JP2012507603A - 1,1,2,3−テトラクロロプロペン及びフッ化水素の共沸混合物様組成物 - Google Patents
1,1,2,3−テトラクロロプロペン及びフッ化水素の共沸混合物様組成物 Download PDFInfo
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- JP2012507603A JP2012507603A JP2011534732A JP2011534732A JP2012507603A JP 2012507603 A JP2012507603 A JP 2012507603A JP 2011534732 A JP2011534732 A JP 2011534732A JP 2011534732 A JP2011534732 A JP 2011534732A JP 2012507603 A JP2012507603 A JP 2012507603A
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- 239000000203 mixture Substances 0.000 title claims abstract description 83
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 title claims abstract description 40
- 229910000040 hydrogen fluoride Inorganic materials 0.000 title claims abstract description 38
- UMGQVBVEWTXECF-UHFFFAOYSA-N 1,1,2,3-tetrachloroprop-1-ene Chemical group ClCC(Cl)=C(Cl)Cl UMGQVBVEWTXECF-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 238000000034 method Methods 0.000 claims abstract description 12
- 238000009835 boiling Methods 0.000 claims description 13
- 239000007789 gas Substances 0.000 claims description 5
- 150000002894 organic compounds Chemical class 0.000 claims description 4
- 239000003380 propellant Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 239000012025 fluorinating agent Substances 0.000 claims description 2
- 239000012459 cleaning agent Substances 0.000 claims 1
- 239000006184 cosolvent Substances 0.000 claims 1
- 239000003701 inert diluent Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 description 13
- FXRLMCRCYDHQFW-UHFFFAOYSA-N 2,3,3,3-tetrafluoropropene Chemical compound FC(=C)C(F)(F)F FXRLMCRCYDHQFW-UHFFFAOYSA-N 0.000 description 5
- 239000012071 phase Substances 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 4
- 150000001875 compounds Chemical group 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000000758 substrate Substances 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- 239000000443 aerosol Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 238000003682 fluorination reaction Methods 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 238000010301 surface-oxidation reaction Methods 0.000 description 2
- PGJHURKAWUJHLJ-UHFFFAOYSA-N 1,1,2,3-tetrafluoroprop-1-ene Chemical compound FCC(F)=C(F)F PGJHURKAWUJHLJ-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000008241 heterogeneous mixture Substances 0.000 description 1
- 229940060367 inert ingredients Drugs 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
- B01J23/8926—Copper and noble metals
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
- C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/04—Chloro-alkenes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/30—Materials not provided for elsewhere for aerosols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/50—Solvents
- C11D7/5036—Azeotropic mixtures containing halogenated solvents
- C11D7/504—Azeotropic mixtures containing halogenated solvents all solvents being halogenated hydrocarbons
