IL124739A - Process for the preparation of aqueous solutions of free hydroxylamine - Google Patents
Process for the preparation of aqueous solutions of free hydroxylamineInfo
- Publication number
- IL124739A IL124739A IL12473996A IL12473996A IL124739A IL 124739 A IL124739 A IL 124739A IL 12473996 A IL12473996 A IL 12473996A IL 12473996 A IL12473996 A IL 12473996A IL 124739 A IL124739 A IL 124739A
- Authority
- IL
- Israel
- Prior art keywords
- hydroxylamine
- column
- solution
- salt
- stripping
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1445—Preparation of hydoxylamine from its salts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/146—Multiple effect distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/38—Steam distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1463—Concentration
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1472—Separation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Compounds Of Unknown Constitution (AREA)
- Seasonings (AREA)
- Gas Separation By Absorption (AREA)
- Disintegrating Or Milling (AREA)
- Extraction Or Liquid Replacement (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19547758 | 1995-12-20 | ||
US08/688,281 US5837107A (en) | 1995-12-20 | 1996-07-29 | Process for production of aqueous solutions of free hydroxylamine |
PCT/EP1996/005773 WO1997022551A1 (de) | 1995-12-20 | 1996-12-20 | Verfahren zur herstellung von wässrigen lösungen von freiem hydroxylamin |
Publications (2)
Publication Number | Publication Date |
---|---|
IL124739A0 IL124739A0 (en) | 1999-01-26 |
IL124739A true IL124739A (en) | 2001-06-14 |
Family
ID=26021480
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IL12473796A IL124737A (en) | 1995-12-20 | 1996-12-20 | Process for separating a fraction containing middle boilers from a mixture of low, middle and high boilers |
IL12473996A IL124739A (en) | 1995-12-20 | 1996-12-20 | Process for the preparation of aqueous solutions of free hydroxylamine |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IL12473796A IL124737A (en) | 1995-12-20 | 1996-12-20 | Process for separating a fraction containing middle boilers from a mixture of low, middle and high boilers |
Country Status (16)
Country | Link |
---|---|
EP (2) | EP0868398B1 (es) |
JP (2) | JP2000505033A (es) |
CN (2) | CN1104376C (es) |
AT (1) | ATE222565T1 (es) |
AU (2) | AU704998B2 (es) |
BR (2) | BR9612073A (es) |
CA (2) | CA2239791C (es) |
DE (2) | DE59609239D1 (es) |
DK (1) | DK0868399T3 (es) |
ES (2) | ES2181933T3 (es) |
HR (1) | HRP960601B1 (es) |
IL (2) | IL124737A (es) |
NO (2) | NO319309B1 (es) |
PT (1) | PT868399E (es) |
TR (2) | TR199801163T2 (es) |
WO (2) | WO1997022551A1 (es) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19725851A1 (de) * | 1997-06-18 | 1998-12-24 | Basf Ag | Verfahren zur Herstellung hochreiner, wässriger Hydroxylaminlösungen |
US5788946A (en) * | 1997-07-16 | 1998-08-04 | Ashland Inc. | Purification of hydroxylamine |
DE19733681A1 (de) | 1997-08-04 | 1999-02-11 | Basf Ag | Verfahren zur Herstellung einer wäßrigen Lösung von freiem Hydroxylamin |
DE19806578A1 (de) * | 1998-02-17 | 1999-08-19 | Basf Ag | Verfahren zur Herstellung wäßriger, im wesentlichen metallionenfreier Hydroxylaminlösungen |
