JP2002520030A - 結晶フルクトースの製造方法 - Google Patents
結晶フルクトースの製造方法Info
- Publication number
- JP2002520030A JP2002520030A JP2000559260A JP2000559260A JP2002520030A JP 2002520030 A JP2002520030 A JP 2002520030A JP 2000559260 A JP2000559260 A JP 2000559260A JP 2000559260 A JP2000559260 A JP 2000559260A JP 2002520030 A JP2002520030 A JP 2002520030A
- Authority
- JP
- Japan
- Prior art keywords
- fructose
- crystals
- syrup
- solution
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 239000005715 Fructose Substances 0.000 title claims abstract description 126
- 229930091371 Fructose Natural products 0.000 title claims abstract description 126
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 title claims abstract description 101
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 239000013078 crystal Substances 0.000 claims abstract description 58
- -1 fructose dihydrate Chemical class 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 26
- 238000010899 nucleation Methods 0.000 claims abstract description 18
- 230000008018 melting Effects 0.000 claims abstract description 16
- 238000002844 melting Methods 0.000 claims abstract description 16
- 238000009331 sowing Methods 0.000 claims abstract description 10
- 238000001704 evaporation Methods 0.000 claims abstract description 9
- LKDRXBCSQODPBY-ARQDHWQXSA-N beta-D-fructopyranose Chemical compound OC[C@@]1(O)OC[C@@H](O)[C@@H](O)[C@@H]1O LKDRXBCSQODPBY-ARQDHWQXSA-N 0.000 claims abstract description 8
- 230000008020 evaporation Effects 0.000 claims abstract description 8
- 235000021433 fructose syrup Nutrition 0.000 claims abstract description 6
- 239000000126 substance Substances 0.000 claims abstract description 3
- 235000020357 syrup Nutrition 0.000 claims description 42
- 239000006188 syrup Substances 0.000 claims description 42
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 235000000346 sugar Nutrition 0.000 claims description 11
- 239000002245 particle Substances 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 8
- 239000012452 mother liquor Substances 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 4
- 229960002737 fructose Drugs 0.000 description 76
- 239000000243 solution Substances 0.000 description 19
- 238000012937 correction Methods 0.000 description 18
- 238000002425 crystallisation Methods 0.000 description 10
- 230000008025 crystallization Effects 0.000 description 9
- 230000015572 biosynthetic process Effects 0.000 description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 239000008103 glucose Substances 0.000 description 3
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 3
- 229910052753 mercury Inorganic materials 0.000 description 3
- 238000007711 solidification Methods 0.000 description 3
- 230000008023 solidification Effects 0.000 description 3
- 125000002015 acyclic group Chemical group 0.000 description 2
- LKDRXBCSQODPBY-ZXXMMSQZSA-N alpha-D-fructopyranose Chemical compound OC[C@]1(O)OC[C@@H](O)[C@@H](O)[C@@H]1O LKDRXBCSQODPBY-ZXXMMSQZSA-N 0.000 description 2
- 235000008504 concentrate Nutrition 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000002845 discoloration Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 150000008163 sugars Chemical class 0.000 description 2
- 238000013519 translation Methods 0.000 description 2
- RFSUNEUAIZKAJO-VRPWFDPXSA-N D-fructofuranose Chemical compound OC[C@H]1OC(O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-VRPWFDPXSA-N 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- RFSUNEUAIZKAJO-ZXXMMSQZSA-N alpha-D-fructofuranose Chemical group OC[C@H]1O[C@@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ZXXMMSQZSA-N 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000004683 dihydrates Chemical class 0.000 description 1
- 150000002231 fructose derivatives Chemical class 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000002054 inoculum Substances 0.000 description 1
- 238000006317 isomerization reaction Methods 0.000 description 1
