CA2239791A1 - Separation of middle boilers from a mixture of low, middle and high boilers - Google Patents
Separation of middle boilers from a mixture of low, middle and high boilersInfo
- Publication number
- CA2239791A1 CA2239791A1 CA002239791A CA2239791A CA2239791A1 CA 2239791 A1 CA2239791 A1 CA 2239791A1 CA 002239791 A CA002239791 A CA 002239791A CA 2239791 A CA2239791 A CA 2239791A CA 2239791 A1 CA2239791 A1 CA 2239791A1
- Authority
- CA
- Canada
- Prior art keywords
- low
- boilers
- mixture
- separation
- boiling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 title abstract 3
- 238000000926 separation method Methods 0.000 title 1
- 238000009835 boiling Methods 0.000 abstract 6
- 239000000126 substance Substances 0.000 abstract 4
- 238000004821 distillation Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1445—Preparation of hydoxylamine from its salts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/146—Multiple effect distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/38—Steam distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1463—Concentration
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1472—Separation
Abstract
A process is disclosed for separating a fraction which contains low and medium boiling substances from a mixture of low, medium and high boiling substances. The mixture is treated at the bottom of the distillation column with low boiling vapour, enriching the low boiling vapour with medium boiling substances which can then be extracted at the temperature level of the low boiling substance.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19547758.8 | 1995-12-20 | ||
DE19547758 | 1995-12-20 | ||
US08/688,281 | 1996-07-29 | ||
US08/688,281 US5837107A (en) | 1995-12-20 | 1996-07-29 | Process for production of aqueous solutions of free hydroxylamine |
PCT/EP1996/005772 WO1997022550A1 (en) | 1995-12-20 | 1996-12-20 | Process for separating medium boiling substances from a mixture of low, medium and high boiling substances |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2239791A1 true CA2239791A1 (en) | 1997-06-26 |
CA2239791C CA2239791C (en) | 2006-01-31 |
Family
ID=26021480
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002239253A Expired - Lifetime CA2239253C (en) | 1995-12-20 | 1996-12-20 | Preparation of aqueous solutions of free hydroxylamine |
CA002239791A Expired - Lifetime CA2239791C (en) | 1995-12-20 | 1996-12-20 | Separation of middle boilers from a mixture of low, middle and high boilers |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002239253A Expired - Lifetime CA2239253C (en) | 1995-12-20 | 1996-12-20 | Preparation of aqueous solutions of free hydroxylamine |
Country Status (16)
Country | Link |
---|---|
EP (2) | EP0868399B1 (en) |
JP (2) | JP4376969B2 (en) |
CN (2) | CN1104376C (en) |
AT (1) | ATE222565T1 (en) |
AU (2) | AU704998B2 (en) |
BR (2) | BR9612073A (en) |
CA (2) | CA2239253C (en) |
DE (2) | DE59609580D1 (en) |
DK (1) | DK0868399T3 (en) |
ES (2) | ES2181933T3 (en) |
HR (1) | HRP960601B1 (en) |
IL (2) | IL124739A (en) |
NO (2) | NO319309B1 (en) |
PT (1) | PT868399E (en) |
TR (2) | TR199801154T2 (en) |
WO (2) | WO1997022551A1 (en) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19725851A1 (en) * | 1997-06-18 | 1998-12-24 | Basf Ag | Process for the preparation of high-purity, aqueous hydroxylamine solutions |
US5788946A (en) * | 1997-07-16 | 1998-08-04 | Ashland Inc. | Purification of hydroxylamine |
