IE37730B1 - Process for the production of n-phosphonomethyl glycine - Google Patents

Process for the production of n-phosphonomethyl glycine

Info

Publication number
IE37730B1
IE37730B1 IE868/73A IE86873A IE37730B1 IE 37730 B1 IE37730 B1 IE 37730B1 IE 868/73 A IE868/73 A IE 868/73A IE 86873 A IE86873 A IE 86873A IE 37730 B1 IE37730 B1 IE 37730B1
Authority
IE
Ireland
Prior art keywords
phosphonomethyl
production
iminodiacetic acid
phosphonomethyl glycine
glycine
Prior art date
Application number
IE868/73A
Other languages
English (en)
Other versions
IE37730L (en
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US05/258,281 external-priority patent/US3954848A/en
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of IE37730L publication Critical patent/IE37730L/xx
Publication of IE37730B1 publication Critical patent/IE37730B1/xx

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Saccharide Compounds (AREA)
IE868/73A 1972-05-31 1973-05-30 Process for the production of n-phosphonomethyl glycine IE37730B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US05/258,281 US3954848A (en) 1972-05-31 1972-05-31 Process for producing N-phosphonomethyl glycine
US05/333,414 US3950402A (en) 1972-05-31 1973-02-16 Process for producing N-phosphonomethyl glycine

Publications (2)

Publication Number Publication Date
IE37730L IE37730L (en) 1973-11-30
IE37730B1 true IE37730B1 (en) 1977-09-28

Family

ID=26946544

Family Applications (1)

Application Number Title Priority Date Filing Date
IE868/73A IE37730B1 (en) 1972-05-31 1973-05-30 Process for the production of n-phosphonomethyl glycine

Country Status (25)

Country Link
US (1) US3950402A (cg-RX-API-DMAC7.html)
JP (1) JPS5111093B2 (cg-RX-API-DMAC7.html)
BE (1) BE800238A (cg-RX-API-DMAC7.html)
BG (1) BG21212A3 (cg-RX-API-DMAC7.html)
CA (1) CA992093A (cg-RX-API-DMAC7.html)
CH (1) CH574968A5 (cg-RX-API-DMAC7.html)
CS (1) CS177133B2 (cg-RX-API-DMAC7.html)
DD (1) DD104303A5 (cg-RX-API-DMAC7.html)
DE (1) DE2327680C3 (cg-RX-API-DMAC7.html)
DK (1) DK138951B (cg-RX-API-DMAC7.html)
EG (1) EG11140A (cg-RX-API-DMAC7.html)
ES (2) ES415335A1 (cg-RX-API-DMAC7.html)
FR (2) FR2186477B1 (cg-RX-API-DMAC7.html)
GB (1) GB1432043A (cg-RX-API-DMAC7.html)
HU (1) HU167343B (cg-RX-API-DMAC7.html)
IE (1) IE37730B1 (cg-RX-API-DMAC7.html)
IL (1) IL42393A (cg-RX-API-DMAC7.html)
IT (1) IT988869B (cg-RX-API-DMAC7.html)
NL (1) NL162656C (cg-RX-API-DMAC7.html)
NO (2) NO140556C (cg-RX-API-DMAC7.html)
PL (1) PL107856B1 (cg-RX-API-DMAC7.html)
RO (2) RO66031A (cg-RX-API-DMAC7.html)
SE (2) SE404019B (cg-RX-API-DMAC7.html)
SU (1) SU623523A3 (cg-RX-API-DMAC7.html)
YU (2) YU36977B (cg-RX-API-DMAC7.html)

