4411024A1 (de) * | 1994-03-30 | 1995-12-21 | Hoechst Ag | Verfahren zur Herstellung von 4,4'-Dimethyl-1,1'-binaphthyl |
| JPH08245459A (ja) * | 1995-03-16 | 1996-09-24 | Dainippon Ink & Chem Inc | フェノール性水酸基含有縮合多環式化合物の二量化物の製法 |
| DE19641344A1 (de) | 1995-10-17 | 1997-04-24 | Basf Ag | Verfahren zur Herstellung von Biarylen |
| JPH09176074A (ja) * | 1995-12-28 | 1997-07-08 | Kibun Foods Inc | 抗菌・抗カビ・抗炎症活性物質とその製造方法 |
| FR2803856B1 (fr) * | 2000-01-13 | 2002-07-05 | Atofina | Synthese de l'hydroxyde de tetramethylammonium |
| DE102004005508A1 (de) | 2004-02-04 | 2005-08-25 | Basf Ag | Anodische Dimerisierung substituierter Benzole |
| DE102005003012A1 (de) * | 2005-01-21 | 2006-07-27 | Basf Ag | Anodische Dimerisierung von Hydroxy-substituierten Aromaten |
| CN100436649C (zh) * | 2005-01-28 | 2008-11-26 | 华东师范大学 | 联苯的电化学合成方法 |
| WO2007131969A2 (en) * | 2006-05-15 | 2007-11-22 | Akzo Nobel N.V. | An electrochemical process to prepare a halogenated carbonyl group-containing compound |
| WO2010023258A1 (de) | 2008-09-01 | 2010-03-04 | Basf Se | Verfahren zur anodischen dehydrodimerisierung von substituierten arylalkoholen |
| CN102459706B (zh) * | 2009-06-05 | 2015-02-11 | 巴斯夫欧洲公司 | 芳烃的阳极交叉脱氢二聚方法 |
-
2010
- 2010-06-01 WO PCT/EP2010/057619 patent/WO2010139687A1/de not_active Ceased
- 2010-06-01 EP EP10724438A patent/EP2438215A1/de not_active Withdrawn
- 2010-06-01 CN CN2010800245846A patent/CN102459707A/zh active Pending
- 2010-06-01 JP JP2012513596A patent/JP2012528825A/ja active Pending
- 2010-06-01 US US13/375,100 patent/US8747645B2/en not_active Expired - Fee Related
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