GB950082A - The manufacture of silicon-iron having cubic texture - Google Patents
The manufacture of silicon-iron having cubic textureInfo
- Publication number
- GB950082A GB950082A GB18345/60A GB1834560A GB950082A GB 950082 A GB950082 A GB 950082A GB 18345/60 A GB18345/60 A GB 18345/60A GB 1834560 A GB1834560 A GB 1834560A GB 950082 A GB950082 A GB 950082A
- Authority
- GB
- United Kingdom
- Prior art keywords
- hydrogen
- silicon
- atmosphere
- iron
- annealed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XWHPIFXRKKHEKR-UHFFFAOYSA-N iron silicon Chemical compound [Si].[Fe] XWHPIFXRKKHEKR-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000001953 recrystallisation Methods 0.000 abstract 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 3
- 239000001257 hydrogen Substances 0.000 abstract 3
- 229910052739 hydrogen Inorganic materials 0.000 abstract 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 abstract 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 2
- 239000005864 Sulphur Substances 0.000 abstract 2
- 229910052799 carbon Inorganic materials 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 abstract 1
- 229910000676 Si alloy Inorganic materials 0.000 abstract 1
- 238000000137 annealing Methods 0.000 abstract 1
- 229910052786 argon Inorganic materials 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000001307 helium Substances 0.000 abstract 1
- 229910052734 helium Inorganic materials 0.000 abstract 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 abstract 1
- -1 hydrogen sulphide Chemical class 0.000 abstract 1
- 239000000395 magnesium oxide Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 239000010703 silicon Substances 0.000 abstract 1
- 238000011282 treatment Methods 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B3/00—Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
- B21B3/02—Rolling special iron alloys, e.g. stainless steel
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/12—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
- C21D8/1216—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the working step(s) being of interest
- C21D8/1233—Cold rolling
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/74—Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
- C21D1/76—Adjusting the composition of the atmosphere
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/12—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
- C21D8/1244—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest
- C21D8/1255—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest with diffusion of elements, e.g. decarburising, nitriding
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/12—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
- C21D8/1244—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest
- C21D8/1261—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest following hot rolling
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/12—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
- C21D8/1244—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest
- C21D8/1266—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest between cold rolling steps
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/12—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
- C21D8/1244—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest
- C21D8/1272—Final recrystallisation annealing
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Electromagnetism (AREA)
- Manufacturing Of Steel Electrode Plates (AREA)
- Metal Rolling (AREA)
- Heat Treatment Of Sheet Steel (AREA)
- Soft Magnetic Materials (AREA)
- Developing Agents For Electrophotography (AREA)
Abstract
In a process for the development of cubic texture in iron-silicon alloys containing 2.5-4% of silicon, the material is hot-rolled to an intermediate gauge, annealed, e.g. at 1400-1800 DEG F., cold rolled with a reduction of 55-80%, annealed in hydrogen in the temperature range 2200-2350 DEG F. whereby the carbon content is reduced, and then given a cold reduction of 75-90% to final size. The sheet is then given a primary recrystallization anneal either box or continuously in the range 1300-1700 DEG F. followed by secondary recrystallization at 1900-2300 DEG F.; these two treatments may be combined, primary recrystallization occurring during heating to the secondary recrystallization temperature. The final heat-treatment is preferably carried out in an atmosphere of hydrogen or a non-reactive gas such as argon or helium, the atmosphere containing a small amount of a highly-polar compound such as hydrogen sulphide, oxides of sulphur or oxides of carbon or mixtures of these. As exemplified an annealing separator of magnesia containing a small amount of sulphur is used in a hydrogen atmosphere.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US81958959A | 1959-06-11 | 1959-06-11 | |
