IL87335A0 - Preparation of 1,6-di(n3-cyano-n1-guanidino)hexane - Google Patents
Preparation of 1,6-di(n3-cyano-n1-guanidino)hexaneInfo
- Publication number
- IL87335A0 IL87335A0 IL87335A IL8733588A IL87335A0 IL 87335 A0 IL87335 A0 IL 87335A0 IL 87335 A IL87335 A IL 87335A IL 8733588 A IL8733588 A IL 8733588A IL 87335 A0 IL87335 A0 IL 87335A0
- Authority
- IL
- Israel
- Prior art keywords
- water
- reaction
- guanidino
- cyano
- hexane
- Prior art date
Links
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 title abstract 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 abstract 2
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical class NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- XMVQMBLTFKAIOX-UHFFFAOYSA-N 6-azaniumylhexylazanium;dichloride Chemical compound [Cl-].[Cl-].[NH3+]CCCCCC[NH3+] XMVQMBLTFKAIOX-UHFFFAOYSA-N 0.000 abstract 1
- 230000001476 alcoholic effect Effects 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 238000011065 in-situ storage Methods 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- IXBPPZBJIFNGJJ-UHFFFAOYSA-N sodium;cyanoiminomethylideneazanide Chemical compound [Na+].N#C[N-]C#N IXBPPZBJIFNGJJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C279/00—Derivatives of guanidine, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
- C07C279/28—Derivatives of guanidine, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of guanidine groups bound to cyano groups, e.g. cyanoguanidines, dicyandiamides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Saccharide Compounds (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19873729530 DE3729530A1 (de) | 1987-09-04 | 1987-09-04 | Verfahren zur herstellung von 1,6-di(n(pfeil hoch)3(pfeil hoch)-cyano-n(pfeil hoch)1(pfeil hoch)-guanidino)hexan |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IL87335A0 true IL87335A0 (en) | 1989-01-31 |
Family
ID=6335176
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL87335A IL87335A0 (en) | 1987-09-04 | 1988-08-04 | Preparation of 1,6-di(n3-cyano-n1-guanidino)hexane |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US5041655A (cs) |
| EP (1) | EP0305721B1 (cs) |
| JP (1) | JP2503056B2 (cs) |
| AT (1) | ATE68478T1 (cs) |
| CA (1) | CA1299584C (cs) |
| DE (2) | DE3729530A1 (cs) |
| ES (1) | ES2025252B3 (cs) |
| FI (1) | FI87768C (cs) |
| IL (1) | IL87335A0 (cs) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5178108A (en) * | 1992-05-15 | 1993-01-12 | Ford Motor Company | Camshaft drive for an automotive engine |
| US5620831A (en) * | 1994-04-05 | 1997-04-15 | Taiyo Ink Manufacturing Co., Ltd. | Cyanoguanidine derivatives, and thermosetting or photocurable, thermosetting resin composition using the same |
| US6008316A (en) * | 1998-09-03 | 1999-12-28 | National Starch And Chemical Investment Holding Corporation | Functionalized polyamines |
| WO2005016994A1 (en) * | 2003-08-18 | 2005-02-24 | Sk Chemicals Co., Ltd. | Method for preparing polyalkylenebiguanidine salt |
| EP2066622B1 (de) * | 2006-09-13 | 2013-11-06 | Evonik Degussa GmbH | Verfahren zur herstellung von hexamethylenbiscyanoguanidin und chlorhexidin |
| CN102993056A (zh) * | 2012-12-04 | 2013-03-27 | 甘肃省化工研究院 | 一种双氯苯双胍己烷化合物的制备方法 |
| CN102993057B (zh) * | 2012-12-04 | 2014-09-17 | 甘肃省化工研究院 | 1,6-双氰基胍基己烷的合成方法 |
| ES2939033T3 (es) | 2019-10-28 | 2023-04-18 | Evonik Operations Gmbh | Mezcla de endurecimiento |
| CN111302976A (zh) * | 2020-04-14 | 2020-06-19 | 苏州敬业医药化工有限公司 | 一种洗必泰碱的制备方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB705838A (en) * | 1951-02-05 | 1954-03-17 | Ici Ltd | New bactericidal substances |
| US2686203A (en) * | 1952-03-05 | 1954-08-10 | American Cyanamid Co | Nu-halo-tall-alkyl cyanamides |
| GB995398A (en) * | 1962-11-07 | 1965-06-16 | American Cyanamid Co | Novel hypotensive composition |
| GB1152243A (en) * | 1965-11-26 | 1969-05-14 | Ici Ltd | Process for the Manufacture of Polymeric Diguanides |
| DE1568581C3 (de) * | 1966-09-08 | 1974-08-15 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung substituierter Cyano-Guanidine |