US6235162B1 (en) | 1998-05-28 | 2001-05-22 | Sachem, Inc. | Ultrapure hydroxylamine compound solutions and process of making same |
DE19936594A1 (de) * | 1999-08-04 | 2001-02-08 | Basf Ag | Verfahren zur Herstellung von hochreinen stabilisierten Hydroxylaminlösungen |
DE10004818A1 (de) * | 2000-02-04 | 2001-08-09 | Basf Ag | Verfahren zum Recycling hydroxylaminhaltiger Stripperlösungen |
JP3503115B2 (ja) * | 2000-06-27 | 2004-03-02 | 東レ・ファインケミカル株式会社 | フリーヒドロキシルアミン水溶液の製造方法 |
DE10037774A1 (de) * | 2000-08-03 | 2002-02-14 | Bayer Ag | Verfahren und Vorrichtung zur Gewinnung organischer Substanzen aus einem diese Substanzen enthaltenden Gasgemisch |
DE10131787A1 (de) * | 2001-07-04 | 2003-01-16 | Basf Ag | Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung |
DE10134389A1 (de) * | 2001-07-04 | 2003-01-16 | Basf Ag | Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung |
DE10131788A1 (de) * | 2001-07-04 | 2003-01-16 | Basf Ag | Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung |
DE10314492B4 (de) * | 2003-03-27 | 2008-10-16 | Domo Caproleuna Gmbh | Verfahren zur Herstellung einer wässrigen Lösung von Hydroxylamin |
JP4578885B2 (ja) * | 2003-08-13 | 2010-11-10 | 昭和電工株式会社 | ヒドロキシルアミンの製造方法 |
TW200508176A (en) * | 2003-08-13 | 2005-03-01 | Showa Denko Kk | Process for producing hydroxylamine |
US7491846B2 (en) | 2003-08-13 | 2009-02-17 | Showa Denko K.K. | Process for producing hydroxylamine |
FR2860223B1 (fr) * | 2003-09-26 | 2005-12-16 | Jean Pierre Schirmann | Procede de fabrication de solutions aqueuses d'hydroxylamine base |
US7396519B2 (en) | 2004-01-26 | 2008-07-08 | San Fu Chemical Company, Ltd. | Preparation of a high purity and high concentration hydroxylamine free base |
JP2005239702A (ja) * | 2004-01-28 | 2005-09-08 | Showa Denko Kk | ヒドロキシルアミンの製造方法 |
JP2006056742A (ja) * | 2004-08-19 | 2006-03-02 | Hosoya Fireworks Co Ltd | 硝酸ヒドロキシルアミン水溶液の製造方法 |
JP4578988B2 (ja) * | 2005-01-21 | 2010-11-10 | 昭和電工株式会社 | ヒドロキシルアミンの製造方法 |
JP2006219343A (ja) * | 2005-02-10 | 2006-08-24 | Showa Denko Kk | ヒドロキシルアミンの製造方法 |
JP4578999B2 (ja) * | 2005-02-10 | 2010-11-10 | 昭和電工株式会社 | ヒドロキシルアミンの製造方法 |
JP4578998B2 (ja) * | 2005-02-10 | 2010-11-10 | 昭和電工株式会社 | ヒドロキシルアミンの製造方法 |
DE102005032430A1 (de) * | 2005-07-12 | 2007-01-25 | Bayer Materialscience Ag | Verfahren zur Herstellung von Toluylendiamin |
WO2017204935A1 (en) | 2016-05-26 | 2017-11-30 | Exxonmobil Chemical Patents Inc. | Production of cyclic imides suitable for oxidation catalysis |
WO2017204936A1 (en) | 2016-05-26 | 2017-11-30 | Exxonmobil Chemical Patents Inc. | Production of cyclic imides suitable for oxidation catalysis |
US10584096B2 (en) | 2016-10-18 | 2020-03-10 | Exxonmobil Chemical Patents Inc. | Cyclic imide slurry compositions |
CN108946741B (zh) * | 2017-05-17 | 2020-05-12 | 新特能源股份有限公司 | 多晶硅冷氢化工艺中的含硅高沸物的回收工艺方法及冷氢化工艺 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4111759A (en) * | 1976-07-08 | 1978-09-05 | United States Steel Corporation | Process for separating ammonia and acid gases from waste waters containing fixed ammonia salts |
JPS597313B2 (ja) * | 1980-02-08 | 1984-02-17 | チツソエンジニアリング株式会社 | アルコ−ルの蒸溜装置 |
DE3302525A1 (de) * | 1983-01-26 | 1984-07-26 | Basf Ag, 6700 Ludwigshafen | Destillationskolonne zur destillativen zerlegung eines aus mehreren fraktionen bestehenden zulaufproduktes |