Families Citing this family (66)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4072706A (en) * 1976-01-02 1978-02-07 Monsanto Company Oxidation of phosphonomethylamines
ES465139A1 (es) * 1976-12-20 1978-10-01 Monsanto Co Un procedimiento para preparar una mono-o disal de n-fosfo- nometilglicina.
US4454043A (en) * 1980-11-17 1984-06-12 Monsanto Company Column switching procedure
IL66824A0 (en) * 1982-06-25 1982-12-31 Geshuri Lab Ltd Process for producing n-phosphonomethylglycine derivatives and herbicidal compounds and compositions prepared thereby
IL68716A (en) * 1983-05-17 1987-03-31 Geshuri Lab Ltd Process for producing n-phosphonomethylglycine
US4579689A (en) * 1985-02-11 1986-04-01 Monsanto Company Oxidation with coated catalyst
US4582650A (en) * 1985-02-11 1986-04-15 Monsanto Company Oxidation with encapsulated co-catalyst
US4696772A (en) * 1985-02-28 1987-09-29 Monsanto Company Amine oxidation using carbon catalyst having oxides removed from surface
US4657705A (en) * 1985-09-23 1987-04-14 Monsanto Company Process for the preparation of N-substituted aminomethylphosphonic acids
GB8726714D0 (en) * 1987-11-14 1987-12-16 Beecham Group Plc Compounds
US5187292A (en) * 1988-08-18 1993-02-16 Rhone-Poulenc Agrochimie N-sulfomethylglycinate, use in the preparation of herbicides of the glyphosate type
FR2635522B1 (fr) * 1988-08-18 1990-11-16 Rhone Poulenc Agrochimie N-sulfonomethylglycinate procede de preparation, utilisation dans la preparation d'herbicides de type glyphosate
US4898972A (en) * 1988-09-26 1990-02-06 Monsanto Company Process for producing N-phosphonomethylglycine
HU204533B (en) * 1988-11-02 1992-01-28 Nitrokemia Ipartelepek Process for producing n-phosphono-methyl-glycine
US4937376A (en) * 1989-05-25 1990-06-26 Monsanto Company Process for producing N-phosphonomethylglycine
US4952723A (en) * 1989-07-31 1990-08-28 Monsanto Company Process for producing N-phosphonomethylglycine
US5047579A (en) * 1990-01-26 1991-09-10 Monsanto Company Process for producing n-phosphonomethylglycine
ES2021229A6 (es) * 1990-03-12 1991-10-16 Ercros Sa Perfeccionamientos introducidos en un procedimiento de obtencion de n-fosfonometilglicina por oxidacion de n-fosfonometiliminodiacetico.
US5077431A (en) * 1990-06-25 1991-12-31 Monsanto Company Peroxide process for producing n-phosphonomethylglycine
US5043475A (en) * 1990-06-25 1991-08-27 Monsanto Company Peroxide process for producing N-phosphonomethylglycine
US5095140A (en) * 1990-06-25 1992-03-10 Monsanto Company Peroxide process for producing N-phosphonomethylglycine
US5023369A (en) * 1990-06-25 1991-06-11 Monsanto Company Process for producing N-phosphonomethylglycine
US5077430A (en) * 1990-06-25 1991-12-31 Monsanto Company Peroxide process for producing N-phosphonomethylglycine
US5061820A (en) * 1990-10-22 1991-10-29 Monsanto Company Process for producing N-phosphonomethylgylcine
US5072033A (en) * 1990-12-11 1991-12-10 Monsanto Company Process for producing N-phosphonomethylglycine
GB9300641D0 (en) * 1993-01-14 1993-03-03 Zeneca Ltd Process
SI9400449A (en) * 1994-12-20 1996-06-30 Pinus D D Process for preparing N-phosphonomethyl glycin
US6365772B1 (en) * 1995-05-30 2002-04-02 Hampshire Chemical Corp. Facile synthesis of phosphonomethylglycine from phosphonomethyliminodiacetic acid
ATE213249T1 (de) * 1995-06-07 2002-02-15 Monsanto Technology Llc Verfahren zur herstellung von n- phosphonomethyliminodiessigesäure.
US5986128A (en) * 1996-11-01 1999-11-16 Monsanto Company Use of monosodium iminodiacetic acid solutions in the preparation of N-phosphonomethyliminodiacetic acid
RU2184118C2 (ru) * 1998-02-12 2002-06-27 Монсанто Компани Способ получения глифосата и катализатор окисления
EP1716923A1 (en) * 1998-02-12 2006-11-02 Monsanto Technology, LLC Oxidation catalyst for making glyphosate
US6232494B1 (en) * 1998-02-12 2001-05-15 Monsanto Company Process for the preparation of N-(phosphonomethyl)glycine by oxidizing N-substituted N-(phosphonomethyl)glycine
US6417133B1 (en) 1998-02-25 2002-07-09 Monsanto Technology Llc Deeply reduced oxidation catalyst and its use for catalyzing liquid phase oxidation reactions
US5962729A (en) * 1998-05-14 1999-10-05 Calgon Carbon Corporation Method for the manufacture of N-phosphonomethylglycine from N-phosphonomethyliminodiacetic acid using a catalytic carbon
AU5030099A (en) * 1998-07-06 2000-01-24 Syngenta Participations Ag Preparation of n-phosphonomethylglycine salts
