HUP0102993A2 - Eljárás víztelenítésre - Google Patents
Eljárás víztelenítésreInfo
- Publication number
- HUP0102993A2 HUP0102993A2 HU0102993A HUP0102993A HUP0102993A2 HU P0102993 A2 HUP0102993 A2 HU P0102993A2 HU 0102993 A HU0102993 A HU 0102993A HU P0102993 A HUP0102993 A HU P0102993A HU P0102993 A2 HUP0102993 A2 HU P0102993A2
- Authority
- HU
- Hungary
- Prior art keywords
- water
- formaldehyde
- starting
- formaldehyde solution
- dewatering process
- Prior art date
Links
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- 239000008098 formaldehyde solution Substances 0.000 abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- 150000001875 compounds Chemical class 0.000 abstract 2
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 abstract 1
- RJUFJBKOKNCXHH-UHFFFAOYSA-N Methyl propionate Chemical compound CCC(=O)OC RJUFJBKOKNCXHH-UHFFFAOYSA-N 0.000 abstract 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 abstract 1
- 229940017219 methyl propionate Drugs 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
- C07C45/84—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation by azeotropic distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
- C07C45/83—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation by extractive distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/20—Power plant
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/22—Accessories
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A találmány tárgya eljárás a kiindulási formaldehid oldaténállényegesen kisebb víztartalmú formaldehid-tartalmú termékelőállítására formaldehidet, vizet és adott esetben metanolttartalmazó kiindulási formaldehid oldatból oly módon, hogy akiindulási formaldehid oldatot egy vízelszállító vegyület jejenlétébendesztillálják. Vízelszállító vegyületként különösen előnyösenhasználható metil-propionát vagy metil-metakrilát. Ó
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB9812083.5A GB9812083D0 (en) | 1998-06-05 | 1998-06-05 | Removal of water |
PCT/GB1999/001724 WO1999064387A1 (en) | 1998-06-05 | 1999-06-01 | Dewatering process |
Publications (3)
Publication Number | Publication Date |
---|---|
HUP0102993A2 true HUP0102993A2 (hu) | 2001-11-28 |
HUP0102993A3 HUP0102993A3 (en) | 2002-08-28 |
HU227631B1 HU227631B1 (en) | 2011-10-28 |
Family
ID=10833241
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU0102993A HU227631B1 (en) | 1998-06-05 | 1999-06-01 | Dewatering process |
Country Status (19)
Country | Link |
---|---|
US (2) | US6478929B1 (hu) |
EP (1) | EP1084095B1 (hu) |
JP (3) | JP2002517477A (hu) |
KR (1) | KR100407510B1 (hu) |
CN (2) | CN1291964C (hu) |
AU (1) | AU762099B2 (hu) |
BR (1) | BR9910957B1 (hu) |
CA (1) | CA2332042C (hu) |
CZ (1) | CZ295063B6 (hu) |
DE (1) | DE69912949T2 (hu) |
ES (1) | ES2211193T3 (hu) |
GB (1) | GB9812083D0 (hu) |
HU (1) | HU227631B1 (hu) |
MY (1) | MY129116A (hu) |
NZ (1) | NZ508175A (hu) |
PL (1) | PL195079B1 (hu) |
RU (2) | RU2338737C2 (hu) |
TW (1) | TW565550B (hu) |
WO (1) | WO1999064387A1 (hu) |