| JPS6045632B2 (ja) * | 1978-03-09 | 1985-10-11 | 三菱化学株式会社 | ω−アミノアルコキシスチルベン類及びその酸付加塩 |
| JPS5533416A (en) * | 1978-08-31 | 1980-03-08 | Sogo Yatsukou Kk | Production of hexamethyene bis-dicyandiamide |
| GB8312663D0 (en) * | 1983-05-09 | 1983-06-15 | Ici Plc | Bisbiguanide compounds |
| US4537746A (en) * | 1983-12-29 | 1985-08-27 | Bausch & Lomb Incorporated | Methods for disinfecting and preserving contact lenses |
| US4792570A (en) * | 1984-04-06 | 1988-12-20 | Syntex (U.S.A.) Inc. | 3- and 4-biphenyloxyaminoalkanes and related compounds as anti-inflammatory and analgetic agents |
| JPS63208566A (ja) * | 1987-02-23 | 1988-08-30 | Mitsui Petrochem Ind Ltd | グアニジン誘導体の製造法 |
-
1987
- 1987-09-04 DE DE19873729530 patent/DE3729530A1/de active Granted
-
1988
- 1988-07-22 DE DE8888111828T patent/DE3865604D1/de not_active Expired - Lifetime
- 1988-07-22 ES ES88111828T patent/ES2025252B3/es not_active Expired - Lifetime
- 1988-07-22 AT AT88111828T patent/ATE68478T1/de active
- 1988-07-22 EP EP88111828A patent/EP0305721B1/de not_active Expired - Lifetime
- 1988-08-04 IL IL87335A patent/IL87335A0/xx unknown
- 1988-08-25 FI FI883935A patent/FI87768C/fi not_active IP Right Cessation
- 1988-09-02 CA CA000576371A patent/CA1299584C/en not_active Expired - Lifetime
- 1988-09-05 JP JP63220592A patent/JP2503056B2/ja not_active Expired - Lifetime
- 1988-09-06 US US07/241,116 patent/US5041655A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| FI883935A0 (fi) | 1988-08-25 |
| JPS6471846A (en) | 1989-03-16 |
| DE3865604D1 (de) | 1991-11-21 |
| CA1299584C (en) | 1992-04-28 |
| EP0305721B1 (de) | 1991-10-16 |
| FI87768B (fi) | 1992-11-13 |
| US5041655A (en) | 1991-08-20 |
| DE3729530C2 (cs) | 1990-07-19 |
| FI883935L (fi) | 1989-03-05 |
| EP0305721A1 (de) | 1989-03-08 |
| DE3729530A1 (de) | 1989-03-16 |
| ES2025252B3 (es) | 1992-03-16 |
| ATE68478T1 (de) | 1991-11-15 |
| FI87768C (fi) | 1993-02-25 |
| JP2503056B2 (ja) | 1996-06-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4564706A (en) | Process for the preparation of propargyl amines | |
| IL87335A0 (en) | Preparation of 1,6-di(n3-cyano-n1-guanidino)hexane | |
| KR100434991B1 (ko) | N-메틸-n'-니트로구아니딘의 제조 방법 | |
| CA2101640C (en) | Pharmaceuticals | |
| US2877220A (en) | Method of preparing lysine | |
| US4230869A (en) | Process for preparing 5-(4-hydroxyphenyl)hydantoin | |
| US4247479A (en) | Process for the manufacture of aromatic amines from α, β-unsaturated cycloaliphatic ketoximes | |
| US3868418A (en) | Novel N-(ortho- and para-nitrobenzoyl)-sulfoximine intermediates and process for their production | |
| US5686625A (en) | Process for the preparation of N-substituted glycine acids or glycine esters and the use of the process for indigo synthesis | |
| FI92400B (fi) | Natriumpuriinien valmistusmenetelmä | |
| US2970159A (en) | Hydrazine derivatives | |
| US4277399A (en) | Process for preparing pyrenzepine | |
| US5688969A (en) | Process for the preparation of thiophene-2-5-dicarboxylic acid and the dichloride thereof | |
| US6133447A (en) | Process for the preparation of substituted pyridines | |
| JPS5758645A (en) | Preparation of carbonate | |
| SU1659400A1 (ru) | Способ получени гидрохлорида N, N-диметил-N-(2,3-дихлорпропил)амина | |
| US5097030A (en) | Process for the preparation of 2-(methylthio)barbituric acid | |
| US4734509A (en) | Preparation of 4(5)-hydroxymethyl-5(4)-methylimidazole | |
| US5210192A (en) | Process for the preparation of 3,7-dialkylxanthines | |
| AU700833B2 (en) | Medicinal products and pure preparations of melarsomine dihydrochloride, process for obtaining them and intermediate products obtained | |
| SU1366517A1 (ru) | Способ получени 3-( @ -D-глюкопиранозил)-4-оксигексагидропиримидин-2-тиона | |
| US4113950A (en) | Process for preparing orotic acid and thioorotic acid | |
| SU461103A1 (ru) | Способ получени мононатриевой соли -( -тиоэтил-2-амино)-тиофосфорной кислоты | |
| JPS6183168A (ja) | ２−メルカプト−４−アミノ−５−ホルミルピリミジンおよびその製法 | |
| JPH01199941A (ja) | システアミン−酸付加塩の製法 |