DE3528463A1 (de) * | 1985-08-08 | 1987-02-19 | Basf Ag | Verfahren zur herstellung von waessrigen loesungen von freiem hydroxylamin |
DE3814255A1 (de) * | 1988-04-27 | 1989-11-09 | Metallgesellschaft Ag | Vorrichtung zum desodorieren von organischen fluessigkeiten |
US5266290A (en) * | 1992-07-10 | 1993-11-30 | Thiokol Corporation | Process for making high purity hydroxylammonium nitrate |
DE4324410C1 (de) * | 1993-07-21 | 1994-08-04 | Enviro Consult Ingenieurgesell | Verfahren zum Entfernen von Ammonium aus dem Zentratwasser einer biologischen Abwasserreinigungsanlage |
US5385646A (en) * | 1993-09-03 | 1995-01-31 | Farmland Industries, Inc. | Method of treating chemical process effluent |
-
1996
- 1996-12-19 HR HR960601A patent/HRP960601B1/xx not_active IP Right Cessation
- 1996-12-20 AU AU13039/97A patent/AU704998B2/en not_active Expired
- 1996-12-20 ES ES96944616T patent/ES2181933T3/es not_active Expired - Lifetime
- 1996-12-20 IL IL12473796A patent/IL124737A/en not_active IP Right Cessation
- 1996-12-20 WO PCT/EP1996/005773 patent/WO1997022551A1/de active IP Right Grant
- 1996-12-20 ES ES96944615T patent/ES2177828T3/es not_active Expired - Lifetime
- 1996-12-20 IL IL12473996A patent/IL124739A/en not_active IP Right Cessation
- 1996-12-20 PT PT96944616T patent/PT868399E/pt unknown
- 1996-12-20 DK DK96944616T patent/DK0868399T3/da active
- 1996-12-20 CN CN96199143A patent/CN1104376C/zh not_active Expired - Lifetime
- 1996-12-20 BR BR9612073A patent/BR9612073A/pt not_active IP Right Cessation
- 1996-12-20 AT AT96944616T patent/ATE222565T1/de active
- 1996-12-20 TR TR1998/01163T patent/TR199801163T2/xx unknown
- 1996-12-20 EP EP96944615A patent/EP0868398B1/de not_active Expired - Lifetime
- 1996-12-20 DE DE59609239T patent/DE59609239D1/de not_active Expired - Lifetime
- 1996-12-20 EP EP96944616A patent/EP0868399B1/de not_active Expired - Lifetime
- 1996-12-20 CN CN96199954A patent/CN1102531C/zh not_active Expired - Lifetime
- 1996-12-20 DE DE59609580T patent/DE59609580D1/de not_active Expired - Lifetime
- 1996-12-20 CA CA002239791A patent/CA2239791C/en not_active Expired - Lifetime
- 1996-12-20 AU AU13040/97A patent/AU707648B2/en not_active Expired
- 1996-12-20 BR BR9612053A patent/BR9612053A/pt not_active IP Right Cessation
- 1996-12-20 TR TR1998/01154T patent/TR199801154T2/xx unknown
- 1996-12-20 JP JP9522524A patent/JP2000505033A/ja active Pending
- 1996-12-20 WO PCT/EP1996/005772 patent/WO1997022550A1/de active IP Right Grant
- 1996-12-20 CA CA002239253A patent/CA2239253C/en not_active Expired - Lifetime
- 1996-12-20 JP JP52252397A patent/JP4376969B2/ja not_active Expired - Lifetime
-
1998
- 1998-06-19 NO NO19982847A patent/NO319309B1/no not_active IP Right Cessation
- 1998-06-19 NO NO19982849A patent/NO322631B1/no not_active IP Right Cessation
Also Published As
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Legal Events
Date | Code | Title | Description |
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FF | Patent granted | ||
KB | Patent renewed | ||
KB | Patent renewed | ||
KB | Patent renewed | ||
KB | Patent renewed | ||
KB | Patent renewed | ||
EXP | Patent expired |