JP2011522811A5 - - Google Patents
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- JP2011522811A5 JP2011522811A5 JP2011512043A JP2011512043A JP2011522811A5 JP 2011522811 A5 JP2011522811 A5 JP 2011522811A5 JP 2011512043 A JP2011512043 A JP 2011512043A JP 2011512043 A JP2011512043 A JP 2011512043A JP 2011522811 A5 JP2011522811 A5 JP 2011522811A5
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- JP
- Japan
- Prior art keywords
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- groups
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 125000000217 alkyl group Chemical group 0.000 claims description 23
- 125000004432 carbon atom Chemical group C* 0.000 claims description 18
- 229910052739 hydrogen Inorganic materials 0.000 claims description 15
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 14
- 239000012074 organic phase Substances 0.000 claims description 14
- 150000001412 amines Chemical class 0.000 claims description 12
- 239000001257 hydrogen Substances 0.000 claims description 12
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 12
- -1 ammonium halide Chemical class 0.000 claims description 11
- 125000003118 aryl group Chemical group 0.000 claims description 11
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- 229910021529 ammonia Inorganic materials 0.000 claims description 7
- 239000003518 caustics Substances 0.000 claims description 7
- 239000007791 liquid phase Substances 0.000 claims description 6
- 239000003495 polar organic solvent Substances 0.000 claims description 6
- 239000000047 product Substances 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 150000001282 organosilanes Chemical class 0.000 claims description 5
- 239000008346 aqueous phase Substances 0.000 claims description 4
- 229910052794 bromium Inorganic materials 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 229910052801 chlorine Inorganic materials 0.000 claims description 4
- 239000012043 crude product Substances 0.000 claims description 4
- 229910052740 iodine Inorganic materials 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 3
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 239000012454 non-polar solvent Substances 0.000 claims description 2
- 238000005191 phase separation Methods 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 239000000243 solution Substances 0.000 claims 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- 239000003960 organic solvent Substances 0.000 claims 2
- 239000012670 alkaline solution Substances 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 238000004821 distillation Methods 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 239000012071 phase Substances 0.000 claims 1
- 235000011118 potassium hydroxide Nutrition 0.000 claims 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims 1
- FZHAPNGMFPVSLP-UHFFFAOYSA-N silanamine Chemical compound [SiH3]N FZHAPNGMFPVSLP-UHFFFAOYSA-N 0.000 claims 1
- 235000011121 sodium hydroxide Nutrition 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 238000003786 synthesis reaction Methods 0.000 claims 1
- 238000010626 work up procedure Methods 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 6
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 4
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 4
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 229910052736 halogen Inorganic materials 0.000 description 2
- 150000003254 radicals Chemical class 0.000 description 2
