JP2011225502A5 - - Google Patents
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- JP2011225502A5 JP2011225502A5 JP2010099198A JP2010099198A JP2011225502A5 JP 2011225502 A5 JP2011225502 A5 JP 2011225502A5 JP 2010099198 A JP2010099198 A JP 2010099198A JP 2010099198 A JP2010099198 A JP 2010099198A JP 2011225502 A5 JP2011225502 A5 JP 2011225502A5
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- JP
- Japan
- Prior art keywords
- mpa
- pressure
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- catalyst
- produce
- Prior art date
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- 239000003054 catalyst Substances 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 13
- -1 nitrile compound Chemical class 0.000 claims description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 6
- BTGRAWJCKBQKAO-UHFFFAOYSA-N adiponitrile Chemical compound N#CCCCCC#N BTGRAWJCKBQKAO-UHFFFAOYSA-N 0.000 claims description 6
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- BWLUMTFWVZZZND-UHFFFAOYSA-N Dibenzylamine Chemical compound C=1C=CC=CC=1CNCC1=CC=CC=C1 BWLUMTFWVZZZND-UHFFFAOYSA-N 0.000 claims description 4
- 125000001931 aliphatic group Chemical group 0.000 claims description 4
- WGQKYBSKWIADBV-UHFFFAOYSA-N benzylamine Chemical compound NCC1=CC=CC=C1 WGQKYBSKWIADBV-UHFFFAOYSA-N 0.000 claims description 4
- KBMSFJFLSXLIDJ-UHFFFAOYSA-N 6-aminohexanenitrile Chemical compound NCCCCCC#N KBMSFJFLSXLIDJ-UHFFFAOYSA-N 0.000 claims description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 3
- 239000001569 carbon dioxide Substances 0.000 claims description 3
- 238000005984 hydrogenation reaction Methods 0.000 claims description 3
- MSHFFPQJBNDWHU-UHFFFAOYSA-N C(C1=CC=CC=C1)N.C(C1=CC=CC=C1)#N Chemical compound C(C1=CC=CC=C1)N.C(C1=CC=CC=C1)#N MSHFFPQJBNDWHU-UHFFFAOYSA-N 0.000 claims description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 150000004678 hydrides Chemical class 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 150000002466 imines Chemical class 0.000 claims description 2
- 150000003141 primary amines Chemical class 0.000 claims description 2
- 239000003223 protective agent Substances 0.000 claims description 2
- 239000012429 reaction media Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- JFDZBHWFFUWGJE-UHFFFAOYSA-N benzonitrile Chemical compound N#CC1=CC=CC=C1 JFDZBHWFFUWGJE-UHFFFAOYSA-N 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 2
- 238000004445 quantitative analysis Methods 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 229920002302 Nylon 6,6 Polymers 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2010099198A JP5565799B2 (ja) | 2010-04-22 | 2010-04-22 | 超臨界二酸化炭素中における有機ニトリル化合物の水素化物の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2010099198A JP5565799B2 (ja) | 2010-04-22 | 2010-04-22 | 超臨界二酸化炭素中における有機ニトリル化合物の水素化物の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011225502A JP2011225502A (ja) | 2011-11-10 |
| JP2011225502A5 true JP2011225502A5 (enExample) | 2013-07-04 |
| JP5565799B2 JP5565799B2 (ja) | 2014-08-06 |
Family
ID=45041354
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010099198A Expired - Fee Related JP5565799B2 (ja) | 2010-04-22 | 2010-04-22 | 超臨界二酸化炭素中における有機ニトリル化合物の水素化物の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP5565799B2 (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5659860B2 (ja) * | 2011-02-28 | 2015-01-28 | エヌ・イーケムキャット株式会社 | ニトリル化合物水素化用パラジウム含有触媒および該触媒を用いたニトリル化合物の水素化方法 |
| CN102924286B (zh) * | 2012-10-31 | 2014-06-11 | 万华化学集团股份有限公司 | 一种n1-(2-氨乙基)-1,2-乙二胺的制备方法 |
| CN104258874A (zh) * | 2014-08-19 | 2015-01-07 | 华南理工大学 | 用于苯腈选择性加氢偶联一步制备亚胺的催化剂及制法与应用 |
| CN110922605B (zh) * | 2019-12-09 | 2022-03-08 | 海南大学 | 一种利用超临界二氧化碳制备共价有机框架材料的方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5663944A (en) * | 1979-10-26 | 1981-05-30 | Takeda Chem Ind Ltd | Reduction of aromatic nitrile |
| US4389348A (en) * | 1981-10-26 | 1983-06-21 | Allied Corporation | Selective hydrogenation of dinitrile to omega-aminonitrile and supported rhodium-containing catalyst therefor |
| GB9607917D0 (en) * | 1996-04-17 | 1996-06-19 | Swan Thomas & Co Ltd | Supercritical hydrogenation |
| GB2374071A (en) * | 2001-04-06 | 2002-10-09 | Swan Thomas & Co Ltd | Hydrogenation reactions using supercritical fluids |
-
2010
- 2010-04-22 JP JP2010099198A patent/JP5565799B2/ja not_active Expired - Fee Related
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