DE19733681A1 (en) | 1997-08-04 | 1999-02-11 | Basf Ag | Process for the preparation of an aqueous solution of free hydroxylamine |
DE19806578A1 (en) | 1998-02-17 | 1999-08-19 | Basf Ag | Production of aqueous hydroxylamine solution containing essentially no metal ions, used in electronics industry |
US6235162B1 (en) | 1998-05-28 | 2001-05-22 | Sachem, Inc. | Ultrapure hydroxylamine compound solutions and process of making same |
DE19936594A1 (en) | 1999-08-04 | 2001-02-08 | Basf Ag | Process for the preparation of high-purity stabilized hydroxylamine solutions |
DE10004818A1 (en) * | 2000-02-04 | 2001-08-09 | Basf Ag | Process for recycling stripper solutions containing hydroxylamine |
JP3503115B2 (en) * | 2000-06-27 | 2004-03-02 | 東レ・ファインケミカル株式会社 | Method for producing free hydroxylamine aqueous solution |
DE10037774A1 (en) * | 2000-08-03 | 2002-02-14 | Bayer Ag | Method and device for obtaining organic substances from a gas mixture containing these substances |
DE10131787A1 (en) | 2001-07-04 | 2003-01-16 | Basf Ag | Process for the preparation of a salt-free, aqueous hydroxylamine solution |
DE10131788A1 (en) * | 2001-07-04 | 2003-01-16 | Basf Ag | Process for the preparation of a salt-free, aqueous hydroxylamine solution |
DE10134389A1 (en) | 2001-07-04 | 2003-01-16 | Basf Ag | Process for the preparation of a salt-free, aqueous hydroxylamine solution |
DE10314492B4 (en) * | 2003-03-27 | 2008-10-16 | Domo Caproleuna Gmbh | Process for the preparation of an aqueous solution of hydroxylamine |
JP4578885B2 (en) * | 2003-08-13 | 2010-11-10 | 昭和電工株式会社 | Method for producing hydroxylamine |
US7491846B2 (en) | 2003-08-13 | 2009-02-17 | Showa Denko K.K. | Process for producing hydroxylamine |
TW200508176A (en) * | 2003-08-13 | 2005-03-01 | Showa Denko Kk | Process for producing hydroxylamine |
FR2860223B1 (en) * | 2003-09-26 | 2005-12-16 | Jean Pierre Schirmann | PROCESS FOR PRODUCING AQUEOUS HYDROXYLAMINE BASE SOLUTIONS |
US7396519B2 (en) | 2004-01-26 | 2008-07-08 | San Fu Chemical Company, Ltd. | Preparation of a high purity and high concentration hydroxylamine free base |
JP2005239702A (en) * | 2004-01-28 | 2005-09-08 | Showa Denko Kk | Method for producing hydroxylamine |
JP2006056742A (en) * | 2004-08-19 | 2006-03-02 | Hosoya Fireworks Co Ltd | Method for producing aqueous solution of hydroxylamine nitrate |
JP4578988B2 (en) * | 2005-01-21 | 2010-11-10 | 昭和電工株式会社 | Method for producing hydroxylamine |
JP4578998B2 (en) * | 2005-02-10 | 2010-11-10 | 昭和電工株式会社 | Method for producing hydroxylamine |
JP4578999B2 (en) * | 2005-02-10 | 2010-11-10 | 昭和電工株式会社 | Method for producing hydroxylamine |
JP2006219343A (en) * | 2005-02-10 | 2006-08-24 | Showa Denko Kk | Method for producing hydroxylamine |
DE102005032430A1 (en) * | 2005-07-12 | 2007-01-25 | Bayer Materialscience Ag | Process for the preparation of toluenediamine |
US11161812B2 (en) | 2016-05-26 | 2021-11-02 | Exxonmobil Chemical Patents Inc. | Production of cyclic imides suitable for oxidation catalysis |
US11014883B2 (en) | 2016-05-26 | 2021-05-25 | Exxonmobil Chemical Patents Inc. | Production of cyclic imides suitable for oxidation catalysis |
US10584096B2 (en) | 2016-10-18 | 2020-03-10 | Exxonmobil Chemical Patents Inc. | Cyclic imide slurry compositions |
