GB876038A - A process for the production of hydrazine hydrates - Google Patents
A process for the production of hydrazine hydratesInfo
- Publication number
- GB876038A GB876038A GB3468759A GB3468759A GB876038A GB 876038 A GB876038 A GB 876038A GB 3468759 A GB3468759 A GB 3468759A GB 3468759 A GB3468759 A GB 3468759A GB 876038 A GB876038 A GB 876038A
- Authority
- GB
- United Kingdom
- Prior art keywords
- sulphate
- amount
- metal
- separation
- alkaline earth
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/16—Hydrazine; Salts thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Hydrazine hydrate is prepared by reaction of an aqueous solution of di-hydrazine sulphate with an amount of an alkali metal or alkaline earth metal hydroxide, or alkaline earth metal oxide, ranging between 100-150% of the amount stoichiometrically equivalent to the sulphate, followed by the addition of a water-soluble organic liquid in amount 20-500% of the total water present at 15-100 DEG C., separation of the resulting metal sulphate, and working up of the remaining solution by distillation. The use of sodium and potassium hydroxides in the form of 40-45% aqueous solutions and of calcium hydroxide or oxide is referred to. The organic liquid may be a readily volatile, aliphatic alcohol, e.g. methyl, ethyl, or propyl alcohols, and dioxane. Prior to separation of the metal sulphate, the reaction mixture may be cooled to 20-30 DEG C.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF26797A DE1087119B (en) | 1958-10-13 | 1958-10-13 | Manufacture of hydrazine hydrate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB876038A true GB876038A (en) | 1961-08-30 |
Family
ID=7092168
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3468759A Expired GB876038A (en) | 1958-10-13 | 1959-10-13 | A process for the production of hydrazine hydrates |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE583504A (en) |
| DE (1) | DE1087119B (en) |
| FR (1) | FR1244517A (en) |
| GB (1) | GB876038A (en) |
-
1958
- 1958-10-13 DE DEF26797A patent/DE1087119B/en active Pending
-
1959
- 1959-10-12 FR FR807231A patent/FR1244517A/en not_active Expired
- 1959-10-12 BE BE583504A patent/BE583504A/en unknown
- 1959-10-13 GB GB3468759A patent/GB876038A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| BE583504A (en) | 1960-02-01 |
| DE1087119B (en) | 1960-08-18 |
| FR1244517A (en) | 1960-10-28 |
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