JO3208B1 - عملية من داي هيدرات-نصف هيدرات لإنتاج حمض فسفوري - Google Patents

عملية من داي هيدرات-نصف هيدرات لإنتاج حمض فسفوري

Info

Publication number
JO3208B1
JO3208B1 JOP/2012/0139A JOP20120139A JO3208B1 JO 3208 B1 JO3208 B1 JO 3208B1 JO P20120139 A JOP20120139 A JO P20120139A JO 3208 B1 JO3208 B1 JO 3208B1
Authority
JO
Jordan
Prior art keywords
slurry
content
phosphoric acid
hemihydrate
producing phosphoric
Prior art date
Application number
JOP/2012/0139A
Other languages
English (en)
Inventor
Dorina Fati
Antoine Hoxha
Original Assignee
Prayon Tech
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Prayon Tech filed Critical Prayon Tech
Application granted granted Critical
Publication of JO3208B1 publication Critical patent/JO3208B1/ar

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/22—Preparation by reacting phosphate-containing material with an acid, e.g. wet process
    • C01B25/222—Preparation by reacting phosphate-containing material with an acid, e.g. wet process with sulfuric acid, a mixture of acids mainly consisting of sulfuric acid or a mixture of compounds forming it in situ, e.g. a mixture of sulfur dioxide, water and oxygen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/22—Preparation by reacting phosphate-containing material with an acid, e.g. wet process
    • C01B25/222—Preparation by reacting phosphate-containing material with an acid, e.g. wet process with sulfuric acid, a mixture of acids mainly consisting of sulfuric acid or a mixture of compounds forming it in situ, e.g. a mixture of sulfur dioxide, water and oxygen
    • C01B25/228—Preparation by reacting phosphate-containing material with an acid, e.g. wet process with sulfuric acid, a mixture of acids mainly consisting of sulfuric acid or a mixture of compounds forming it in situ, e.g. a mixture of sulfur dioxide, water and oxygen one form of calcium sulfate being formed and then converted to another form
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/22—Preparation by reacting phosphate-containing material with an acid, e.g. wet process
    • C01B25/222—Preparation by reacting phosphate-containing material with an acid, e.g. wet process with sulfuric acid, a mixture of acids mainly consisting of sulfuric acid or a mixture of compounds forming it in situ, e.g. a mixture of sulfur dioxide, water and oxygen
    • C01B25/228—Preparation by reacting phosphate-containing material with an acid, e.g. wet process with sulfuric acid, a mixture of acids mainly consisting of sulfuric acid or a mixture of compounds forming it in situ, e.g. a mixture of sulfur dioxide, water and oxygen one form of calcium sulfate being formed and then converted to another form
    • C01B25/231—Dihydrate-hemihydrate process

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

طريقة لإنتاج حمض الفسفوريك, يشتمل على تعريض صخور الفوسفات في وسيط مائي بحمض الكبيرتيك, وتشكيل روبة ثنائية الهيدرات معلقة بطور مائي ذات محتوى P2O5 بنسبة تتراوح ما بين 38% الى 50% ومحتوى SO3 خالي لنسبة تقل عن 0.5% لتحويل الروبة الاولى من خلال التسخين بحرارة مع اعداد بلورة كبريتات الكالسيوم المذابة لتسنح الفرصة للحصول على روبة ثانية مجففة جزئيا, و من ثمة فصل الروبة الثانية ما بين انتاج حمض الفسفوريك وكتلة متراصة مجففة جزئيا, حيث تتميز في أنها تشتمل على اضافة مصدر الفلور اثناء الهجوم في الروبة الاولى التي يتراوح المحتوى بنسبة من 1% الى 5% من نسبة الوزن الاجمالي من الفلور مقارنة الى P2O5 التي تحتوي على صخور الفوسفات .
JOP/2012/0139A 2011-06-01 2012-05-31 عملية من داي هيدرات-نصف هيدرات لإنتاج حمض فسفوري JO3208B1 (ar)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/EP2011/059128 WO2012163425A1 (fr) 2011-06-01 2011-06-01 Procede de production d'acide phosphorique du type dihydrate/hemihydrate

Publications (1)

Publication Number Publication Date
JO3208B1 true JO3208B1 (ar) 2018-03-08

Family

ID=44626803

Family Applications (1)

Application Number Title Priority Date Filing Date
JOP/2012/0139A JO3208B1 (ar) 2011-06-01 2012-05-31 عملية من داي هيدرات-نصف هيدرات لإنتاج حمض فسفوري

Country Status (18)

