IL26082A - Skin care products containing phyllozin, isofilosin and their salts - Google Patents
Skin care products containing phyllozin, isofilosin and their saltsInfo
- Publication number
- IL26082A IL26082A IL26082A IL2608266A IL26082A IL 26082 A IL26082 A IL 26082A IL 26082 A IL26082 A IL 26082A IL 2608266 A IL2608266 A IL 2608266A IL 26082 A IL26082 A IL 26082A
- Authority
- IL
- Israel
- Prior art keywords
- pilosine
- isopilosine
- solution
- extracting
- mixture
- Prior art date
Links
- DZOVBAVEJYPSLL-UHFFFAOYSA-N Epiisopilosin Natural products CN1C=NC=C1CC1C(C(O)C=2C=CC=CC=2)C(=O)OC1 DZOVBAVEJYPSLL-UHFFFAOYSA-N 0.000 title claims description 47
- DZOVBAVEJYPSLL-QEJZJMRPSA-N (3s,4r)-3-[(r)-hydroxy(phenyl)methyl]-4-[(3-methylimidazol-4-yl)methyl]oxolan-2-one Chemical compound CN1C=NC=C1C[C@@H]1[C@@H]([C@@H](O)C=2C=CC=CC=2)C(=O)OC1 DZOVBAVEJYPSLL-QEJZJMRPSA-N 0.000 title claims description 24
- DZOVBAVEJYPSLL-CFVMTHIKSA-N Pilosine Chemical compound CN1C=NC=C1C[C@@H]1[C@H]([C@@H](O)C=2C=CC=CC=2)C(=O)OC1 DZOVBAVEJYPSLL-CFVMTHIKSA-N 0.000 title claims description 23
- 238000002360 preparation method Methods 0.000 title claims description 9
- 150000003839 salts Chemical class 0.000 title claims description 5
- 239000000203 mixture Substances 0.000 claims description 15
- QCHFTSOMWOSFHM-WPRPVWTQSA-N (+)-Pilocarpine Chemical compound C1OC(=O)[C@@H](CC)[C@H]1CC1=CN=CN1C QCHFTSOMWOSFHM-WPRPVWTQSA-N 0.000 claims description 11
- QCHFTSOMWOSFHM-UHFFFAOYSA-N SJ000285536 Natural products C1OC(=O)C(CC)C1CC1=CN=CN1C QCHFTSOMWOSFHM-UHFFFAOYSA-N 0.000 claims description 11
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 10
- 239000000284 extract Substances 0.000 claims description 9
- 239000012452 mother liquor Substances 0.000 claims description 9
- 229960001416 pilocarpine Drugs 0.000 claims description 9
- 239000002904 solvent Substances 0.000 claims description 9
- 238000011084 recovery Methods 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 7
- 241001299787 Pilocarpus Species 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- 238000001704 evaporation Methods 0.000 claims description 4
- 239000006188 syrup Substances 0.000 claims description 4
- 235000020357 syrup Nutrition 0.000 claims description 4
- 239000004480 active ingredient Substances 0.000 claims description 3
- 239000011260 aqueous acid Substances 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 2
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 2
- 229910017604 nitric acid Inorganic materials 0.000 claims description 2
- 230000000699 topical effect Effects 0.000 claims description 2
- 239000000243 solution Substances 0.000 description 27
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 9
- 229910021653 sulphate ion Inorganic materials 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
- 206010039792 Seborrhoea Diseases 0.000 description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 208000008742 seborrheic dermatitis Diseases 0.000 description 6
- 210000004761 scalp Anatomy 0.000 description 5
- 201000004681 Psoriasis Diseases 0.000 description 4
- 229930013930 alkaloid Natural products 0.000 description 4
- 239000002585 base Substances 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
- 208000004631 alopecia areata Diseases 0.000 description 3
- 239000004359 castor oil Substances 0.000 description 3
- 235000019438 castor oil Nutrition 0.000 description 3
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 239000002453 shampoo Substances 0.000 description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 201000004384 Alopecia Diseases 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 150000003797 alkaloid derivatives Chemical class 0.000 description 2
- 231100000360 alopecia Toxicity 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 2
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 2
- 229960002139 pilocarpine hydrochloride Drugs 0.000 description 2
- RNAICSBVACLLGM-GNAZCLTHSA-N pilocarpine hydrochloride Chemical compound Cl.C1OC(=O)[C@@H](CC)[C@H]1CC1=CN=CN1C RNAICSBVACLLGM-GNAZCLTHSA-N 0.000 description 2
- 239000002798 polar solvent Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001299781 Pilocarpus pennatifolius Species 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- VHCQVGQULWFQTM-VOTSOKGWSA-N Rubone Chemical compound COC1=CC(OC)=CC(O)=C1C(=O)\C=C\C1=CC(OC)=C(OC)C=C1OC VHCQVGQULWFQTM-VOTSOKGWSA-N 0.000 description 1
- VHCQVGQULWFQTM-UHFFFAOYSA-N Rubone Natural products COC1=CC(OC)=CC(O)=C1C(=O)C=CC1=CC(OC)=C(OC)C=C1OC VHCQVGQULWFQTM-UHFFFAOYSA-N 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 229960002798 cetrimide Drugs 0.000 description 1
- 229960000541 cetyl alcohol Drugs 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000035475 disorder Diseases 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 230000003779 hair growth Effects 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 150000003840 hydrochlorides Chemical class 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- ZUSAAICYKOPBSX-UHFFFAOYSA-N nitric acid;propan-2-one Chemical compound CC(C)=O.O[N+]([O-])=O ZUSAAICYKOPBSX-UHFFFAOYSA-N 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 150000003431 steroids Chemical class 0.000 description 1
