JP2003300949A5 - - Google Patents
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- Publication number
- JP2003300949A5 JP2003300949A5 JP2002096244A JP2002096244A JP2003300949A5 JP 2003300949 A5 JP2003300949 A5 JP 2003300949A5 JP 2002096244 A JP2002096244 A JP 2002096244A JP 2002096244 A JP2002096244 A JP 2002096244A JP 2003300949 A5 JP2003300949 A5 JP 2003300949A5
- Authority
- JP
- Japan
- Prior art keywords
- amine
- group
- represented
- process according
- anion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 14
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims 6
- 150000003512 tertiary amines Chemical class 0.000 claims 5
- KXDAEFPNCMNJSK-UHFFFAOYSA-N Benzamide Chemical compound NC(=O)C1=CC=CC=C1 KXDAEFPNCMNJSK-UHFFFAOYSA-N 0.000 claims 4
- -1 N-substituted piperazines Chemical class 0.000 claims 4
- 150000001450 anions Chemical class 0.000 claims 4
- WFKAJVHLWXSISD-UHFFFAOYSA-N isobutyramide Chemical compound CC(C)C(N)=O WFKAJVHLWXSISD-UHFFFAOYSA-N 0.000 claims 4
- 150000003335 secondary amines Chemical class 0.000 claims 4
- SDTMFDGELKWGFT-UHFFFAOYSA-N 2-methylpropan-2-olate Chemical compound CC(C)(C)[O-] SDTMFDGELKWGFT-UHFFFAOYSA-N 0.000 claims 3
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims 3
- SJRJJKPEHAURKC-UHFFFAOYSA-N N-Methylmorpholine Chemical group CN1CCOCC1 SJRJJKPEHAURKC-UHFFFAOYSA-N 0.000 claims 3
- 239000000654 additive Substances 0.000 claims 3
- 150000001412 amines Chemical class 0.000 claims 3
- JFDZBHWFFUWGJE-UHFFFAOYSA-N benzonitrile Chemical compound N#CC1=CC=CC=C1 JFDZBHWFFUWGJE-UHFFFAOYSA-N 0.000 claims 3
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 claims 3
- HHFAWKCIHAUFRX-UHFFFAOYSA-N ethoxide Chemical compound CC[O-] HHFAWKCIHAUFRX-UHFFFAOYSA-N 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical group [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 3
- NBTOZLQBSIZIKS-UHFFFAOYSA-N methoxide Chemical compound [O-]C NBTOZLQBSIZIKS-UHFFFAOYSA-N 0.000 claims 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims 3
- OGHBATFHNDZKSO-UHFFFAOYSA-N propan-2-olate Chemical compound CC(C)[O-] OGHBATFHNDZKSO-UHFFFAOYSA-N 0.000 claims 3
- UWYZHKAOTLEWKK-UHFFFAOYSA-N 1,2,3,4-tetrahydroisoquinoline Chemical compound C1=CC=C2CNCCC2=C1 UWYZHKAOTLEWKK-UHFFFAOYSA-N 0.000 claims 2
- NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 claims 2
- 230000000996 additive effect Effects 0.000 claims 2
- 125000003342 alkenyl group Chemical group 0.000 claims 2
- 125000000217 alkyl group Chemical group 0.000 claims 2
- 125000003710 aryl alkyl group Chemical group 0.000 claims 2
- 125000004432 carbon atom Chemical group C* 0.000 claims 2
- JQVDAXLFBXTEQA-UHFFFAOYSA-N dibutylamine Chemical compound CCCCNCCCC JQVDAXLFBXTEQA-UHFFFAOYSA-N 0.000 claims 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims 2
- 229940047889 isobutyramide Drugs 0.000 claims 2
- LRDFRRGEGBBSRN-UHFFFAOYSA-N isobutyronitrile Chemical compound CC(C)C#N LRDFRRGEGBBSRN-UHFFFAOYSA-N 0.000 claims 2
- 239000003960 organic solvent Substances 0.000 claims 2
- FVSKHRXBFJPNKK-UHFFFAOYSA-N propionitrile Chemical compound CCC#N FVSKHRXBFJPNKK-UHFFFAOYSA-N 0.000 claims 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims 1
- BWLUMTFWVZZZND-UHFFFAOYSA-N Dibenzylamine Chemical compound C=1C=CC=CC=1CNCC1=CC=CC=C1 BWLUMTFWVZZZND-UHFFFAOYSA-N 0.000 claims 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 1
- 150000004703 alkoxides Chemical class 0.000 claims 1
- UPABQMWFWCMOFV-UHFFFAOYSA-N benethamine Chemical compound C=1C=CC=CC=1CNCCC1=CC=CC=C1 UPABQMWFWCMOFV-UHFFFAOYSA-N 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- XXBDWLFCJWSEKW-UHFFFAOYSA-N dimethylbenzylamine Chemical compound CN(C)CC1=CC=CC=C1 XXBDWLFCJWSEKW-UHFFFAOYSA-N 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 239000002638 heterogeneous catalyst Substances 0.000 claims 1