| US145540A US3130094A (en) | 1959-06-11 | 1961-10-13 | Manufacture of silicon-iron having cubic texture |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB950082A true GB950082A (en) | 1964-02-19 |
Family
ID=26843076
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB18345/60A Expired GB950082A (en) | 1959-06-11 | 1960-05-24 | The manufacture of silicon-iron having cubic texture |
| GB35311/62A Expired GB974686A (en) | 1959-06-11 | 1962-09-17 | The manufacture of silicon-iron having cube-on-face texture |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB35311/62A Expired GB974686A (en) | 1959-06-11 | 1962-09-17 | The manufacture of silicon-iron having cube-on-face texture |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3130094A (en) |
| BE (1) | BE622386A (en) |
| CH (2) | CH432566A (en) |
| DE (2) | DE1277287B (en) |
| FR (1) | FR1272943A (en) |
| GB (2) | GB950082A (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3333992A (en) * | 1964-06-29 | 1967-08-01 | Armco Steel Corp | Production of oriented silicon-iron using grain growth inhibitor during primary recrystallization heat treatment |
| US3333993A (en) * | 1965-04-02 | 1967-08-01 | Armco Steel Corp | Production of thin, oriented siliconiron wherein grain growth inhibitor is added to primary recrystallization heat treatment atmosphere as function of mn content and final thickness |
| FR2007129A1 (en) * | 1968-04-27 | 1970-01-02 | Yawata Iron & Steel Co | |
| US3640780A (en) * | 1970-06-25 | 1972-02-08 | United States Steel Corp | Method of producing electrical sheet steel with cube texture |
| US3892605A (en) * | 1972-02-22 | 1975-07-01 | Westinghouse Electric Corp | Method of producing primary recrystallized textured iron alloy member having an open gamma loop |
| BE795763A (en) * | 1972-02-22 | 1973-08-22 | Westinghouse Electric Corp | FERROUS ALLOYS AND METHODS FOR MAKING SUCH ALLOYS |
| US3789647A (en) * | 1972-10-20 | 1974-02-05 | United States Steel Corp | Method of surface-conditioning heat-treating-furnace hearth rolls having sleeves of rebonded fused silica thereon by processing silicon steel strip |
| JPS51151215A (en) * | 1975-06-21 | 1976-12-25 | Kawasaki Steel Corp | Process for manufacturing non-oriented silicon steel plate with low co re loss and high magnetic flux density |
| CA1202549A (en) * | 1982-07-19 | 1986-04-01 | Robert F. Miller | Method for producing cube-on-edge oriented silicon steel |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2307391A (en) * | 1938-10-14 | 1943-01-05 | American Rolling Mill Co | Art of producing magnetic material |
| US2303343A (en) * | 1941-01-14 | 1942-12-01 | Carnegie Illinois Steel Corp | Silicon steel electrical strip |
| US2473156A (en) * | 1944-11-16 | 1949-06-14 | Armco Steel Corp | Process for developing high magnetic permeability and low core loss in very thin silicon steel |
| US2599340A (en) * | 1948-10-21 | 1952-06-03 | Armco Steel Corp | Process of increasing the permeability of oriented silicon steels |
| DE1009214B (en) * | 1954-03-27 | 1957-05-29 | Ver Deutsche Metallwerke Ag | Process for creating a distinctive cube texture in magnetizable strips and sheets made of iron alloys containing silicon and / or aluminum |
| US2992952A (en) * | 1955-12-01 | 1961-07-18 | Vacuumschmelze Ag | Method of manufacturing magnetic sheets |
-
0
- BE BE622386D patent/BE622386A/xx unknown
-
1960
- 1960-05-24 GB GB18345/60A patent/GB950082A/en not_active Expired
- 1960-05-25 FR FR828311A patent/FR1272943A/en not_active Expired
- 1960-06-10 DE DEA34859A patent/DE1277287B/en active Pending
- 1960-06-11 CH CH667660A patent/CH432566A/en unknown
-
1961
- 1961-10-13 US US145540A patent/US3130094A/en not_active Expired - Lifetime
-
1962
- 1962-09-17 GB GB35311/62A patent/GB974686A/en not_active Expired
- 1962-10-08 CH CH1179262A patent/CH485857A/en unknown
- 1962-10-11 DE DEA41362A patent/DE1293180B/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| DE1277287B (en) | 1968-09-12 |
| CH432566A (en) | 1967-03-31 |
| GB974686A (en) | 1964-11-11 |
| FR1272943A (en) | 1961-10-06 |
| CH485857A (en) | 1970-02-15 |
| US3130094A (en) | 1964-04-21 |
| BE622386A (en) | |
| DE1293180B (en) | 1969-04-24 |
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