IL110861A - Process for preparing pure ethylediaminetetra (methylenphosphonic acid) - Google Patents

Process for preparing pure ethylediaminetetra (methylenphosphonic acid)

Info

Publication number
IL110861A
IL110861A IL11086190A IL11086190A IL110861A IL 110861 A IL110861 A IL 110861A IL 11086190 A IL11086190 A IL 11086190A IL 11086190 A IL11086190 A IL 11086190A IL 110861 A IL110861 A IL 110861A
Authority
IL
Israel
Prior art keywords
ethylediaminetetra
preparing pure
methylenphosphonic acid
methylenphosphonic
acid
Prior art date
Application number
IL11086190A
Other languages
English (en)
Inventor
Joseph R Garlich
Simon Jaime
Tipton T Masterson
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Publication of IL110861A publication Critical patent/IL110861A/xx

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/44—Amides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6524—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having four or more nitrogen atoms as the only ring hetero atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/025—Purification; Separation; Stabilisation; Desodorisation of organo-phosphorus compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3817—Acids containing the structure (RX)2P(=X)-alk-N...P (X = O, S, Se)

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
IL11086190A 1989-08-04 1990-07-16 Process for preparing pure ethylediaminetetra (methylenphosphonic acid) IL110861A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/389,441 US4937333A (en) 1989-08-04 1989-08-04 Method for purifying aminomethylenephosphonic acids for pharmaceutical use
IL9509490A IL95094A (en) 1989-08-04 1990-07-16 A process for the purification of aminophosphonic amino acids

Publications (1)

Publication Number Publication Date
IL110861A true IL110861A (en) 1999-07-14

Family

ID=23538280

Family Applications (3)

Application Number Title Priority Date Filing Date
IL11086190A IL110861A (en) 1989-08-04 1990-07-16 Process for preparing pure ethylediaminetetra (methylenphosphonic acid)
IL9509490A IL95094A (en) 1989-08-04 1990-07-16 A process for the purification of aminophosphonic amino acids
IL11086194A IL110861A0 (en) 1989-08-04 1994-09-05 Process for preparing pure ethylenediaminetetra (methylenephosphonic acid)

Family Applications After (2)

Application Number Title Priority Date Filing Date
IL9509490A IL95094A (en) 1989-08-04 1990-07-16 A process for the purification of aminophosphonic amino acids
IL11086194A IL110861A0 (en) 1989-08-04 1994-09-05 Process for preparing pure ethylenediaminetetra (methylenephosphonic acid)

Country Status (38)