- 150000002576 ketones Chemical group 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 230000027870 phototropism Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000020374 simple syrup Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Saccharide Compounds (AREA)
- Jellies, Jams, And Syrups (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP98202278A EP0971040B1 (fr) | 1998-07-08 | 1998-07-08 | Procédé de fabrication de fructose cristallisé |
| EP98202278.2 | 1998-07-08 | ||
| PCT/EP1999/004732 WO2000003040A1 (fr) | 1998-07-08 | 1999-07-05 | Procede de fabrication de fructose cristallise |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2002520030A true JP2002520030A (ja) | 2002-07-09 |
| JP2002520030A5 JP2002520030A5 (https=) | 2006-08-31 |
Family
ID=8233899
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2000559260A Ceased JP2002520030A (ja) | 1998-07-08 | 1999-07-05 | 結晶フルクトースの製造方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US6607603B1 (https=) |
| EP (1) | EP0971040B1 (https=) |
| JP (1) | JP2002520030A (https=) |
| AT (1) | ATE249524T1 (https=) |
| DE (1) | DE69818023T2 (https=) |
| DK (1) | DK0971040T3 (https=) |
| ES (1) | ES2206826T3 (https=) |
| IL (1) | IL140640A (https=) |
| WO (1) | WO2000003040A1 (https=) |
| ZA (1) | ZA200100133B (https=) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2292803B1 (en) | 2009-07-07 | 2013-02-13 | DuPont Nutrition Biosciences ApS | Separation process |
| WO2013049424A1 (en) * | 2011-09-28 | 2013-04-04 | Wisconsin Alumni Research Foundation | Catalytic conversion of cellulose to fuels and chemicals using boronic acids |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2588449A (en) * | 1950-03-03 | 1952-03-11 | Us Agriculture | Levulose dihydrate |
| US3513023A (en) * | 1966-04-29 | 1970-05-19 | Boehringer Mannheim Gmbh | Process for the production of crystalline fructose |
| US3607392A (en) * | 1967-12-21 | 1971-09-21 | Boehringer Mannheim Gmbh | Process and apparatus for the recovery of crystalline fructose from methanolic solution |
| US3883365A (en) * | 1972-01-04 | 1975-05-13 | Suomen Sokeri Oy | PH adjustment in fructose crystallization for increased yield |
| US4199373A (en) * | 1979-04-13 | 1980-04-22 | Chimicasa Gmbh | Process for the manufacture of crystalline fructose |
| GB8506482D0 (en) * | 1985-03-13 | 1985-04-17 | Tate & Lyle Plc | Sugar process |
| US5047088A (en) * | 1989-06-30 | 1991-09-10 | A. E. Staley Manufacturing Company | Method for crystallization of fructose |
-
1998
- 1998-07-08 DE DE69818023T patent/DE69818023T2/de not_active Expired - Fee Related
- 1998-07-08 ES ES98202278T patent/ES2206826T3/es not_active Expired - Lifetime
- 1998-07-08 EP EP98202278A patent/EP0971040B1/fr not_active Expired - Lifetime
- 1998-07-08 DK DK98202278T patent/DK0971040T3/da active
- 1998-07-08 AT AT98202278T patent/ATE249524T1/de not_active IP Right Cessation
-
1999
- 1999-07-05 US US09/743,157 patent/US6607603B1/en not_active Expired - Fee Related
- 1999-07-05 IL IL14064099A patent/IL140640A/xx not_active IP Right Cessation
- 1999-07-05 JP JP2000559260A patent/JP2002520030A/ja not_active Ceased
- 1999-07-05 WO PCT/EP1999/004732 patent/WO2000003040A1/fr not_active Ceased
-
2001
- 2001-01-05 ZA ZA200100133A patent/ZA200100133B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ES2206826T3 (es) | 2004-05-16 |
| WO2000003040A1 (fr) | 2000-01-20 |
| US6607603B1 (en) | 2003-08-19 |
| IL140640A0 (en) | 2002-02-10 |
| IL140640A (en) | 2005-11-20 |
| EP0971040A1 (fr) | 2000-01-12 |
| DE69818023T2 (de) | 2004-07-08 |
| DE69818023D1 (de) | 2003-10-16 |
| ZA200100133B (en) | 2001-07-23 |
| DK0971040T3 (da) | 2003-12-08 |
| EP0971040B1 (fr) | 2003-09-10 |
| ATE249524T1 (de) | 2003-09-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20060704 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20060704 |
|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20080829 |
|
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20090526 |
|
| A045 | Written measure of dismissal of application [lapsed due to lack of payment] |
Free format text: JAPANESE INTERMEDIATE CODE: A045 Effective date: 20090924 |