JP2008511655A - 最適化液相酸化 - Google Patents

最適化液相酸化 Download PDF

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Publication number
JP2008511655A
JP2008511655A JP2007530276A JP2007530276A JP2008511655A JP 2008511655 A JP2008511655 A JP 2008511655A JP 2007530276 A JP2007530276 A JP 2007530276A JP 2007530276 A JP2007530276 A JP 2007530276A JP 2008511655 A JP2008511655 A JP 2008511655A
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Japan
Prior art keywords
reaction medium
oxidation
xylene
reaction
reactor
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JP2007530276A
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Japanese (ja)
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JP2008511655A5 (enExample
Inventor
ジョージ ワンダース，アラン
ジョルジュ ラボワ，ジーノ
エドワン，ジュニア サムナー，チャールズ
ウェイン ダベンポート，ブライアン
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Eastman Chemical Co
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Eastman Chemical Co
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Publication date
Application filed by Eastman Chemical Co filed Critical Eastman Chemical Co
Publication of JP2008511655A publication Critical patent/JP2008511655A/ja
Publication of JP2008511655A5 publication Critical patent/JP2008511655A5/ja
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Ink Jet (AREA)
  • Golf Clubs (AREA)
  • Lubricants (AREA)
JP2007530276A 2004-09-02 2005-08-29 最適化液相酸化 Pending JP2008511655A (ja)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US60673904P 2004-09-02 2004-09-02
US63149404P 2004-11-29 2004-11-29
US11/154,478 US20060047153A1 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
PCT/US2005/030854 WO2006028815A2 (en) 2004-09-02 2005-08-29 Optimized liquid-phase oxidation

Publications (2)

Publication Number Publication Date
JP2008511655A true JP2008511655A (ja) 2008-04-17
JP2008511655A5 JP2008511655A5 (enExample) 2008-10-16

Family

ID=35504646

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2007530276A Pending JP2008511655A (ja) 2004-09-02 2005-08-29 最適化液相酸化

Country Status (10)

Country Link
US (1) US20060047153A1 (enExample)
EP (1) EP1784377B1 (enExample)
JP (1) JP2008511655A (enExample)
KR (1) KR101392653B1 (enExample)
CN (2) CN101010279B (enExample)
AT (1) ATE482178T1 (enExample)
CA (1) CA2576654A1 (enExample)
DE (1) DE602005023744D1 (enExample)
MX (1) MX2007002413A (enExample)
WO (1) WO2006028815A2 (enExample)

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5141624B1 (enExample) * 1970-12-30 1976-11-11
JPS5257134A (en) * 1975-10-31 1977-05-11 Mitsubishi Chem Ind Ltd Process for preparation of aromatic polycarboxylic acids
JPS61106535A (ja) * 1984-10-30 1986-05-24 Mitsubishi Chem Ind Ltd 安息香酸の回収法
JPH09278709A (ja) * 1996-02-13 1997-10-28 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
JP2000128824A (ja) * 1998-10-27 2000-05-09 Mitsui Chemicals Inc 芳香族カルボン酸の製造方法
JP2001247511A (ja) * 2000-03-07 2001-09-11 Mitsubishi Chemicals Corp 芳香族カルボン酸の製造方法
JP2006509044A (ja) * 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法