- 150000005840 aryl radicals Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102008002181A DE102008002181A1 (de) | 2008-06-03 | 2008-06-03 | Verfahren zur wässrigen Aufarbeitung eines Ammoniumhalogenide und/oder organische Aminhydrohalogenide enthaltenden aminofunktionellen Organosilans |
| DE102008002181.4 | 2008-06-03 | ||
| PCT/EP2009/054282 WO2009146969A1 (de) | 2008-06-03 | 2009-04-09 | Verfahren zur wässrigen aufarbeitung eines ammoniumhalogenide und/oder organische aminhydrohalogenide enthaltenden aminofunktionellen organosilans |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011522811A JP2011522811A (ja) | 2011-08-04 |
| JP2011522811A5 true JP2011522811A5 (https=) | 2012-03-29 |
| JP5627572B2 JP5627572B2 (ja) | 2014-11-19 |
Family
ID=40791459
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011512043A Expired - Fee Related JP5627572B2 (ja) | 2008-06-03 | 2009-04-09 | ハロゲン化アンモニウムおよび／または有機アミンハロゲン化水素酸塩を含有するアミノ官能性オルガノシランの水系後処理法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20110046405A1 (https=) |
| EP (1) | EP2291385B1 (https=) |
| JP (1) | JP5627572B2 (https=) |
| KR (1) | KR101588913B1 (https=) |
| CN (1) | CN101597300B (https=) |
| DE (1) | DE102008002181A1 (https=) |
| ES (1) | ES2524313T3 (https=) |
| WO (1) | WO2009146969A1 (https=) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102008002182A1 (de) * | 2008-06-03 | 2009-12-10 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Alkylaminoalkylalkoxysilanen |
| DE102008002183A1 (de) * | 2008-06-03 | 2009-12-10 | Evonik Degussa Gmbh | Verfahren zur Aufarbeitung salzhaltiger Rückstände aus der Herstellung von aminofunktionellen Organosilanen |
| CN103333200B (zh) * | 2013-07-22 | 2015-08-12 | 荆州市江汉精细化工有限公司 | 一种正丁基氨丙基三烷氧基硅烷的合成方法 |
| CN104926852A (zh) * | 2014-03-19 | 2015-09-23 | 张家港市国泰华荣化工新材料有限公司 | 正丁胺基丙基三甲氧基硅烷的制备方法 |
| CN104086584A (zh) * | 2014-07-29 | 2014-10-08 | 荆州市江汉精细化工有限公司 | 一种双-（烷氧基硅丙基）-胺的制备方法 |
| DE102015225883A1 (de) | 2015-12-18 | 2017-06-22 | Evonik Degussa Gmbh | Bis(alkylalkoxysilyl)amin-reiche Zusammensetzungen, ein Verfahren zur deren Herstellung und deren Verwendung |
| DE102015225879A1 (de) | 2015-12-18 | 2017-06-22 | Evonik Degussa Gmbh | Tris-(alkylalkoxysilyl)amin-reiche Zusammensetzungen, deren Herstellung und deren Verwendung |
| DE102016215260A1 (de) | 2016-08-16 | 2018-02-22 | Evonik Degussa Gmbh | Verwendung einer (Alkylalkoxysily)amin-, Bis-(alkylalkoxysilyl)amin und/oder Tris-(alkylalkoxysilyl)amin-enthaltenden Zusammensetzung |
| DE102016215256A1 (de) | 2016-08-16 | 2018-02-22 | Evonik Degussa Gmbh | Bis- und Tris(organosilyl)amine enthaltende Zusammensetzungen, deren Herstellung und deren Verwendung |
| CN112430245B (zh) * | 2020-11-24 | 2023-03-03 | 江西晨光新材料股份有限公司 | 一种硅氮杂环氨基硅烷的合成系统及合成方法 |
Family Cites Families (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE544555A (https=) | 1955-01-21 | |||
| JPS5112608B2 (https=) * | 1973-05-29 | 1976-04-21 | ||
| DE2749316C2 (de) | 1977-11-04 | 1979-05-03 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur Herstellung von yAminopropylalkoxisilanen |
| DE2753124A1 (de) | 1977-11-29 | 1979-06-07 | Dynamit Nobel Ag | Verfahren zur herstellung von aminoalkylsilanen |
| US4498538A (en) | 1983-06-21 | 1985-02-12 | Union Oil Company Of California | Method for maintaining the permeability of fines-containing formations |
| US4580633A (en) | 1983-12-21 | 1986-04-08 | Union Oil Company Of California | Increasing the flow of fluids through a permeable formation |
| DE4130643A1 (de) * | 1991-09-14 | 1993-03-18 | Degussa | Verfahren zur reinigung von alkoxysilanen |