- 150000002462 imidazolines Chemical class 0.000 claims 1
- 150000002500 ions Chemical class 0.000 claims 1
- 229940035429 isobutyl alcohol Drugs 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- YWWNNLPSZSEZNZ-UHFFFAOYSA-N n,n-dimethyldecan-1-amine Chemical compound CCCCCCCCCCN(C)C YWWNNLPSZSEZNZ-UHFFFAOYSA-N 0.000 claims 1
- GTWJETSWSUWSEJ-UHFFFAOYSA-N n-benzylaniline Chemical compound C=1C=CC=CC=1CNC1=CC=CC=C1 GTWJETSWSUWSEJ-UHFFFAOYSA-N 0.000 claims 1
- 239000007800 oxidant agent Substances 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 150000003222 pyridines Chemical class 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP02252303A EP1348692B1 (en) | 2002-03-28 | 2002-03-28 | Process for the preparation of amine oxides |
| US10/113,208 US6617454B1 (en) | 2002-03-28 | 2002-03-28 | Process for the preparation of amine oxides |
| JP2002096244A JP4173676B2 (ja) | 2002-03-28 | 2002-03-29 | アミンオキシドの製造方法 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP02252303A EP1348692B1 (en) | 2002-03-28 | 2002-03-28 | Process for the preparation of amine oxides |
| US10/113,208 US6617454B1 (en) | 2002-03-28 | 2002-03-28 | Process for the preparation of amine oxides |
| JP2002096244A JP4173676B2 (ja) | 2002-03-28 | 2002-03-29 | アミンオキシドの製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2003300949A JP2003300949A (ja) | 2003-10-21 |
| JP2003300949A5 true JP2003300949A5 (enExample) | 2005-10-27 |
| JP4173676B2 JP4173676B2 (ja) | 2008-10-29 |
Family
ID=29553805
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2002096244A Expired - Fee Related JP4173676B2 (ja) | 2002-03-28 | 2002-03-29 | アミンオキシドの製造方法 |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US6617454B1 (enExample) |
| EP (1) | EP1348692B1 (enExample) |
| JP (1) | JP4173676B2 (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB201122163D0 (en) * | 2011-12-22 | 2012-02-01 | Scg Chemicals Co Ltd | Modification of layered double hydroxides |
| JP6188028B2 (ja) * | 2012-07-02 | 2017-08-30 | 国立大学法人大阪大学 | 脂環式ｎ−オキシル化合物の製造方法 |
| CN107118132B (zh) * | 2017-06-13 | 2019-08-23 | 贵州医科大学 | 酚氧类氮氧化物作为去乙酰化酶抑制剂的抗肿瘤应用 |
| CN109096143B (zh) * | 2018-10-09 | 2021-08-27 | 南京工业大学 | 一种采用过氧乙酸合成二乙基羟胺的方法 |
| CN109761859B (zh) * | 2019-03-04 | 2021-06-08 | 济宁康德瑞化工科技有限公司 | 一种有机胺氧化物的制备方法 |
| CN113651773A (zh) * | 2021-09-23 | 2021-11-16 | 上海昶法新材料有限公司 | 一种氧化甲基吗啉的合成和提纯方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3283007A (en) | 1963-06-28 | 1966-11-01 | Du Pont | Production of amine oxides |
| US3424780A (en) | 1964-03-16 | 1969-01-28 | Upjohn Co | Process for manufacturing polyisocyanates |
| US4565891A (en) | 1984-07-19 | 1986-01-21 | The Procter & Gamble Company | Oxidation of tertiary amines using octacyanomolybdate or iron (III) salts as catalysts |
| US4889954A (en) | 1988-06-30 | 1989-12-26 | Ethyl Corporation | Amine oxide process |
| US5130488A (en) | 1989-04-26 | 1992-07-14 | Ethyl Corporation | Process for preparing tert-amine oxides |
| US5563288A (en) * | 1995-06-07 | 1996-10-08 | Osi Specialties, Inc. | Process for the preparation of tertiary aminocarbonates and aminoethers |
| US6323367B1 (en) | 2000-11-22 | 2001-11-27 | Council Of Scientific And Industrial Research | Process for the preparation of amine oxides |
-
2002
- 2002-03-28 US US10/113,208 patent/US6617454B1/en not_active Expired - Fee Related
- 2002-03-28 EP EP02252303A patent/EP1348692B1/en not_active Expired - Lifetime
- 2002-03-29 JP JP2002096244A patent/JP4173676B2/ja not_active Expired - Fee Related
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