IES980552A2 (en) * 1998-07-09 1999-08-11 Agritech Chemical Ltd Improved process for preparing N-phosphonomethyl iminodiacetic acid
AU6024599A (en) * 1998-09-08 2000-03-27 Hampshire Chemical Corp. Synthesis of phosphonomethyliminodiacetic acid with reduced effluent
ES2195929T3 (es) 1999-07-23 2003-12-16 Basf Ag Procedimiento para la obtencion de glifosatos o de una sal de los mismos.
EP1200450B1 (de) 1999-08-11 2003-11-12 Basf Aktiengesellschaft Verfahren zur herstellung von phosphonomethylglycin
EP1923395A1 (en) 1999-12-21 2008-05-21 Monsanto Technology, LLC Use of supplemental promoter in conjuction with a carbon-supported, noble-metal-containing catalyst in liquid phase oxidation reactions
PT102419A (pt) * 2000-02-09 2001-08-30 Pedro Manuel Brito Da Silva Co N-fosfonoalquil)glicina n-(fosfonobenzil)glicina e n-(fosfonofenetil)glicina e seu processo de fabrico e a sua aplicacao como herbicida
AU2001264605C1 (en) * 2000-05-15 2005-10-06 Monsanto Technology Llc Preparation of iminodiacetic acid compounds from monoethanolamine substrates
US6927304B2 (en) 2000-05-22 2005-08-09 Monsanto Technology Llc De-oxygenation treatment for noble metal on carbon catalysts used in liquid phase oxidation reactions
CA2409745A1 (en) * 2000-05-22 2001-12-06 Monsanto Technology, Llc Reaction systems for making n-(phosphonomethyl)glycine compounds
WO2002095373A1 (en) * 2001-05-22 2002-11-28 Monsanto Technology Llc Use of infrared spectroscopy for on-line process control and endpoint detection
DE10130136A1 (de) * 2001-06-22 2003-01-02 Basf Ag Verfahren zur Gewinnung von N-Phosphonomethylglycin
AU2002362929B2 (en) 2001-10-18 2007-08-09 Monsanto Technology Llc Process and catalyst for dehydrogenating primary alcohols to make carboxylic acid salts
BRPI0307672B1 (pt) * 2002-02-14 2015-12-22 Monsanto Technology Llc processo para a oxidação de aminas terciárias
US7390920B2 (en) * 2002-02-14 2008-06-24 Monsanto Technology Llc Oxidation catalyst and process
US6921834B2 (en) 2002-05-22 2005-07-26 Dow Agrosciences Llc Continuous process for preparing N-phosphonomethyl glycine
JP4202047B2 (ja) * 2002-05-24 2008-12-24 富士通株式会社 ヘッド位置制御方法及びデイスク記憶装置
AR040319A1 (es) * 2002-06-28 2005-03-23 Monsanto Technology Llc Uso de telurio en catalizadores con contenido de metales nobles y con soporte de carbon para reacciones de oxidacion en fase liquida
BRPI0413586A (pt) 2003-08-14 2006-10-17 Monsanto Technology Llc catalisadores contendo metal de transição e processo para a preparação dos mesmos e uso como catalisadores de oxidação e de desidrogenação
ES2299874T3 (es) * 2003-09-17 2008-06-01 Monsanto Technology Llc Procedimiento para recuperar un producto cristalino de una solucion.
WO2006031938A2 (en) * 2004-09-15 2006-03-23 Monsanto Technology Llc Oxidation catalyst and its use for catalyzing liquid phase oxidation reactions
AR054096A1 (es) * 2004-11-12 2007-06-06 Monsanto Technology Llc Recuperacion de metales nobles de corrientes de proceso acuosas y proceso de preparacion de n-(fosfonometil)-glicina
BRPI0608355B1 (pt) * 2005-02-17 2016-05-24 Monsanto Technology Llc processo para oxidação de ácido n-(fosfonometil) iminodiacético ou seu sal e catalisador de oxidação
AR056660A1 (es) * 2005-04-25 2007-10-17 Monsanto Technology Llc Alteracion de la distribucion de tamanos de cristales de acido n-(fosfonometil) iminodiacetico para mejorar la filtracion y la calidad del producto
BRPI0708081A2 (pt) * 2006-02-17 2011-05-17 Monsanto Technology Llc catalisadores contendo metal de transição e processos para a sua preparação e uso como catalisadores de pilha termoelétrica
US7771494B2 (en) * 2007-01-31 2010-08-10 Monsanto Technology Llc Process for selective removal of water and impurities from N-(phosphonomethyl)glycine
US8252953B2 (en) 2008-05-01 2012-08-28 Monsanto Technology Llc Metal utilization in supported, metal-containing catalysts
CN101353358B (zh) * 2008-09-05 2011-01-19 江苏好收成韦恩农化股份有限公司 用改进反应系统制备n-(膦酰基甲基)甘氨酸的方法
CN103044486A (zh) * 2013-01-02 2013-04-17 北京化工大学 一种直接氧化双甘膦制备草甘膦的方法
WO2019005718A1 (en) 2017-06-26 2019-01-03 Monsanto Technology Llc PHOSPHORUS CONTROL FOR WASTE FLOWS FROM GLYPHOSATE MANUFACTURING PROCESSES
CN109796491A (zh) * 2018-12-24 2019-05-24 荆州鸿翔化工有限公司 一种制备草甘膦的方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL285361A (cg-RX-API-DMAC7.html) * 1961-11-13 1900-01-01
US3429914A (en) * 1964-09-03 1969-02-25 Monsanto Co Organo-phosphono-amine oxides
DE2132511C3 (de) * 1971-06-30 1974-06-27 Joh. A. Benckiser Gmbh, 6700 Ludwigshafen Verfahren zur Herstellung von Aminomethylenphosphonsäuren

