GR3036234T3 - Water-swelling polymers cross-linked with unsaturated amino alcohols, the production and use of same - Google Patents

Water-swelling polymers cross-linked with unsaturated amino alcohols, the production and use of same

Info

Publication number
GR3036234T3
GR3036234T3 GR20010401086T GR20010401086T GR3036234T3 GR 3036234 T3 GR3036234 T3 GR 3036234T3 GR 20010401086 T GR20010401086 T GR 20010401086T GR 20010401086 T GR20010401086 T GR 20010401086T GR 3036234 T3 GR3036234 T3 GR 3036234T3
Authority
GR
Greece
Prior art keywords
meth
pct
date
cross
polymers
Prior art date
Application number
GR20010401086T
Other languages
Greek (el)
English (en)
Inventor
Ludger Breitbach
Kurt Dahmen
Jochen Houben
Erich Kuester
Original Assignee
Stockhausen Chem Fab Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stockhausen Chem Fab Gmbh filed Critical Stockhausen Chem Fab Gmbh
Publication of GR3036234T3 publication Critical patent/GR3036234T3/el

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/26Synthetic macromolecular compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/04Acids; Metal salts or ammonium salts thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/60Liquid-swellable gel-forming materials, e.g. super-absorbents
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F251/00Macromolecular compounds obtained by polymerising monomers on to polysaccharides or derivatives thereof
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F261/00Macromolecular compounds obtained by polymerising monomers on to polymers of oxygen-containing monomers as defined in group C08F16/00
    • C08F261/02Macromolecular compounds obtained by polymerising monomers on to polymers of oxygen-containing monomers as defined in group C08F16/00 on to polymers of unsaturated alcohols
    • C08F261/04Macromolecular compounds obtained by polymerising monomers on to polymers of oxygen-containing monomers as defined in group C08F16/00 on to polymers of unsaturated alcohols on to polymers of vinyl alcohol
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C08F290/02Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups on to polymers modified by introduction of unsaturated end groups
    • C08F290/06Polymers provided for in subclass C08G
    • C08F290/062Polyethers
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K17/00Soil-conditioning materials or soil-stabilising materials
    • C09K17/14Soil-conditioning materials or soil-stabilising materials containing organic compounds only
    • C09K17/18Prepolymers; Macromolecular compounds
    • C09K17/20Vinyl polymers
    • C09K17/22Polyacrylates; Polymethacrylates
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B3/00Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/18Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
    • H01B3/20Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances liquids, e.g. oils

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Dispersion Chemistry (AREA)
  • Hematology (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Physics & Mathematics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Soil Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Graft Or Block Polymers (AREA)
  • Absorbent Articles And Supports Therefor (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Macromonomer-Based Addition Polymer (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Soil Conditioners And Soil-Stabilizing Materials (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
GR20010401086T 1995-11-21 2001-07-18 Water-swelling polymers cross-linked with unsaturated amino alcohols, the production and use of same GR3036234T3 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19543366A DE19543366C2 (de) 1995-11-21 1995-11-21 Mit ungesättigten Aminoalkoholen vernetzte, wasserquellbare Polymerisate, deren Herstellung und Verwendung
PCT/EP1996/005073 WO1997018889A1 (de) 1995-11-21 1996-11-18 Mit ungesättigten aminoalkoholen vernetzte, wasserquellbare polymerisate, deren herstellung und verwendung

Publications (1)

Publication Number Publication Date
GR3036234T3 true GR3036234T3 (en) 2001-10-31

Family

ID=7778012

Family Applications (1)

Application Number Title Priority Date Filing Date
GR20010401086T GR3036234T3 (en) 1995-11-21 2001-07-18 Water-swelling polymers cross-linked with unsaturated amino alcohols, the production and use of same

Country Status (14)

Country Link
US (1) US6087450A (OSRAM)
EP (1) EP0873187B1 (OSRAM)
JP (1) JP3957004B2 (OSRAM)
KR (1) KR19990071528A (OSRAM)
CN (1) CN1207691A (OSRAM)
AT (1) ATE202298T1 (OSRAM)
CZ (1) CZ156198A3 (OSRAM)
DE (2) DE19543366C2 (OSRAM)
DK (1) DK0873187T3 (OSRAM)
ES (1) ES2159052T3 (OSRAM)
GR (1) GR3036234T3 (OSRAM)
PT (1) PT873187E (OSRAM)
TW (1) TW363980B (OSRAM)
WO (1) WO1997018889A1 (OSRAM)