Families Citing this family (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19925870A1 (de) * | 1999-06-07 | 2000-12-14 | Basf Ag | Verfahren zur Umsetzung einer ein Gemisch enthaltenden Lösung |
US20090133437A1 (en) * | 2005-07-28 | 2009-05-28 | Rian Reyneke | Recovery of Co-Rich Product From a Mixed Gas Containing Heavy Hydrocarbons |
US9486441B2 (en) | 2008-04-21 | 2016-11-08 | Signum Biosciences, Inc. | Compounds, compositions and methods for making the same |
MX2011001788A (es) * | 2008-08-20 | 2011-08-17 | Futurefuel Chemical Co | Preparacion de dibutoximetano. |
US9249081B2 (en) * | 2011-12-16 | 2016-02-02 | Celanese International Corporation | Processes for the production of acrylic acids and acrylates |
WO2013121594A1 (en) * | 2012-02-17 | 2013-08-22 | Mitsubishi Rayon Co., Ltd. | Dehydration of water containing source of formaldehyde, and a method for producing an ethylenically unsaturated carboxylic ester |
JP2015506908A (ja) * | 2012-02-17 | 2015-03-05 | ルーサイト インターナショナル ユーケー リミテッド | ホルムアルデヒドの水含有供給源の脱水、およびエチレン性不飽和カルボン酸エステルを生成するための方法 |
US9713732B2 (en) | 2012-03-16 | 2017-07-25 | Meggitt Safety Systems, Inc. | Fire suppressing materials and systems and methods of use |
US8920668B2 (en) * | 2012-03-16 | 2014-12-30 | Meggitt Safety Systems Inc. | Fire suppressing materials and systems and methods of use |
US9034202B2 (en) * | 2012-03-16 | 2015-05-19 | Meggitt Safety Systems Inc. | Fire suppressing materials and systems and methods of use |
CN104147800B (zh) * | 2014-08-27 | 2017-01-18 | 江苏凯茂石化科技有限公司 | 一种两段式甲醇蒸发塔及甲醇蒸发工艺方法 |
GB201617534D0 (en) * | 2016-10-14 | 2016-11-30 | Lucite International Uk Limited | A process for the production of Ethylenically unsaturated carboxylic acid esters and a catalyst therefor |
GB201621985D0 (en) | 2016-12-22 | 2017-02-08 | Johnson Matthey Davy Technologies Ltd | Process |
CN107337600A (zh) * | 2017-07-04 | 2017-11-10 | 湖北三里枫香科技有限公司 | 一种甲醇和醋酸甲酯生产甲基丙烯酸甲酯的方法及工艺装置 |
CN109133232A (zh) * | 2018-09-27 | 2019-01-04 | 南通天泽化工有限公司 | 一种高浓度甲醛溶液的回收系统及其回收方法 |
CN113509921B (zh) * | 2021-07-16 | 2023-03-17 | 中国科学院兰州化学物理研究所 | 一种双功能催化剂体系及其应用 |
CN113943205A (zh) * | 2021-09-26 | 2022-01-18 | 西南化工研究设计院有限公司 | 一种甲醛溶液脱水浓缩的方法 |
CN115819231B (zh) * | 2021-10-31 | 2024-06-25 | 浙江新和成股份有限公司 | 甲基丙烯酸甲酯的制备方法和装置 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3174912A (en) * | 1965-03-23 | Purification of formaldehyde | ||
BE560841A (hu) | 1953-07-16 | |||
GB1107234A (en) | 1965-10-22 | 1968-03-27 | Air Reduction | Production of acrylate and methacrylate esters |
US3535371A (en) | 1965-12-29 | 1970-10-20 | Commercial Solvents Corp | Process for the preparation of acrylic esters |
NL6814946A (en) | 1968-10-18 | 1970-04-21 | Recovery of formaldehyde from aqueous formaldehyde - streams | |
DE1928633C3 (de) * | 1969-06-06 | 1978-03-23 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von wasserarmen Lösungen von Formaldehyd |
US3629997A (en) * | 1970-05-08 | 1971-12-28 | Borden Inc | Process for producing methanol-formaldehyde solution of low-water content |
IT1010299B (it) * | 1973-05-11 | 1977-01-10 | Basf Ag | Processo per la preparazione di formaldeide |