- C11D7/5059—Mixtures containing (hydro)chlorocarbons
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
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Abstract
【選択図】図1
Description
本発明は共沸混合物様組成物に関する。より詳しくは、本発明はヒドロフルオロオレフィン及びフッ化水素を含む共沸混合物様組成物に関する。
本発明の他の形態においては、フッ化水素を1,1,2,3−テトラクロロプロペンと約0℃〜約60℃の温度及び約7psia〜約58psiaの圧力においてブレンドして、約1〜約95重量%のフッ化水素及び約5〜約99重量%の1,1,2,3−テトラクロロプロペンから実質的に構成される共沸混合物様混合物を製造することを含む、共沸性又は共沸混合物様組成物を形成する方法が提供される。
本発明の他の形態においては、1,1,2,3−テトラクロロプロペン及びフッ化水素から実質的に構成される共沸混合物様組成物を含む噴霧可能な組成物が提供される。
共沸混合物様組成物の成分に関してここで用いる「実質的に構成される」という用語は、組成物が、示されている成分を共沸混合物様の比で含み、更なる成分が新しい共沸混合物様の系を形成しないならば更なる成分を含んでいてもよいことを意味する。例えば、2種類の化合物から実質的に構成される共沸混合物様混合物は、二元共沸混合物を形成し、更なる成分が混合物を非共沸性にせず、化合物のいずれか又は両方と共沸混合物を形成しない(例えば3元共沸混合物を形成しない)ならば1以上の更なる成分を含んでいてもよいものである。
ここで用いる「分配形態」という用語は、それを一定の領域の上又は一定の体積に展開、分散、及び/又は拡散させた際の流体の物理的形態を指す。分配形態の例としては、エアロゾル及びスプレーが挙げられる。
実施例1:
約9gの1,1,2,3−テトラクロロプロペン(TCP)を、約25℃及び約14.6psiaにおいて91gのHF中にブレンドした。不均一な共沸混合物様組成物の形成が観察された。
TCP及びHFをブレンドして、異なる組成の不均一共沸混合物を形成した。混合物の蒸気圧を、約0、25、及び60℃において測定した。これらの測定の結果を表1に与える。
実施例3:
本実施例は、気−液−液平衡(VLLE)によるTCP/HF混合物の共沸混合物様の特性を示す。
Claims (10)
- 1,1,2,3−テトラクロロプロペン及びフッ化水素から実質的に構成される共沸混合物様混合物を含む組成物。
- 該共沸混合物様混合物が約1〜約95重量%のフッ化水素及び約5〜約99重量%の1,1,2,3−テトラクロロプロペンから実質的に構成される、請求項28に記載の組成物。
- 該共沸混合物様混合物が約5〜約95重量%のフッ化水素及び約5〜約95重量%の1,1,2,3−テトラクロロプロペンから実質的に構成される、請求項28に記載の組成物。
- 該共沸混合物様混合物が約55〜約95重量%のフッ化水素及び約5〜約45重量%の1,1,2,3−テトラクロロプロペンから実質的に構成される、請求項28に記載の組成物。
- 該共沸混合物様混合物から実質的に構成される、請求項1に記載の組成物。
- 不活性希釈剤、洗浄剤、噴射剤、共噴射剤、及び共溶媒から選択される少なくとも1種類の成分を更に含む、請求項1に記載の組成物。
- 少なくとも約50重量%の該共沸混合物様混合物を有する、請求項8に記載の組成物。
- 請求項1〜7に記載の組成物を含む噴霧可能な組成物。
- a.1,1,2,3−テトラクロロプロペン及びフッ化水素から実質的に構成される共沸混合物様組成物を準備し;
b.1,1,2,3−テトラクロロプロペンの少なくとも一部を気相中においてフッ素化剤と反応させて少なくとも1種類のフッ素化有機化合物を製造する;
ことを含む、有機化合物をフッ素化する方法。 - 有効量の1,1,2,3−テトラクロロプロペン及びフッ化水素をブレンドして、1,1,2,3−テトラクロロプロペン及びフッ化水素から実質的に構成される共沸混合物様混合物を形成することを含む、ヒドロクロロプロパンの沸点を低下させる方法。
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11022708P | 2008-10-31 | 2008-10-31 | |
US61/110,227 | 2008-10-31 | ||
US12/607,802 US8008243B2 (en) | 2008-10-31 | 2009-10-28 | Azeotrope-like compositions of 1,1,2,3-tetrachloropropene and hydrogen fluoride |
US12/607,802 | 2009-10-28 | ||
PCT/US2009/062454 WO2010051327A2 (en) | 2008-10-31 | 2009-10-29 | Azeotrope-like compositions of 1,1,2,3-tetrachloropropene and hydrogen fluoride |
Related Child Applications (1)
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JP2015167779A Division JP6214603B2 (ja) | 2008-10-31 | 2015-08-27 | 1,1,2,3−テトラクロロプロペン及びフッ化水素の共沸混合物様組成物 |
Publications (2)
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JP2012507603A true JP2012507603A (ja) | 2012-03-29 |
JP5846914B2 JP5846914B2 (ja) | 2016-01-20 |
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JP2011534732A Active JP5846914B2 (ja) | 2008-10-31 | 2009-10-29 | 1,1,2,3−テトラクロロプロペン及びフッ化水素の共沸混合物様組成物 |
JP2015167779A Active JP6214603B2 (ja) | 2008-10-31 | 2015-08-27 | 1,1,2,3−テトラクロロプロペン及びフッ化水素の共沸混合物様組成物 |
JP2017176448A Pending JP2018035358A (ja) | 2008-10-31 | 2017-09-14 | 1,1,2,3−テトラクロロプロペン及びフッ化水素の共沸混合物様組成物 |