| EP0702017B1 (de) * | 1994-09-14 | 2001-11-14 | Degussa AG | Verfahren zur Herstellung von chloridarmen bzw. chloridfreien aminofunktionellen Organosilanen |
| DE19516386A1 (de) | 1995-05-04 | 1996-11-07 | Huels Chemische Werke Ag | Verfahren zur Herstellung von an chlorfunktionellen Organosilanen armen bzw. freien aminofunktionellen Organosilanen |
| US5760019A (en) * | 1996-07-12 | 1998-06-02 | The Research Foundation Of State University Of New York | Silanol enzyme inhibitors |
| DE19652642A1 (de) | 1996-12-18 | 1998-06-25 | Degussa | Kontinuierliches Verfahren zur Herstellung von gamma-Aminopropyltrialkoxysilanen |
| DE19849196A1 (de) * | 1998-10-26 | 2000-04-27 | Degussa | Verfahren zur Neutralisation und Minderung von Resthalogengehalten in Alkoxysilanen oder Alkoxysilan-basierenden Zusammensetzungen |
| EP0999214B1 (de) * | 1998-11-06 | 2004-12-08 | Degussa AG | Verfahren zur Herstellung von chloridarmen oder chloridfreien Alkoxysilanen |
| DE10058620A1 (de) | 2000-11-25 | 2002-05-29 | Degussa | Verfahren zur Herstellung von Aminoalkylsilanen |
| DE10126669A1 (de) | 2001-06-01 | 2002-12-05 | Degussa | Verfahren zur Spaltung von cyclischen Organosilanen bei der Herstellung von aminofunktionellen Organoalkoxysilanen |
| DE10140563A1 (de) | 2001-08-18 | 2003-02-27 | Degussa | Verfahren zur Herstellung von aminofunktionellen Organosilanen |
| DE10143568C2 (de) * | 2001-09-05 | 2003-07-03 | Degussa | Verfahren zur Behandlung von Aminosilanverfärbungen |
| DE10146087A1 (de) | 2001-09-19 | 2003-04-03 | Degussa | Verfahren zur Herstellung von Aminoalkylsilanen |
| US6963006B2 (en) * | 2003-01-15 | 2005-11-08 | Air Products And Chemicals, Inc. | Process for the production and purification of bis(tertiary-butylamino)silane |
| US20040177957A1 (en) | 2003-03-10 | 2004-09-16 | Kalfayan Leonard J. | Organosilicon containing compositions for enhancing hydrocarbon production and method of using the same |
| DE10353063B4 (de) * | 2003-11-13 | 2006-03-02 | Wacker-Chemie Gmbh | Verfahren zur Herstellung von (N-Organylaminoorganyl)- und (N,N-Diorganylaminoorganyl)triorganylsilanen sowie (N-Cyclohexylaminomethyl)trimethoxysilan und [N,N-Bis-(N',N'-dimethylaminopropyl)aminomethyl]triorganylsilan erhältliche mittels dieses Verfahrens |
| NO347244B1 (no) | 2004-06-17 | 2023-07-31 | Equinor Energy As | Brønnbehandling |
| EA012242B1 (ru) | 2004-06-17 | 2009-08-28 | Статойл Аса | Обработка скважин |
| DE102004060627A1 (de) * | 2004-12-16 | 2006-07-06 | Wacker Chemie Ag | Verfahren zur kontinuierlichen Herstellung von Amino-Gruppen tragenden Silicium-Verbindungen |
| DE102008002183A1 (de) * | 2008-06-03 | 2009-12-10 | Evonik Degussa Gmbh | Verfahren zur Aufarbeitung salzhaltiger Rückstände aus der Herstellung von aminofunktionellen Organosilanen |
| DE102008002182A1 (de) * | 2008-06-03 | 2009-12-10 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Alkylaminoalkylalkoxysilanen |
-
2008
- 2008-06-03 DE DE102008002181A patent/DE102008002181A1/de not_active Withdrawn
-
2009
- 2009-04-09 EP EP09757352.1A patent/EP2291385B1/de not_active Not-in-force
- 2009-04-09 ES ES09757352.1T patent/ES2524313T3/es active Active
- 2009-04-09 KR KR1020107027075A patent/KR101588913B1/ko not_active Expired - Fee Related
- 2009-04-09 WO PCT/EP2009/054282 patent/WO2009146969A1/de not_active Ceased
- 2009-04-09 JP JP2011512043A patent/JP5627572B2/ja not_active Expired - Fee Related
- 2009-04-09 US US12/988,637 patent/US20110046405A1/en not_active Abandoned
- 2009-06-02 CN CN200910141345.8A patent/CN101597300B/zh not_active Expired - Fee Related
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