US4040913A (en) * | 1975-09-02 | 1977-08-09 | Rohm And Haas Company | Recovery of methacrylic acid from the effluent obtained from the condensation of formaldehyde and propionic acid |
FR2409975A1 (fr) * | 1977-11-29 | 1979-06-22 | Sterlitamaxky O Promyshlenny | Procede d'isolement du formaldehyde a partir de ses solutions aqueuses |
DE3004467A1 (de) | 1980-02-07 | 1981-08-13 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von methylmethacrylat durch umsetzung von methylpropionat und methanol |
US4348540A (en) * | 1981-06-29 | 1982-09-07 | Monsanto Company | Manufacture of aqueous formaldehyde |
JPS6115858A (ja) | 1984-06-25 | 1986-01-23 | アモコ・コーポレーシヨン | アルファーベータエチレン性不飽和カルボン酸化合物の製造方法 |
US4942258A (en) | 1984-06-25 | 1990-07-17 | Amoco Corporation | Process for preparation of methacrylic acid with regeneration of catalyst |
DE3446528A1 (de) * | 1984-12-20 | 1986-06-26 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von glyoxylsaeurehemiacetalestern |
JPS632951A (ja) * | 1986-06-23 | 1988-01-07 | Mitsubishi Gas Chem Co Inc | メチルメタアクリレ−トの製造方法 |
JPH078812B2 (ja) | 1986-09-24 | 1995-02-01 | 住友化学工業株式会社 | ホルムアルデヒドの製法 |
GB2218089B (en) | 1988-04-07 | 1991-11-06 | Asahi Chemical Ind | Process for producing high purity formaldehyde |
-
1998
- 1998-06-05 GB GBGB9812083.5A patent/GB9812083D0/en not_active Ceased
-
1999
- 1999-06-01 KR KR10-2000-7013112A patent/KR100407510B1/ko not_active IP Right Cessation
- 1999-06-01 ES ES99955468T patent/ES2211193T3/es not_active Expired - Lifetime
- 1999-06-01 HU HU0102993A patent/HU227631B1/hu unknown
- 1999-06-01 CA CA002332042A patent/CA2332042C/en not_active Expired - Lifetime
- 1999-06-01 RU RU2004103423/04A patent/RU2338737C2/ru active
- 1999-06-01 CN CNB2004100385388A patent/CN1291964C/zh not_active Expired - Lifetime
- 1999-06-01 CZ CZ20004459A patent/CZ295063B6/cs not_active IP Right Cessation
- 1999-06-01 PL PL99344472A patent/PL195079B1/pl unknown
- 1999-06-01 CN CNB998070629A patent/CN1223570C/zh not_active Expired - Lifetime
- 1999-06-01 RU RU2001101477/04A patent/RU2232744C2/ru active
- 1999-06-01 BR BRPI9910957-3A patent/BR9910957B1/pt not_active IP Right Cessation
- 1999-06-01 EP EP19990955468 patent/EP1084095B1/en not_active Expired - Lifetime
- 1999-06-01 DE DE69912949T patent/DE69912949T2/de not_active Expired - Lifetime
- 1999-06-01 JP JP2000553397A patent/JP2002517477A/ja not_active Withdrawn
- 1999-06-01 NZ NZ50817599A patent/NZ508175A/en not_active IP Right Cessation
- 1999-06-01 WO PCT/GB1999/001724 patent/WO1999064387A1/en active IP Right Grant
- 1999-06-01 AU AU42749/99A patent/AU762099B2/en not_active Expired
- 1999-06-01 US US09/701,877 patent/US6478929B1/en not_active Expired - Lifetime
- 1999-06-02 TW TW088109129A patent/TW565550B/zh not_active IP Right Cessation
- 1999-06-03 MY MYPI99002232A patent/MY129116A/en unknown
-
2002
- 2002-05-23 US US10/152,819 patent/US7338579B2/en not_active Expired - Fee Related
-
2007
- 2007-05-09 JP JP2007125044A patent/JP5485501B2/ja not_active Expired - Lifetime
-
2013
- 2013-11-22 JP JP2013241621A patent/JP2014111594A/ja active Pending
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