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JP2015167779A Active JP6214603B2 (ja) | 2008-10-31 | 2015-08-27 | 1,1,2,3−テトラクロロプロペン及びフッ化水素の共沸混合物様組成物 |
JP2017176448A Pending JP2018035358A (ja) | 2008-10-31 | 2017-09-14 | 1,1,2,3−テトラクロロプロペン及びフッ化水素の共沸混合物様組成物 |
Country Status (8)
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US (2) | US8008243B2 (ja) |
EP (1) | EP2344434B2 (ja) |
JP (3) | JP5846914B2 (ja) |
KR (2) | KR101862844B1 (ja) |
CN (1) | CN102203037B (ja) |
ES (1) | ES2548247T5 (ja) |
MX (1) | MX2011004346A (ja) |
WO (1) | WO2010051327A2 (ja) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2016026249A (ja) * | 2008-10-31 | 2016-02-12 | ハネウェル・インターナショナル・インコーポレーテッド | 1,1,2,3−テトラクロロプロペン及びフッ化水素の共沸混合物様組成物 |
Families Citing this family (8)
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US8741828B2 (en) * | 2011-02-23 | 2014-06-03 | Honeywell International Inc. | Azeotrope and azeotrope-like compositions useful for the production of haloolefins |
US9222177B2 (en) | 2013-03-13 | 2015-12-29 | Honeywell International Inc. | Azeotropic compositions of 1,3,3,3-tetrachloroprop-1-ene and hydrogen fluoride |
US9334210B2 (en) | 2013-03-13 | 2016-05-10 | Honeywell International Inc. | Azeotropic compositions of 1,1,3,3-tetrachloroprop-1-ene and hydrogen fluoride |
US9334206B2 (en) * | 2013-03-15 | 2016-05-10 | Honeywell International Inc. | Integrated process to produce 2,3,3,3-tetrafluoropropene |
US10029964B2 (en) | 2016-08-30 | 2018-07-24 | Honeywell International Inc. | Azeotropic or azeotrope-like compositions of 3,3,3-trifluoropropyne and water |
US9950973B2 (en) * | 2016-08-31 | 2018-04-24 | Honeywell International Inc. | Azeotropic or azeotrope-like compositions of 1,3-dichloro-3,3-difluoroprop-1-ene (HCFO-1232zd) and hydrogen fluoride (HF) |
US9950974B2 (en) * | 2016-08-31 | 2018-04-24 | Honeywell International Inc. | Azeotropic or azeotrope-like compositions of 1,3,3-trichloro-3-fluoro-1-ene (HCFO-1231zd) and hydrogen fluoride (HF) |
GB2546845A (en) * | 2016-09-05 | 2017-08-02 | Mexichem Fluor Sa De Cv | Composition |
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JP2018035358A (ja) | 2018-03-08 |
US8247366B2 (en) | 2012-08-21 |
KR20170080708A (ko) | 2017-07-10 |
ES2548247T3 (es) | 2015-10-15 |
US8008243B2 (en) | 2011-08-30 |
MX2011004346A (es) | 2011-05-25 |
KR101862844B1 (ko) | 2018-05-30 |
JP2016026249A (ja) | 2016-02-12 |
JP5846914B2 (ja) | 2016-01-20 |
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WO2010051327A3 (en) | 2010-08-12 |
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US20110287996A1 (en) | 2011-11-24 |
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EP2344434A4 (en) | 2013-11-13 |
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EP2344434A2 (en) | 2011-07-20 |
EP2344434B1 (en) | 2015-07-22 |
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CN102203037B (zh) | 2014-08-13 |
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