Country Link
US (1) US4937333A (de)
EP (1) EP0411941B1 (de)
JP (1) JP2922263B2 (de)
KR (2) KR0178779B1 (de)
CN (2) CN1024196C (de)
AP (1) AP163A (de)
AT (1) ATE140459T1 (de)
AU (1) AU634267B2 (de)
BG (1) BG60519B1 (de)
BR (2) BR9003694A (de)
CA (1) CA2020950C (de)
CZ (1) CZ290556B6 (de)
DD (1) DD297414A5 (de)
DE (1) DE69027818T2 (de)
DK (1) DK0411941T3 (de)
DZ (1) DZ1436A1 (de)
EG (1) EG19250A (de)
ES (1) ES2090105T3 (de)
FI (1) FI105033B (de)
GR (1) GR3020932T3 (de)
HK (1) HK1007558A1 (de)
HU (1) HU205128B (de)
IE (1) IE902812A1 (de)
IL (3) IL110861A (de)
LV (1) LV10718B (de)
MA (1) MA21922A1 (de)
NO (2) NO178196C (de)
NZ (2) NZ247888A (de)
OA (1) OA09300A (de)
PH (1) PH26901A (de)
PL (2) PL164908B1 (de)
PT (1) PT94188B (de)
RO (1) RO105967B1 (de)
RU (1) RU1838321C (de)
SA (1) SA90110175B1 (de)
SK (1) SK279107B6 (de)
YU (1) YU47368B (de)
ZA (1) ZA905564B (de)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4937333A (en) * 1989-08-04 1990-06-26 The Dow Chemical Company Method for purifying aminomethylenephosphonic acids for pharmaceutical use
MC2260A1 (fr) * 1990-06-18 1993-04-26 Dow Chemical Co Formulations de produits radiopharmaceutiques,leur methode d'administration et leur procede de preparation
EP0494603A3 (en) * 1991-01-10 1993-10-20 Hoechst Ag Process for extractive separation of phospho- and sulphobetaines from acidic reaction solutions
US5410043A (en) * 1991-12-06 1995-04-25 Schering Aktiengesellschaft Process for the production of mono-N-substituted tetraaza macrocycles
US5320829A (en) * 1991-12-10 1994-06-14 The Dow Chemical Company Oral compositions for inhibiting plaque formation
DE4218744C2 (de) * 1992-06-04 1997-11-06 Schering Ag Verfahren zur Herstellung von N-ß-Hxdroxyalkyl-tri-N-carboxylalkyl-1,4,7,10-tetraazacyclododecan- und N-ß-Hydroxyalkyl-tri-N-carboxyalkyl-1,4,8,11-tetraazacyclotetradecan-Derivaten und deren Metallkomplexe
US5495042A (en) * 1993-11-04 1996-02-27 Cytogen Corporation Non-alkaline purification of aminophosphonic acids
EP1191948A2 (de) * 1999-06-11 2002-04-03 Neorx Corporation Hochdosierte radionuklide komplexe zur knochenmark-unterdrückung
US7094885B2 (en) * 1999-07-11 2006-08-22 Neorx Corporation Skeletal-targeted radiation to treat bone-associated pathologies
AU1092601A (en) * 1999-10-18 2001-04-30 Dow Global Technologies Inc. Aminoalkylenephosphonates for treatment of bone disorders
US6794371B1 (en) * 1999-10-18 2004-09-21 The Dow Chemical Company Aminoalkylenephosphonates for treatment of bone disorders
WO2002062398A2 (en) 2001-01-08 2002-08-15 Neorx Corporation Radioactively labelled conjugates of phosphonates
KR101108310B1 (ko) * 2002-12-27 2012-01-25 스미또모 가가꾸 가부시키가이샤 결정화 방법 및 결정화 장치
EP1778699A4 (de) * 2004-08-10 2009-02-25 Dow Global Technologies Inc Targeting von chelanten und chelaten
CN101381377B (zh) * 2008-10-23 2011-05-04 山东省泰和水处理有限公司 一种适用于电子级固体己二胺四亚甲基膦酸的制备工艺
JP5581832B2 (ja) * 2010-06-11 2014-09-03 三菱瓦斯化学株式会社 高純度アミノメチレンホスホン酸の製造方法
CN103724373A (zh) * 2014-01-02 2014-04-16 山东省泰和水处理有限公司 多聚甲醛生产氨基三亚甲基膦酸的方法
TR201905374T4 (tr) 2014-06-02 2019-05-21 Zschimmer & Schwarz Mohsdorf Gmbh & Co Kg Kristalin dtpmp üretilmesine yönelik yöntem.
DE102014210378B4 (de) * 2014-06-02 2018-10-04 Zschimmer & Schwarz Mohsdorf GmbH &Co.KG. Verfahren zur Herstellung hochreiner Aminoalkylenphosphonsäuren
CN113263580A (zh) * 2021-04-23 2021-08-17 广东工业大学 一种多功能床头柜制造设备

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2599807A (en) * 1950-06-01 1952-06-10 Frederick C Bersworth Alkylene polyamine methylene phosphonic acids
NL285361A (de) * 1961-11-13 1900-01-01
US3738937A (en) * 1970-05-08 1973-06-12 Textilana Corp Polyalkylene polyamino polykis methylene phosphonic acids and salts thereof and methods for producing same
NL7903500A (nl) * 1979-05-04 1980-11-06 Philips Nv Verbrandingsflitslamp en flitsinrichting voorzien van verscheidene verbrandingsflitslampen.
JPS5775990A (en) * 1980-10-27 1982-05-12 Mitsubishi Gas Chem Co Inc Preparation of n,n,n',n'-tetra(phosphonomethyl) diaminoalkane
EP0225409A1 (de) * 1985-12-02 1987-06-16 The Dow Chemical Company Organoaminophosphonische Säurekomplexe für die Behandlung von Kalktumoren
US4937333A (en) * 1989-08-04 1990-06-26 The Dow Chemical Company Method for purifying aminomethylenephosphonic acids for pharmaceutical use
GB8903023D0 (en) * 1989-02-10 1989-03-30 Parker David Chemical compounds
DE3911816A1 (de) * 1989-04-11 1990-10-25 Hoechst Ag Substituierte 1,4,7,10-tetraazacyclotridecane, verfahren zu deren herstellung sowie verwendung derselben zur markierung von substanzen mit radionukliden