- 239000001117 sulphuric acid Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 229940095064 tartrate Drugs 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000820 toxicity test Toxicity 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Epidemiology (AREA)
- Microbiology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Pharmacology & Pharmacy (AREA)
- Alternative & Traditional Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Medical Informatics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
- Medicines Containing Plant Substances (AREA)
Priority Applications (14)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IL26082A IL26082A (en) | 1966-07-03 | 1966-07-03 | Skin care products containing phyllozin, isofilosin and their salts |
| NO168780A NO122073B (fr) | 1966-07-03 | 1967-06-27 | |
| GB29762/67A GB1196454A (en) | 1966-07-03 | 1967-06-28 | Improvements in Dermatological Compositions |
| DE19671695587 DE1695587A1 (de) | 1966-07-03 | 1967-06-29 | Verfahren zur Gewinnung von Pilosin und Pilosin enthaltendes dermatologisches Praeparat |
| SE10078/67*A SE340101B (fr) | 1966-07-03 | 1967-06-30 | |
| NL6709137A NL6709137A (fr) | 1966-07-03 | 1967-06-30 | |
| ES342537A ES342537A1 (es) | 1966-07-03 | 1967-07-01 | Procedimiento para la recuperacion de pilosina e isopilosi-na desde la hojas de jaborandi microphylous. |
| CH939667A CH475280A (fr) | 1966-07-03 | 1967-07-03 | Procédé d'obtention de la pilosine et de l'isopilosine |
| BE700861D BE700861A (fr) | 1966-07-03 | 1967-07-03 | |
| LU54008D LU54008A1 (fr) | 1966-07-03 | 1967-07-03 | |
| DK342867AA DK121377B (da) | 1966-07-03 | 1967-07-03 | Fremgangsmåde til udvinding af pilosin og isopilosin fra en remanens af alokaloidbaser fremstiller ved ekstraktion af bladene af Jaborandi Microphylous og fordampning af ekstraktionsmidlet, eller syreadditionssalte heraf. |
| FR112897A FR6731M (fr) | 1966-07-03 | 1967-07-03 | |
| FR1562788D FR1562788A (fr) | 1966-07-03 | 1967-07-03 | |
| US00020473A US3761595A (en) | 1966-07-03 | 1970-03-25 | Treating skin and scalp conditions |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IL26082A IL26082A (en) | 1966-07-03 | 1966-07-03 | Skin care products containing phyllozin, isofilosin and their salts |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IL26082A true IL26082A (en) | 1970-04-20 |
Family
ID=11043963
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL26082A IL26082A (en) | 1966-07-03 | 1966-07-03 | Skin care products containing phyllozin, isofilosin and their salts |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US3761595A (fr) |
| BE (1) | BE700861A (fr) |
| CH (1) | CH475280A (fr) |
| DE (1) | DE1695587A1 (fr) |
| DK (1) | DK121377B (fr) |
| ES (1) | ES342537A1 (fr) |
| FR (2) | FR1562788A (fr) |
| GB (1) | GB1196454A (fr) |
| IL (1) | IL26082A (fr) |
| LU (1) | LU54008A1 (fr) |
| NL (1) | NL6709137A (fr) |
| NO (1) | NO122073B (fr) |
| SE (1) | SE340101B (fr) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4009392A1 (de) * | 1990-03-23 | 1991-09-26 | Merck Patent Gmbh | Verfahren zur herstellung von pilocarpin aus in vitro-kulturen von pilocarpus |
| WO1996016667A1 (fr) * | 1994-11-29 | 1996-06-06 | Pvp Sociedade Anônima | Compositions cosmetiques comportant des extraits de pilocarpus jaborandi et d'aloes ordinaire |
-
1966
- 1966-07-03 IL IL26082A patent/IL26082A/en unknown
-
1967
- 1967-06-27 NO NO168780A patent/NO122073B/no unknown
- 1967-06-28 GB GB29762/67A patent/GB1196454A/en not_active Expired
- 1967-06-29 DE DE19671695587 patent/DE1695587A1/de active Pending
- 1967-06-30 SE SE10078/67*A patent/SE340101B/xx unknown
- 1967-06-30 NL NL6709137A patent/NL6709137A/xx unknown
- 1967-07-01 ES ES342537A patent/ES342537A1/es not_active Expired
- 1967-07-03 FR FR1562788D patent/FR1562788A/fr not_active Expired
- 1967-07-03 CH CH939667A patent/CH475280A/fr not_active IP Right Cessation
- 1967-07-03 BE BE700861D patent/BE700861A/xx unknown
- 1967-07-03 FR FR112897A patent/FR6731M/fr not_active Expired
- 1967-07-03 LU LU54008D patent/LU54008A1/xx unknown
- 1967-07-03 DK DK342867AA patent/DK121377B/da unknown
-
1970
- 1970-03-25 US US00020473A patent/US3761595A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| FR6731M (fr) | 1969-02-24 |
| SE340101B (fr) | 1971-11-08 |
| FR1562788A (fr) | 1969-04-11 |
| CH475280A (fr) | 1969-07-15 |
| NL6709137A (fr) | 1968-01-04 |
| DE1695587A1 (de) | 1971-02-11 |
| ES342537A1 (es) | 1968-10-16 |
| DK121377B (da) | 1971-10-11 |
| BE700861A (fr) | 1968-01-03 |
| US3761595A (en) | 1973-09-25 |
| NO122073B (fr) | 1971-05-18 |
| GB1196454A (en) | 1970-06-24 |
| LU54008A1 (fr) | 1968-03-12 |
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