GB910220A - Process for refining alkyl sulphochlorides - Google Patents
Process for refining alkyl sulphochloridesInfo
- Publication number
- GB910220A GB910220A GB2865161A GB2865161A GB910220A GB 910220 A GB910220 A GB 910220A GB 2865161 A GB2865161 A GB 2865161A GB 2865161 A GB2865161 A GB 2865161A GB 910220 A GB910220 A GB 910220A
- Authority
- GB
- United Kingdom
- Prior art keywords
- mixture
- sulphochlorides
- alkyl
- refined
- refining
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/42—Separation; Purification; Stabilisation; Use of additives
- C07C303/44—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
An alkyl sulphochloride or a mixture thereof with the oil used as starting material for its production is refined by treatment with anhydrous hydrofluoric acid, e.g. at the boiling point of the HF and under appropriate excess pressure, or at 0-15 DEG C. under atmospheric pressure. In examples, hydrogenated diesel oil fractions are sulphochlorinated, the products refined with HF, and hydrolysed with caustic soda to the sulphonate or treated with a mixture of phenol and cresol to produce the corresponding sulphonic acid esters.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEF32173A DE1119855B (en) | 1960-09-22 | 1960-09-22 | Process for the purification of alkyl sulfochlorides |
Publications (1)
Publication Number | Publication Date |
---|---|
GB910220A true GB910220A (en) | 1962-11-14 |
Family
ID=7094525
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2865161A Expired GB910220A (en) | 1960-09-22 | 1961-08-08 | Process for refining alkyl sulphochlorides |
Country Status (2)
Country | Link |
---|---|
DE (1) | DE1119855B (en) |
GB (1) | GB910220A (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2748024B1 (en) * | 1996-04-24 | 1998-06-05 | Atochem Elf Sa | PROCESS FOR THE PURIFICATION OF AN ALKANESULFONYL CHLORIDE AND CORRESPONDING ACANESULFONIC ACID |
-
1960
- 1960-09-22 DE DEF32173A patent/DE1119855B/en active Pending
-
1961
- 1961-08-08 GB GB2865161A patent/GB910220A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
DE1119855B (en) | 1961-12-21 |
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