Family Cites Families (101)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1902550A (en) * 1930-01-31 1933-03-21 Nat Synthetic Corp Process of oxidizing cyclic organic compounds
US3082250A (en) * 1958-05-05 1963-03-19 Standard Oil Co Recovery of phthalic acid products
US3071447A (en) * 1958-09-09 1963-01-01 Whiting Corp Hydraulic classifier
US3029278A (en) * 1958-12-11 1962-04-10 Standard Oil Co Process for separation of phthalic acids
GB1007570A (en) * 1961-07-24 1965-10-13 Socaty Process for the catalytic oxidation of xylenes or industrial mixtures of xylenes
NL282031A (enExample) * 1961-08-14
NL294776A (enExample) * 1962-10-06
US3244744A (en) * 1963-02-27 1966-04-05 Standard Oil Co Separation process for isophthalic acid and terephthalic acid
DE1276628C2 (de) * 1963-05-20 1975-01-16 Rudzki, Henryk Stanislaw, Dr., Los Angeles, Calif. (V.St.A.) Verfahren zur herstellung von isophtalsaeure und/oder terephthalsaeure
US3388157A (en) * 1965-02-10 1968-06-11 Ethyl Corp Process for the production of dicarboxylic acids
NL6606774A (enExample) * 1965-05-17 1966-11-18
US3497552A (en) * 1966-07-18 1970-02-24 Standard Oil Co Continuous crystallization in a plurality of cooling stages using dilutions by cooled solvent of feed to each stage
US3584039A (en) * 1967-08-30 1971-06-08 Standard Oil Co Fiber-grade terephthalic acid by catalytic hydrogen treatment of dissolved impure terephthalic acid
US3556733A (en) * 1968-04-05 1971-01-19 Struthers Scientific Int Corp Fines dissolver for crystallizers
AT282466B (de) * 1968-07-25 1970-06-25 Oemv Ag Bitumenblasverfahren und Einrichtung zur Durchführung desselben
DE1792402A1 (de) * 1968-08-29 1971-11-11 Dynamit Nobel Ag Verfahren zur Durchfuehrung exothermer chemischer Reaktionen in heterogenen Gas-Fluessigkeits-Gemischen
US3660476A (en) * 1968-10-30 1972-05-02 Teijin Ltd Method for the preparation of terephthalic acid
US3708532A (en) * 1968-11-04 1973-01-02 Teijin Ltd Process for the continuous purification of crude terephthalic acid
JPS5328419B1 (enExample) * 1971-04-26 1978-08-15
US3785779A (en) * 1971-08-02 1974-01-15 Exxon Research Engineering Co Gas liquid inlet distributor
JPS5544644B2 (enExample) * 1971-09-23 1980-11-13
NL169993C (nl) * 1972-01-13 1982-09-16 Maruzen Oil Co Ltd Werkwijze ter bereiding van tereftaalzuur.
DE2217003C2 (de) * 1972-04-08 1983-12-15 Chemische Werke Hüls AG, 4370 Marl Verfahren und Vorrichtung zur kontinuierlichen Herstellung von gesättigten aliphatischen Dicarbonsäuren
US3931305A (en) * 1973-08-20 1976-01-06 Standard Oil Company Terephthalic acid recovery by continuous flash crystallization
JPS5278846A (en) * 1975-12-25 1977-07-02 Matsuyama Sekyu Kagaku Kk Continuous production of high purity telephthalic acid
GB1574651A (en) * 1976-02-24 1980-09-10 Matsuyama Petrochemicals Inc Process and apparatus for producing aromatic dicarboxylic acids
DE2623977C3 (de) * 1976-05-28 1979-04-12 Nukem Gmbh, 6450 Hanau Verfahren und Vorrichtung zur Herstellung von rieselfähigem, direkt verpressbarem Urandioxid-Pulver
SU1126202A3 (ru) * 1976-05-28 1984-11-23 Институт Фор Атомэнерги (Фирма) Способ непрерывной многостадийной кристаллизации из раствора
US4185073A (en) * 1976-07-26 1980-01-22 Standard Oil Company (Indiana) Apparatus for iso- or terephthalic acid production in and recovery from benzoic acid-water solvent system