Families Citing this family (57)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19854575A1 (de) 1998-11-26 2000-05-31 Basf Ag Vernetzte quellfähige Polymere
WO2000040626A1 (en) * 1999-01-06 2000-07-13 The Stewart Group, Inc. Flexible water absorbent polymer coating
GB9900298D0 (en) * 1999-01-07 1999-02-24 Medical Res Council Optical sorting method
DE19909653A1 (de) * 1999-03-05 2000-09-07 Stockhausen Chem Fab Gmbh Pulverförmige, vernetzte, wässrige Flüssigkeiten sowie Blut absorbierende Polymere, Verfahren zu ihrer Herstellung und ihre Verwendung
DE19941423A1 (de) * 1999-08-30 2001-03-01 Stockhausen Chem Fab Gmbh Polymerzusammensetzung und ein Verfahren zu dessen Herstellung
DE10053858A1 (de) 2000-10-30 2002-05-08 Stockhausen Chem Fab Gmbh Absorbierendes Gebilde mit verbesserten Blockingeigenschaften
DE10161496A1 (de) * 2001-12-14 2003-06-26 Stockhausen Chem Fab Gmbh Kompaktierte absorbierende Polymere, deren Herstellung und Verwendung
US7005143B2 (en) * 2002-04-12 2006-02-28 3M Innovative Properties Company Gel materials, medical articles, and methods
WO2004037900A1 (de) 2002-10-25 2004-05-06 Stockhausen Gmbh Zweistufiges mischverfahren zur herstellung eines absorbierenden polymers
US8247491B2 (en) * 2003-02-10 2012-08-21 Nippon Shokubai Co., Ltd. Water-absorbent resin composition and its production process
EP1594556B1 (en) * 2003-02-10 2007-04-11 Nippon Shokubai Co., Ltd. Particulate water-absorbing agent
DE10321536B4 (de) * 2003-05-14 2013-03-07 Evonik Goldschmidt Gmbh Aminoalkohol-basierte Tenside mit geringer Oberflächenspannung und deren Verwendung
DE10334286B4 (de) 2003-07-25 2006-01-05 Stockhausen Gmbh Pulverförmige,wasserabsorbierende Polymere mit mittels thermoplastischen Klebstoffen gebundenen Feinteilchen, Verfahren zu deren Herstellung sowie diese beinhaltende chemische Produkte und Verbunde
DE10334271B4 (de) 2003-07-25 2006-02-23 Stockhausen Gmbh Verfahren zur Agglomeration von Superabsorberfeinteilchen, daraus erhältliche Superabsorberpartikel, deren Verwendung sowie diese beinhaltende Verbunde
US7291674B2 (en) * 2003-10-28 2007-11-06 Stockhausen, Inc. Superabsorbent polymer
BRPI0417388B1 (pt) * 2003-12-12 2014-11-18 Nippon Catalytic Chem Ind Agente para absorção de água e método de fabricação do mesmo
DE102004016650A1 (de) * 2004-03-31 2005-10-20 Basf Ag Diallylamine enthaltende Polymerisate
TWI353360B (en) * 2005-04-07 2011-12-01 Nippon Catalytic Chem Ind Production process of polyacrylic acid (salt) wate
DE102005018924A1 (de) * 2005-04-22 2006-10-26 Stockhausen Gmbh Wasserabsorbierende Polymergebilde mit verbesserten Absorptionseigenschaften
TWI394789B (zh) 2005-12-22 2013-05-01 Nippon Catalytic Chem Ind 吸水性樹脂組成物及其製造方法、吸收性物品
EP1837348B9 (en) 2006-03-24 2020-01-08 Nippon Shokubai Co.,Ltd. Water-absorbing resin and method for manufacturing the same
EP1840137B1 (en) 2006-03-29 2009-11-25 Nippon Shokubai Co., Ltd. Method of Producing Polyacrylic Acid (Salt) Water-Absorbent Resin
US20080164067A1 (en) * 2007-01-09 2008-07-10 Ahmadi Tehrani Method for Reducing Aqueous Content of Oil-Based Fluids
JP2010538016A (ja) * 2007-08-29 2010-12-09 ソーベント セラピューティクス インコーポレイテッド 異なる対イオン含有量を有する吸収性ポリマー組成物、ならびにその調製および使用の方法
US20110054375A1 (en) 2007-11-27 2011-03-03 Hans Smola Dressing comprising polyacrylate particles and use thereof
CA2710259C (en) * 2007-12-21 2013-04-09 S.P.C.M. S.A. Polymeric thickener composition
WO2009154568A1 (en) * 2008-06-20 2009-12-23 Agency For Science, Technology And Research Water swellable and water soluble polymers and use thereof
JP5117337B2 (ja) * 2008-09-18 2013-01-16 ユニチカ株式会社 熱可塑性樹脂用添加剤
DE102009031992A1 (de) 2009-07-06 2011-01-13 Paul Hartmann Ag Vorrichtung zur Unterdrucktherapie von Wunden
WO2011040472A1 (ja) 2009-09-29 2011-04-07 株式会社日本触媒 粒子状吸水剤及びその製造方法
CA2780274C (en) 2009-11-09 2018-06-26 Spotlight Technology Partners Llc Fragmented hydrogels
CN106913902A (zh) 2009-11-09 2017-07-04 聚光灯技术合伙有限责任公司 多糖基水凝胶