CN108946741B (en) * | 2017-05-17 | 2020-05-12 | 新特能源股份有限公司 | Process method for recovering silicon-containing high-boiling-point substance in polycrystalline silicon cold hydrogenation process and cold hydrogenation process |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4111759A (en) * | 1976-07-08 | 1978-09-05 | United States Steel Corporation | Process for separating ammonia and acid gases from waste waters containing fixed ammonia salts |
JPS597313B2 (en) * | 1980-02-08 | 1984-02-17 | チツソエンジニアリング株式会社 | Alcohol distillation equipment |
DE3302525A1 (en) * | 1983-01-26 | 1984-07-26 | Basf Ag, 6700 Ludwigshafen | DISTILLATION COLUMN FOR THE DISTILLATIVE DISASSEMBLY OF AN INLET PRODUCT MULTIPLE FRACTIONS |
DE3528463A1 (en) * | 1985-08-08 | 1987-02-19 | Basf Ag | Process for the preparation of aqueous solutions of free hydroxylamine |
DE3814255A1 (en) * | 1988-04-27 | 1989-11-09 | Metallgesellschaft Ag | DEVICE FOR DESODORING ORGANIC LIQUIDS |
US5266290A (en) * | 1992-07-10 | 1993-11-30 | Thiokol Corporation | Process for making high purity hydroxylammonium nitrate |
DE4324410C1 (en) * | 1993-07-21 | 1994-08-04 | Enviro Consult Ingenieurgesell | Removing ammonium from process water in effluent water treatment units |
US5385646A (en) * | 1993-09-03 | 1995-01-31 | Farmland Industries, Inc. | Method of treating chemical process effluent |
-
1996
- 1996-12-19 HR HR960601A patent/HRP960601B1/en not_active IP Right Cessation
- 1996-12-20 DE DE59609580T patent/DE59609580D1/en not_active Expired - Lifetime
- 1996-12-20 WO PCT/EP1996/005773 patent/WO1997022551A1/en active IP Right Grant
- 1996-12-20 CN CN96199143A patent/CN1104376C/en not_active Expired - Lifetime
- 1996-12-20 BR BR9612073A patent/BR9612073A/en not_active IP Right Cessation
- 1996-12-20 EP EP96944616A patent/EP0868399B1/en not_active Expired - Lifetime
- 1996-12-20 JP JP52252397A patent/JP4376969B2/en not_active Expired - Lifetime
- 1996-12-20 TR TR1998/01154T patent/TR199801154T2/en unknown
- 1996-12-20 ES ES96944616T patent/ES2181933T3/en not_active Expired - Lifetime
- 1996-12-20 WO PCT/EP1996/005772 patent/WO1997022550A1/en active IP Right Grant
- 1996-12-20 AU AU13039/97A patent/AU704998B2/en not_active Expired
- 1996-12-20 AT AT96944616T patent/ATE222565T1/en active
- 1996-12-20 CA CA002239253A patent/CA2239253C/en not_active Expired - Lifetime
- 1996-12-20 BR BR9612053A patent/BR9612053A/en not_active IP Right Cessation
- 1996-12-20 IL IL12473996A patent/IL124739A/en not_active IP Right Cessation
- 1996-12-20 CA CA002239791A patent/CA2239791C/en not_active Expired - Lifetime
- 1996-12-20 TR TR1998/01163T patent/TR199801163T2/en unknown
- 1996-12-20 CN CN96199954A patent/CN1102531C/en not_active Expired - Lifetime
- 1996-12-20 EP EP96944615A patent/EP0868398B1/en not_active Expired - Lifetime
- 1996-12-20 DE DE59609239T patent/DE59609239D1/en not_active Expired - Lifetime
- 1996-12-20 DK DK96944616T patent/DK0868399T3/en active
- 1996-12-20 PT PT96944616T patent/PT868399E/en unknown
- 1996-12-20 JP JP9522524A patent/JP2000505033A/en active Pending
- 1996-12-20 IL IL12473796A patent/IL124737A/en not_active IP Right Cessation
- 1996-12-20 ES ES96944615T patent/ES2177828T3/en not_active Expired - Lifetime
- 1996-12-20 AU AU13040/97A patent/AU707648B2/en not_active Expired
-
1998
- 1998-06-19 NO NO19982847A patent/NO319309B1/en not_active IP Right Cessation
- 1998-06-19 NO NO19982849A patent/NO322631B1/en not_active IP Right Cessation
Also Published As
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EEER | Examination request | ||
MKEX | Expiry |
Effective date: 20161220 |