US4081464A (en) * 1976-07-26 1978-03-28 Standard Oil Company Iso- or terephthalic acid production in and recovery from benzoic acid-water solvent system
GB1542320A (en) * 1976-10-26 1979-03-14 Labofina Sa Process for the preparation of aromatic dicarboxylic acids
US4158738A (en) * 1977-05-26 1979-06-19 E. I. Du Pont De Nemours And Company Process for the production of fiber-grade terephthalic acid
DE2805915C3 (de) * 1978-02-13 1981-11-05 Dynamit Nobel Ag, 5210 Troisdorf Reaktor zur Oxidation von Gemischen aus p-Xylol und p-Toluylsäuremethylester mit sauerstoffhaltigen Gasen in flüssiger Phase
US4263448A (en) * 1979-03-30 1981-04-21 Halcon Research And Development Corp. Process for oxidation of hydrocarbons
US4255590A (en) * 1979-11-08 1981-03-10 Standard Oil Company (Indiana) Combination of pyrolysis and incineration of solid mixture of oxygen-containing aromatic compounds obtained as residue of manufacture of benzene di- and tricarboxylic acids
US4334086A (en) * 1981-03-16 1982-06-08 Labofina S.A. Production of terephthalic acid
US4459365A (en) * 1981-05-29 1984-07-10 Mitsubishi Gas Chemical Company, Inc. Method of recovering a catalytic metal
US4456767A (en) * 1981-07-27 1984-06-26 Rhone-Poulenc, Inc. Solvent and catalyst recovery and recycle in the manufacture of phenoxybenzoic acid
US4391985A (en) * 1981-11-16 1983-07-05 Eastman Kodak Company Process for the separation of isophthalic acid from terephthalic acid
DE3363127D1 (en) * 1982-02-09 1986-05-28 Bbc Brown Boveri & Cie Method and apparatus for treating a liquid with a gas
JPS59104345A (ja) * 1982-12-03 1984-06-16 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造方法
JPS6036439A (ja) * 1983-08-09 1985-02-25 Mitsubishi Chem Ind Ltd テレフタル酸の製法
US4500732A (en) * 1983-09-15 1985-02-19 Standard Oil Company (Indiana) Process for removal and recycle of p-toluic acid from terephthalic acid crystallizer solvent
US4835307A (en) * 1984-12-13 1989-05-30 Amoco Corporation Method and apparatus for controlling the manufacture of terephthalic acid to control the level and variability of the contaminant content and the optical density
US4648999A (en) * 1985-07-22 1987-03-10 M. W. Kellogg Company Apparatus for contacting fluid with solid
US5099064A (en) * 1985-12-30 1992-03-24 Amoco Corporation Method for increasing conversion efficiency for oxidation of an alkyl aromatic compound to an aromatic carboxylic acid
US4892970A (en) * 1985-12-30 1990-01-09 Amoco Corporation Staged aromatics oxidation in aqueous systems
US4914230A (en) * 1986-07-28 1990-04-03 Amoco Corporation Catalyst recovery method
JPH078821B2 (ja) * 1986-09-26 1995-02-01 三井石油化学工業株式会社 芳香族カルボン酸の製造方法
JPH078823B2 (ja) * 1986-10-20 1995-02-01 三井石油化学工業株式会社 高純度テレフタル酸の製造方法
US4900480A (en) * 1986-10-21 1990-02-13 Union Carbide Corporation Gas-liquid mixing
DE3704720A1 (de) * 1987-02-14 1988-08-25 Huels Troisdorf Verfahren und vorrichtung zur herstellung von benzolcarbonsaeuren bzw. benzoldicarbonsaeureestern
US5211924A (en) * 1988-02-29 1993-05-18 Amoco Corporation Method and apparatus for increasing conversion efficiency and reducing power costs for oxidation of an aromatic alkyl to an aromatic carboxylic acid
GB8811114D0 (en) * 1988-05-11 1988-06-15 Ici Plc Fermentation process & apparatus