DE102010043113A1 (de) 2010-10-29 2012-05-03 Evonik Stockhausen Gmbh Verfahren zur Herstellung von verbesserten absorbierenden Polymeren mittels kryogenem Mahlen
DE102011007723A1 (de) 2011-04-20 2012-10-25 Evonik Stockhausen Gmbh Verfahren zur Herstellung von wasserabsorbierenden Polymeren mit hoher Absorptionsgeschwindigkeit
DE102011086516A1 (de) 2011-11-17 2013-05-23 Evonik Degussa Gmbh Superabsorbierende Polymere mit schnellen Absorptionseigenschaften sowieVerfahren zu dessen Herstellung
KR101655104B1 (ko) * 2011-12-30 2016-09-07 에보닉 코포레이션 가교결합제를 갖는 초흡수성 중합체
US8420567B1 (en) 2011-12-30 2013-04-16 Evonik Stockhausen, Llc Process for superabsorbent polymer and crosslinker composition
DE102013203781A1 (de) 2013-03-06 2014-09-11 Evonik Industries Ag Superabsorbierende Polymere mit verbesserten Eigenschaften, insbesondere Geruchskontrolle und Farbbeständigkeit, sowie Verfahren zu dessen Herstellung
DE102013203779A1 (de) 2013-03-06 2014-09-11 Evonik Industries Ag Superabsorbierende Polymere mit verbesserter Geruchskontrolleigenschaft sowie Verfahren zu dessen Herstellung
DE102013003755A1 (de) * 2013-03-06 2014-09-11 Carl Freudenberg Kg Belüftungseinsatz
US9302248B2 (en) 2013-04-10 2016-04-05 Evonik Corporation Particulate superabsorbent polymer composition having improved stability
US9375507B2 (en) 2013-04-10 2016-06-28 Evonik Corporation Particulate superabsorbent polymer composition having improved stability
DE102013208942A1 (de) 2013-05-15 2014-11-20 Evonik Industries Ag Superabsorbierende Polymere mit schnellen Absorptionseigenschaften sowie Verfahren zu dessen Herstellung
DE102013209023A1 (de) 2013-05-15 2014-11-20 Evonik Industries Ag Superabsorbierende Polymere mit schnellen Absorptionseigenschaften sowie Verfahren zu dessen Herstellung
BR112016005768B1 (pt) 2013-09-19 2021-09-21 Microvention, Inc Películas de polímero
JP6405369B2 (ja) 2013-09-19 2018-10-17 テルモ株式会社 ポリマー粒子
AU2014346486B2 (en) 2013-11-08 2016-12-08 Terumo Corporation Polymer particles
EP2915548B1 (de) 2014-03-05 2017-11-01 Evonik Degussa GmbH Superabsorbierende polymere mit verbesserter geruchskontrolleigenschaft sowie verfahren zu deren herstellung
ES2790858T3 (es) * 2014-03-24 2020-10-29 Nitto Boseki Co Ltd Polímero de injerto y método para producir el mismo
US11680184B2 (en) 2014-07-25 2023-06-20 Evonik Superabsorber Gmbh Anti-stick processing aids and use thereof in the production of water-absorbing particles
EP3000486B1 (de) 2014-09-23 2017-11-08 Evonik Degussa GmbH Superabsorberproduktion unter Einsatz bestimmter Fördermaschinen
WO2016154592A1 (en) 2015-03-26 2016-09-29 Microvention, Inc. Embiolic particles
JP6695756B2 (ja) * 2016-07-21 2020-05-20 エボニック コーポレイションEvonik Corporation 架橋剤を含む超吸収性ポリマー
JP6898373B2 (ja) * 2016-07-21 2021-07-07 エボニック コーポレイションEvonik Corporation 架橋剤を含む超吸収性ポリマー
CA3038719C (en) 2016-09-28 2020-04-21 Terumo Corporation Polymer particles
CN109553730B (zh) * 2018-12-06 2020-12-29 太仓宝霓实业有限公司 一种低温皂洗剂共聚物及其制备方法和组合物
CN119797856B (zh) * 2025-03-11 2025-07-22 四川公路桥梁建设集团有限公司 一种c80等级改善低温韧性的混凝土及制备方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63199205A (ja) * 1987-02-12 1988-08-17 Lion Corp 高吸水性ポリマ−の製造方法
DE4206857C2 (de) * 1992-03-05 1996-08-29 Stockhausen Chem Fab Gmbh Polymerzusammensetzung, Absorptionsmaterialzusammensetzung, deren Herstellung und Verwendung
GB9208449D0 (en) * 1992-04-16 1992-06-03 Dow Deutschland Inc Crosslinked hydrophilic resins and method of preparation
WO1994009043A1 (en) * 1992-10-14 1994-04-28 The Dow Chemical Company Water-absorbent polymer having improved properties
IL110134A (en) * 1993-07-09 1998-07-15 Stockhausen Chem Fab Gmbh Polymers capable of absorbing aqueous liquids and body fluids their preparation and use
US5314420A (en) * 1993-09-17 1994-05-24 Nalco Chemical Company Superabsorbent polymer having improved absorption rate and absorption under pressure
US5610208A (en) * 1994-02-17 1997-03-11 Nippon Shokubai Co., Ltd. Water-absorbent agent, method for production thereof, and water-absorbent composition