Also Published As

Publication number Publication date
ES440610A1 (es) 1977-03-01
YU36977B (en) 1984-08-31
DE2327680C3 (de) 1979-01-04
GB1432043A (en) 1976-04-14
AU5627773A (en) 1974-12-05
DD104303A5 (cg-RX-API-DMAC7.html) 1974-03-05
NO149176C (no) 1984-02-29
NL162656C (nl) 1980-06-16
NL7307449A (cg-RX-API-DMAC7.html) 1973-12-04
SE407579B (sv) 1979-04-02
SE7600415L (sv) 1976-01-16
IT988869B (it) 1975-04-30
CS177133B2 (cg-RX-API-DMAC7.html) 1977-07-29
NO140556B (no) 1979-06-18
FR2186477A1 (cg-RX-API-DMAC7.html) 1974-01-11
BE800238A (fr) 1973-11-30
YU142773A (en) 1982-06-18
DE2327680A1 (de) 1973-12-13
NO140556C (no) 1979-09-26
HU167343B (cg-RX-API-DMAC7.html) 1975-09-27
NO783636L (no) 1973-12-03
FR2186477B1 (cg-RX-API-DMAC7.html) 1977-12-30
IL42393A0 (en) 1973-07-30
YU262880A (en) 1983-06-30
JPS4948620A (cg-RX-API-DMAC7.html) 1974-05-11
CA992093A (en) 1976-06-29
US3950402A (en) 1976-04-13
IE37730L (en) 1973-11-30
YU42985B (en) 1989-02-28
FR2193831A1 (cg-RX-API-DMAC7.html) 1974-02-22
ES415335A1 (es) 1976-05-01
DK138951B (da) 1978-11-20
SU623523A3 (ru) 1978-09-05
EG11140A (en) 1977-08-15
DE2327680B2 (de) 1978-05-11
RO62901A (cg-RX-API-DMAC7.html) 1977-08-15
NO149176B (no) 1983-11-21
RO66031A (ro) 1980-07-15
DK138951C (cg-RX-API-DMAC7.html) 1979-06-05
IL42393A (en) 1975-12-31
JPS5111093B2 (cg-RX-API-DMAC7.html) 1976-04-08
PL107856B1 (pl) 1980-03-31
CH574968A5 (cg-RX-API-DMAC7.html) 1976-04-30
FR2193831B1 (cg-RX-API-DMAC7.html) 1978-01-06
NL162656B (nl) 1980-01-15
SE404019B (sv) 1978-09-18
BG21212A3 (bg) 1976-03-20

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