US4833269A (en) * 1988-08-05 1989-05-23 Amoco Corporation Method for purifying terephthalic acid recycle streams
US4939297A (en) * 1989-06-05 1990-07-03 Eastman Kodak Company Extraction process for removal of impurities from terephthalic acid filtrate
US5004830A (en) * 1989-11-29 1991-04-02 Amoco Corporation Process for oxidation of alkyl aromatic compounds
US5126037A (en) * 1990-05-04 1992-06-30 Union Oil Company Of California Geopreater heating method and apparatus
ES2064912T3 (es) * 1990-06-25 1995-02-01 Mitsubishi Gas Chemical Co Procedimiento para producir acido isoftalico de elevada pureza.
US5095145A (en) * 1990-11-05 1992-03-10 Amoco Corporation Preparation of purified terephthalic acid from waste polyethylene terephthalate
US5095142A (en) * 1990-11-29 1992-03-10 Amoco Corporation Solvent recovery during production of aromatic polycarboxylic acids
GB9102393D0 (en) * 1991-02-05 1991-03-20 Ici Plc Production of terephthalic acid
GB9104776D0 (en) * 1991-03-07 1991-04-17 Ici Plc Process for the production of terephthalic acid
US5227570A (en) * 1991-12-02 1993-07-13 Taiwan Styrene Monomer Corporation Process for separation of ethylbenzene or ethylbenzene/p-xylene from a xylene isomers mixture
US5292934A (en) * 1992-06-18 1994-03-08 Amoco Corporation Method for preparing aromatic carboxylic acids
JPH0795538A (ja) * 1993-09-17 1995-04-07 Canon Inc 画像記録再生装置
US5523474A (en) * 1994-05-11 1996-06-04 Praxair Technology, Inc. Terephthalic acid production using evaporative cooling
US5518700A (en) * 1994-06-25 1996-05-21 Shell Oil Company Cyclonic reactor
US5712412A (en) * 1994-12-26 1998-01-27 Mitsubishi Gas Chemical Co., Inc. Process for producing highly pure terephthalic acid
GB2299767B (en) * 1995-04-07 1998-05-13 Norske Stats Oljeselskap Regneration of fischer-tropsch catalysts
US6013835A (en) * 1995-06-07 2000-01-11 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid
US5767311A (en) * 1995-06-07 1998-06-16 Glitsch International, Inc. Method and apparatus for preparing purified terephtalic acid
FR2739375B1 (fr) * 1995-09-29 1997-12-05 Inst Francais Du Petrole Production de paraxylene a partir d'un effluent de dismutation paraselective du toluene par un procede de cristallisation associe a une adsorption en lit mobile simule
US6376733B1 (en) * 1996-01-25 2002-04-23 Exxonmobil Chemical Patents Inc. Process for production of paraxylene
US5756833A (en) * 1996-02-01 1998-05-26 Amoco Corporation Catalytic purification and recovery of dicarboxylic aromatic acids
ID15851A (id) * 1996-02-13 1997-08-14 Mitsubishi Chem Corp Proses untuk menghasilkan suatu asam aromatik karboksilik
JP3757995B2 (ja) * 1996-07-12 2006-03-22 三菱瓦斯化学株式会社 高純度イソフタル酸の製造方法
JPH1045667A (ja) * 1996-07-29 1998-02-17 Mitsubishi Gas Chem Co Inc 分散媒置換装置を用いた高純度テレフタル酸の製造方法
US6133476A (en) * 1996-09-17 2000-10-17 Lin; Tsong-Dar Vincent Process for purification of aromatic polycarboxylic acids
ES2274549T3 (es) * 1996-09-24 2007-05-16 MERCK & CO., INC. Compuestos para la inhibicion de la angiogenesis por terapia de genes .
IT1288760B1 (it) * 1996-10-17 1998-09-24 Fiat Ricerche Motore elettrostatico lineare
GB9701251D0 (en) * 1997-01-22 1997-03-12 Bp Chem Int Ltd Process
US6037491A (en) * 1997-07-25 2000-03-14 Rpc Inc. Methods and devices for controlling hydrocarbon oxidations to respective acids by adjusting the solvent to hydrocarbon ratio