Also Published As

Publication number Publication date
CN1207691A (zh) 1999-02-10
WO1997018889A1 (de) 1997-05-29
EP0873187A1 (de) 1998-10-28
PT873187E (pt) 2001-09-28
JP3957004B2 (ja) 2007-08-08
EP0873187B1 (de) 2001-06-20
ATE202298T1 (de) 2001-07-15
DE19543366A1 (de) 1997-05-22
JP2000501437A (ja) 2000-02-08
DK0873187T3 (da) 2001-09-03
DE19543366C2 (de) 1998-09-10
US6087450A (en) 2000-07-11
DE59607142D1 (de) 2001-07-26
ES2159052T3 (es) 2001-09-16
CZ156198A3 (cs) 1998-11-11
TW363980B (en) 1999-07-11
KR19990071528A (ko) 1999-09-27

Similar Documents

Publication Publication Date Title
GR3036234T3 (en) Water-swelling polymers cross-linked with unsaturated amino alcohols, the production and use of same
ES2139394T3 (es) Polimeros absorbedores de agua con una mejores propiedades, procedimiento para su produccion y su empleo
DE59608767D1 (de) Absorptionsmittel für wasser und wässrige flüssigkeiten sowie verfahren zu ihrer herstellung und verwendung
MX202050B (es) Polimeros absorbedores de fluidos, procesos utilizados en su produccion y su aplicacion.
AU2012203303A1 (en) Water circulation systems for ponds, lakes, and other bodies of water
ATE372792T1 (de) Superabsorptionsfähiges polymer
KR890017291A (ko) 흡수 속도가 우수한 고흡수성 수지의 제조방법
DK1185581T3 (da) Forbedringer af eller i relation til polymermaterialers modstand over for vejrpåvirkning
FR2846970A1 (fr) Procede de traitement de surface par photopolymerisation pour obtenir des proprietes biocides
ATE471166T1 (de) Vernetzte polyaminbeschichtung auf superabsorbierenden hydrogelen
UA91193C2 (ru) Гомополимер и/или сополимер акриловой кислоты, полученные контролируемой радикальной полимеризацией акриловой кислоты с использованием серных соединений как агентов передачи цепи, и их применение
BR0115816A (pt) Composições cosméticas, dermatológicas e farmacêuticas contendo tensìdios
AR035164A1 (es) Una composicion acuosa para la limpieza de la piel
ES2140468T3 (es) Material hidrofilo y membrana semipermeable fabricada a partir del mismo.
ES8707980A1 (es) Procedimiento de fabricacion de resinas hidro-absorbentes.
JPS56167757A (en) Production of water-swelling material
BR0205156A (pt) Géis capilares borrifáveis
BR0111504A (pt) Composições dilatáveis em água
KR830006396A (ko) 본 발명에 따른 접착제를 사용하여 만든 팬츠 라이너의 일부 종단면을 도시한 사시도
SE9702698D0 (sv) Compositions for lubricating and separating tissues and biological membranes
BR0304303A (pt) Composição para um sistema espessante hidrofóbico de viscosidade reduzida para o espessamento de um sistema aquoso contendo polìmero, e, métodos para fornecer um sistema espessante de viscosidade reduzida para um sistema aquoso contendo polìmero e para aumentar a viscosidade de um sistema aquoso contendo polìmero
AR037206A1 (es) Una composicion de limpieza abrasiva liquida acuosa y un procedimiento para limpiar superficies duras que utiliza dicha composicion
JPS5496541A (en) Photosensitive resin composition
ATE175403T1 (de) Füllkörperblock
ATE109803T1 (de) Hydrophile, quellbare polymerisate.

Legal Events

Date Code Title Description
ML Lapse due to non-payment of fees