GB1023856A - Method for purifying aqueous solutions of methylbutynol - Google Patents
Method for purifying aqueous solutions of methylbutynolInfo
- Publication number
- GB1023856A GB1023856A GB33842/63A GB3384263A GB1023856A GB 1023856 A GB1023856 A GB 1023856A GB 33842/63 A GB33842/63 A GB 33842/63A GB 3384263 A GB3384263 A GB 3384263A GB 1023856 A GB1023856 A GB 1023856A
- Authority
- GB
- United Kingdom
- Prior art keywords
- aqueous solutions
- methylbutynol
- purifying aqueous
- butyn
- acetone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C33/00—Unsaturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C33/02—Acyclic alcohols with carbon-to-carbon double bonds
- C07C33/025—Acyclic alcohols with carbon-to-carbon double bonds with only one double bond
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/07—Optical isomers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Acetone, present in amounts of up to 6% by weight, is removed from aqueous solutions of 2-methyl-3-butyn-2-ol by azeotropic distillation with benzene to give pure 2-methyl-3-butyn-2-ol. The process is applicable to the aqueous solutions of methylbutynol obtained by the reaction of acetone and acetylene. Examples are provided.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT1760762 | 1962-09-04 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1023856A true GB1023856A (en) | 1966-03-30 |
Family
ID=11150496
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB33842/63A Expired GB1023856A (en) | 1962-09-04 | 1963-08-27 | Method for purifying aqueous solutions of methylbutynol |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1023856A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014009452A1 (en) | 2012-07-11 | 2014-01-16 | Lonza Ltd | Process for the production of methylbutinol |
CN108299161A (en) * | 2018-03-30 | 2018-07-20 | 西南化工研究设计院有限公司 | A kind of method and entrainer removing water in 2- methyl -3- butyne-2-alcohols |
-
1963
- 1963-08-27 GB GB33842/63A patent/GB1023856A/en not_active Expired
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014009452A1 (en) | 2012-07-11 | 2014-01-16 | Lonza Ltd | Process for the production of methylbutinol |
CN104470879A (en) * | 2012-07-11 | 2015-03-25 | 隆萨有限公司 | Process for the production of methylbutinol |
US9284243B2 (en) | 2012-07-11 | 2016-03-15 | Lonza Ltd | Process for the production of methylbutynol |
CN104470879B (en) * | 2012-07-11 | 2017-03-22 | 隆萨有限公司 | Process for the production of methylbutinol |
EA026542B1 (en) * | 2012-07-11 | 2017-04-28 | Лонца Лтд. | Process for producing and purifying methylbutinol |
AU2013288761B2 (en) * | 2012-07-11 | 2017-08-31 | Lonza Ltd | Process for the production of methylbutynol |
CN108299161A (en) * | 2018-03-30 | 2018-07-20 | 西南化工研究设计院有限公司 | A kind of method and entrainer removing water in 2- methyl -3- butyne-2-alcohols |
CN108299161B (en) * | 2018-03-30 | 2020-05-19 | 西南化工研究设计院有限公司 | Method for removing water in 2-methyl-3-butyne-2-alcohol and entrainer |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
GB1017605A (en) | Improvements in or relating to the preparation of dialkyl terephthalates | |
GB1023856A (en) | Method for purifying aqueous solutions of methylbutynol | |
GB879728A (en) | Process for the manufacture of isoprene from 4.4-dimethylmetadioxane | |
GB990612A (en) | A process for purifying aliphatic glycols | |
GB1059669A (en) | Process for purifying propylene oxide contaminated with methyl formate | |
ES252830A1 (en) | Production of 2, 3-dihydropyran | |
GB961174A (en) | Process of purifying crude ethylenediamine | |
GB1064276A (en) | Improvements in or relating to vinyl fluoride production | |
GB723454A (en) | Improvements in or relating to the manufacture of hydroquinone | |
GB961387A (en) | Process for the preparation of 2-cyano-4-nitrostilbenes | |
GB951294A (en) | Improved process for the recovery of cyclohexane | |
GB889649A (en) | Process for the bromination of acetylene | |
GB910130A (en) | Diphenylamine purification process | |
CA521086A (en) | Process for the treatment of liquors to recover potassium and magnesium values | |
CA593722A (en) | Process for catalyzed abnormal addition of hydrogen sulfide to unsaturated compounds | |
ES263590A1 (en) | A concentrated acetylene purification procedure (Machine-translation by Google Translate, not legally binding) | |
GB976831A (en) | The manufacture of zeaxanthin dimethyl ether and 15,15-dehydro-zeaxanthin dimethyl ether | |
AU254059B2 (en) | Improved carbon blackand process of producing same | |
GB1004936A (en) | Process for the manufacture of 2:2:2-trifluoro-1-chloro-1-bromethane | |
GB857932A (en) | Improvements relating to methods for the purification of acetylene obtained by the cracking of gaseous hydrocarbons | |
AU247850B2 (en) | Process forthe manufacture of acetylene by electropyrolysis | |
AU242409B2 (en) | Process of producing, separating and recovering' reaction products from bark and products so obtained | |
AU6366760A (en) | Improved carbon blackand process of producing same | |
GB993299A (en) | Process for the preparation of ninhydrin | |
FR1286111A (en) | Process for the production of gas mixtures containing acetylene |