Country Link
US (1) US9371230B2 (ar)
EP (1) EP2714589B1 (ar)
JP (1) JP5798241B2 (ar)
KR (1) KR101770814B1 (ar)
AR (1) AR086618A1 (ar)
BR (1) BR112013030374B1 (ar)
CA (1) CA2837495C (ar)
EA (1) EA025514B1 (ar)
ES (1) ES2562034T3 (ar)
IL (1) IL229664A (ar)
JO (1) JO3208B1 (ar)
MA (1) MA35179B1 (ar)
MX (1) MX339999B (ar)
PL (1) PL2714589T3 (ar)
TN (1) TN2013000497A1 (ar)
TW (1) TWI529122B (ar)
WO (1) WO2012163425A1 (ar)
ZA (1) ZA201309397B (ar)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105776303A (zh) * 2016-01-30 2016-07-20 瓮福（集团）有限责任公司 一种α型半水石膏的生产方法
BE1023754B1 (fr) * 2016-06-23 2017-07-12 Prayon Technologies Procede de production de sulfate de calcium
BE1025894B1 (fr) 2017-08-11 2020-02-21 Prayon Tech Procede d’attaque acide d’une source phosphatee
CN113443614A (zh) * 2021-07-14 2021-09-28 东华工程科技股份有限公司 一种二水-半水湿法浸提磷酸工艺中二水硫酸钙转化α-半水硫酸钙的方法
BE1029993B1 (fr) 2021-12-27 2023-09-25 Prayon Méthode de purification d’au moins une solution aqueuse d’acide phosphorique

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA915883A (en) * 1972-12-05 Pavonet Engelhard Method for manufacturing phosphoric acid and hemihydrate calcium sulphate by the wet process
LU49007A1 (ar) 1965-07-07 1967-01-09
US3523754A (en) * 1966-04-02 1970-08-11 Central Glass Co Ltd Process for preparing phosphoric acil
DE1592287A1 (de) * 1966-08-19 1971-04-15 Piesteritz Stickstoff Verfahren zur Herstellung von Phosphorsaeure
US3984525A (en) 1967-02-01 1976-10-05 Albright & Wilson Limited Manufacture of phosphoric acid
JPS5230959B2 (ar) * 1972-11-25 1977-08-11
GB1520273A (en) * 1974-07-06 1978-08-02 Fisons Ltd Phosphoric acid and gypsum from phosphatic material
JPS5891021A (ja) * 1981-11-27 1983-05-30 Toyo Soda Mfg Co Ltd 湿式リン酸の製造方法
LU84713A1 (fr) 1983-03-25 1984-11-14 Prayon Soc Procede et preparation d'acide phosphorique et de sulfate de calcium hemihydrate alpha
DE3583209D1 (de) * 1984-11-05 1991-07-18 Prayon Dev Sa Kontinuierliches verfahren zur herstellung von phosphorsaeure und von calciumsulfat.
US5093088A (en) * 1987-07-28 1992-03-03 Potash Corporation Of Saskatchewan Apparatus for producing phosphoric acid from phosphate ore
JP2000264612A (ja) * 1999-03-16 2000-09-26 Asahi Chem Ind Co Ltd 湿式燐酸の製造方法
CN1340457A (zh) * 2000-09-01 2002-03-20 山东鲁北企业集团总公司 一种磷酸生产工艺
JP4036426B2 (ja) * 2001-08-23 2008-01-23 下関三井化学株式会社 ろ過性の優れた石膏の製造方法
BE1016065A3 (fr) 2004-06-01 2006-02-07 Prayon Technologies Procede de production d'acide phosphorique.
BE1019055A3 (fr) * 2009-12-02 2012-02-07 Prayon Technologies Procede de production d'acide phosphorique.

Also Published As

Publication number Publication date
ZA201309397B (en) 2015-04-29
CA2837495C (en) 2018-01-09
KR101770814B1 (ko) 2017-08-23
ES2562034T3 (es) 2016-03-02
KR20140035400A (ko) 2014-03-21
MX2013013956A (es) 2014-01-23
EA025514B1 (ru) 2016-12-30
EA201391665A1 (ru) 2014-04-30
US9371230B2 (en) 2016-06-21
TWI529122B (zh) 2016-04-11
TN2013000497A1 (fr) 2015-03-30
JP5798241B2 (ja) 2015-10-21
BR112013030374A2 (pt) 2016-12-13
IL229664A0 (en) 2014-01-30
BR112013030374B1 (pt) 2019-12-31
IL229664A (en) 2016-06-30
WO2012163425A1 (fr) 2012-12-06
PL2714589T3 (pl) 2016-05-31
EP2714589A1 (fr) 2014-04-09
JP2014516908A (ja) 2014-07-17
AR086618A1 (es) 2014-01-08
CA2837495A1 (en) 2012-12-06
EP2714589B1 (fr) 2015-12-16
US20140120020A1 (en) 2014-05-01
MA35179B1 (fr) 2014-06-02
TW201305045A (zh) 2013-02-01
MX339999B (es) 2016-06-20

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