Also Published As

Publication number Publication date
NZ247888A (en) 1994-07-26
PL286349A1 (en) 1991-05-20
LV10718A (lv) 1995-06-20
JPH0366697A (ja) 1991-03-22
BG60519B1 (bg) 1995-07-28
ATE140459T1 (de) 1996-08-15
AU6023790A (en) 1991-02-07
CN1031191C (zh) 1996-03-06
KR0178779B1 (ko) 1999-05-15
AP9000202A0 (en) 1990-10-31
ZA905564B (en) 1992-03-25
FI903864A0 (fi) 1990-08-03
GR3020932T3 (en) 1996-12-31
NZ234464A (en) 1994-06-27
DE69027818D1 (de) 1996-08-22
NO903419L (no) 1991-02-05
IL95094A (en) 1995-05-26
SK379690A3 (en) 1998-06-03
EP0411941B1 (de) 1996-07-17
MA21922A1 (fr) 1991-04-01
DE69027818T2 (de) 1996-11-21
HK1007558A1 (en) 2003-07-10
EP0411941A2 (de) 1991-02-06
CA2020950C (en) 2000-04-11
PT94188B (pt) 1996-12-31
YU145390A (sh) 1992-09-07
PT94188A (pt) 1991-04-18
IE902812A1 (en) 1991-02-27
BR9003694A (pt) 1991-09-03
CA2020950A1 (en) 1991-02-05
HU205128B (en) 1992-03-30
OA09300A (en) 1992-09-15
NO178196C (no) 1996-02-07
IL110861A0 (en) 1994-11-28
RU1838321C (ru) 1993-08-30
DD297414A5 (de) 1992-01-09
CN1091744A (zh) 1994-09-07
CN1049351A (zh) 1991-02-20
CZ379690A3 (cs) 2000-08-16
SK279107B6 (sk) 1998-06-03
EP0411941A3 (en) 1992-04-15
US4937333A (en) 1990-06-26
DZ1436A1 (fr) 2004-09-13
CN1024196C (zh) 1994-04-13
BG92627A (bg) 1993-12-24
LV10718B (en) 1996-04-20
NO178196B (no) 1995-10-30
ES2090105T3 (es) 1996-10-16
NO970653D0 (no) 1997-02-12
EG19250A (en) 1994-09-29
NO903419D0 (no) 1990-08-03
IL95094A0 (en) 1991-06-10
YU47368B (sh) 1995-01-31
KR0178877B1 (ko) 1999-05-15
DK0411941T3 (da) 1996-11-11
BR1101174A (pt) 2000-08-08
SA90110175B1 (ar) 2004-03-09
HU904890D0 (en) 1991-01-28
AP163A (en) 1992-01-11
NO970653L (no) 1991-02-05
FI105033B (fi) 2000-05-31
KR910004642A (ko) 1991-03-29
PH26901A (en) 1992-12-03
RO105967B1 (ro) 1993-01-30
HUT54698A (en) 1991-03-28
PL164908B1 (pl) 1994-10-31
AU634267B2 (en) 1993-02-18
JP2922263B2 (ja) 1999-07-19
PL166453B1 (pl) 1995-05-31
CZ290556B6 (cs) 2002-08-14

Similar Documents

Publication Publication Date Title
HU906977D0 (en) Process for producing 2,3-dihydro-2-oxo-1h-imidazo(4,5-b)quinolinyl-oxyalkane-carboxylic acid amides
HUT45530A (en) Process for producing 3-pyrrolidinyl-thio-1-azobicyclo (3-2-0)hept-2-en-2-carboxylic acid derivatives
IL110861A (en) Process for preparing pure ethylediaminetetra (methylenphosphonic acid)
YU67290A (en) Process for preparing cephodizim-disodium
HUT46021A (en) Process for producing ceph-3-eme-4-carboxylic acid derivatives
CS647590A3 (en) Process for preparing 6-hydroxynicotinic acid
GB2215720B (en) Process for preparing n-phosphono-methyl-imino-diacetic acid
GB2199030B (en) Process for preparing alpha-phenylpropionic acid derivative
GB8824278D0 (en) New isopolypeptides & process for preparation thereof
YU96988A (en) Process for preparing 4,4'-dinitrostilbene-2,2'-disulphonic acid
HU906329D0 (en) Process for producing pyridyl-cyclopropane-carboxylic acid derivatives
EP0546906A3 (en) Novel process for preparing 4-amino-5-hexenoic acid
GR3001433T3 (en) Process for preparing an aromatic acid
HU905833D0 (en) Process for producing 3-methyl-quinoline-8-carboxylic acid
DE3760506D1 (en) Process for preparing cyclohexanonecarboxylic acid compounds
EP0230895A3 (en) Process for producing hydroxylamine-0-sulfonic acid
EP0239063A3 (en) Process for preparing n-omega-trifluoroacetyl amino acid
GB8921692D0 (en) Process for preparing pure n-methyl-antranilic acid methyl ester
CS505187A2 (en) Process for preparing 1-/3-brom-/2s/-methylpropionyl/pyrrolidin-/2s/-carboxylic acid
GB8730298D0 (en) Novel aminoalkanoyl-dibenzo(d g)(1 3 6)dioxazocines & process for preparation thereof
GB2221905B (en) Process for preparing methoxyacetic acid
YU185288A (en) Process for preparing 6-amino-6-deoxy-ascorbinic acid
HU906452D0 (en) Process for producing thiazeto-quinoline-carboxylic acid
CS915987A1 (en) Process for preparing d-galactopyranuroic acid
CS960187A1 (en) Process for preparing trichlorisocyanuric acid

Legal Events

Date Code Title Description
FF Patent granted
FF Patent granted
KB Patent renewed
KB Patent renewed