WO1999040058A1 (en) * 1998-02-09 1999-08-12 Rpc, Inc. Process for treating cobalt catalyst in oxidation mixtures of hydrocarbons to dibasic acids
US6362367B2 (en) * 1998-04-21 2002-03-26 Union Carbide Chemicals & Plastics Technology Corp. Preparation of organic acids
US6080372A (en) * 1998-09-11 2000-06-27 Air Products And Chemicals, Inc. Two stage reactor for continuous three phase slurry hydrogenation and method of operation
US6392091B2 (en) * 1998-11-24 2002-05-21 Tsong-Dar Vincent Lin Process of purifying and producing high purity aromatic polycarboxylic acids
KR100642625B1 (ko) * 1998-11-24 2006-11-10 티. 디. 빈센트 린 고순도 방향족 폴리카르복실산 및 이것의 유도체를 정제및 생성하는 방법
IT1311976B1 (it) * 1999-03-25 2002-03-22 Franco Codignola Procedimento per la produzione di acidi aromatici.
CA2396967A1 (en) * 2000-01-21 2001-07-26 Bp Corporation North America Inc. Production of high purity aromatic carboxylic acid by oxidation in benzoic acid and water solvent
US6541525B2 (en) * 2001-03-27 2003-04-01 Exxonmobil Research And Engineering Company Slurry catalyst rejuvenation in-situ in slurry reactor
US6984753B2 (en) * 2001-05-15 2006-01-10 Dow Italia S.R.L. Agitation system for alkylbenzene oxidation reactors
US7135596B2 (en) * 2002-04-23 2006-11-14 Bp Corporation North America Inc. Method of removing iron contaminants from liquid streams during the manufacture and/or purification of aromatic acids
US7161027B2 (en) * 2002-12-09 2007-01-09 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7132566B2 (en) * 2003-09-22 2006-11-07 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7494641B2 (en) * 2003-06-05 2009-02-24 Eastman Chemical Company Extraction process for removal of impurities from an oxidizer purge stream in the synthesis of carboxylic acid
US7485746B2 (en) * 2003-11-14 2009-02-03 Bp Corporation North America Inc. Staged countercurrent oxidation
US6838487B1 (en) * 2003-12-04 2005-01-04 Rentech, Inc. Method and apparatus for regenerating an iron-based Fischer-Tropsch catalyst
US7615663B2 (en) * 2004-09-02 2009-11-10 Eastman Chemical Company Optimized production of aromatic dicarboxylic acids
US7504535B2 (en) * 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5141624B1 (enExample) * 1970-12-30 1976-11-11
JPS5257134A (en) * 1975-10-31 1977-05-11 Mitsubishi Chem Ind Ltd Process for preparation of aromatic polycarboxylic acids
JPS61106535A (ja) * 1984-10-30 1986-05-24 Mitsubishi Chem Ind Ltd 安息香酸の回収法
JPH09278709A (ja) * 1996-02-13 1997-10-28 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
JP2000128824A (ja) * 1998-10-27 2000-05-09 Mitsui Chemicals Inc 芳香族カルボン酸の製造方法
JP2001247511A (ja) * 2000-03-07 2001-09-11 Mitsubishi Chemicals Corp 芳香族カルボン酸の製造方法
JP2006509044A (ja) * 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法

Also Published As

Publication number Publication date
CN101010279A (zh) 2007-08-01
US20060047153A1 (en) 2006-03-02
KR101392653B1 (ko) 2014-05-07
CN102701961A (zh) 2012-10-03
KR20070054696A (ko) 2007-05-29
EP1784377B1 (en) 2010-09-22
WO2006028815A3 (en) 2006-04-27
MX2007002413A (es) 2007-04-23
EP1784377A2 (en) 2007-05-16
CA2576654A1 (en) 2006-03-16
WO2006028815A2 (en) 2006-03-16
DE602005023744D1 (en) 2010-11-04
CN102701961B (zh) 2015-11-25
ATE482178T1 (de) 2010-10-15
CN101010279B (zh) 2012-06-13

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