GB862497A - A process for the manufacture of hydrogen peroxide - Google Patents
A process for the manufacture of hydrogen peroxideInfo
- Publication number
- GB862497A GB862497A GB2074158A GB2074158A GB862497A GB 862497 A GB862497 A GB 862497A GB 2074158 A GB2074158 A GB 2074158A GB 2074158 A GB2074158 A GB 2074158A GB 862497 A GB862497 A GB 862497A
- Authority
- GB
- United Kingdom
- Prior art keywords
- alkyl
- mixture
- benzene
- peracid
- hydrogen peroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
Abstract
In the process of Specifications 747,190 and the parent Specification for producing hydrogen peroxide involving successive reduction and oxidation of a solution of an alkylated anthraquinone in a mixture of an aliphatic ester of cyclohexanol or of an alkylcyclohexanol. e.g. methyl cyclohexanol acetate, and one or more alkyl-substituted benzenes containing one or more alkyl e.g. methyl or ethyl, groups, the alkyl benzene is purified by treatment with an aliphatic peracid in liquid phase before incorporation into the mixture. The alkyl benzenes may be petroleum fractions containing a mixture of xylene isomers, or containing 50% mesitylene (1 : 3 : 5) and 1 : 3 : 4 trimethyl benzene. The peracid should contain not more than 4C atoms, and is preferably generated in situ, and the reaction products should be separated before addition to the solvent mixture. H.COCH is added to the alkyl benzene and then H2O2 and the reaction with the resulting performic acid may be 3-6 hours with constant stirring at, say, 30-50 DEG C.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2074158A GB862497A (en) | 1958-06-27 | 1958-06-27 | A process for the manufacture of hydrogen peroxide |
| ES0250670A ES250670A1 (en) | 1958-06-27 | 1959-06-26 | A process for the manufacture of hydrogen peroxide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2074158A GB862497A (en) | 1958-06-27 | 1958-06-27 | A process for the manufacture of hydrogen peroxide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB862497A true GB862497A (en) | 1961-03-08 |
Family
ID=10150880
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2074158A Expired GB862497A (en) | 1958-06-27 | 1958-06-27 | A process for the manufacture of hydrogen peroxide |
Country Status (2)
| Country | Link |
|---|---|
| ES (1) | ES250670A1 (en) |
| GB (1) | GB862497A (en) |
-
1958
- 1958-06-27 GB GB2074158A patent/GB862497A/en not_active Expired
-
1959
- 1959-06-26 ES ES0250670A patent/ES250670A1/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| ES250670A1 (en) | 1959-12-16 |
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