GB859643A - Process for the preparation of lactone adducts and polyesters - Google Patents
Process for the preparation of lactone adducts and polyestersInfo
- Publication number
- GB859643A GB859643A GB1216357A GB1216357A GB859643A GB 859643 A GB859643 A GB 859643A GB 1216357 A GB1216357 A GB 1216357A GB 1216357 A GB1216357 A GB 1216357A GB 859643 A GB859643 A GB 859643A
- Authority
- GB
- United Kingdom
- Prior art keywords
- lactone
- compound
- epsilon
- methanol
- caprolactone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000002596 lactones Chemical class 0.000 title abstract 10
- 229920000728 polyester Polymers 0.000 title abstract 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 18
- 150000001875 compounds Chemical class 0.000 abstract 8
- -1 cycloaliphatic Chemical group 0.000 abstract 6
- 239000003054 catalyst Substances 0.000 abstract 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 5
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 abstract 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
- 125000001931 aliphatic group Chemical group 0.000 abstract 4
- 125000003118 aryl group Chemical group 0.000 abstract 4
- 125000004432 carbon atom Chemical group C* 0.000 abstract 4
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract 4
- 239000001117 sulphuric acid Substances 0.000 abstract 4
- 235000011149 sulphuric acid Nutrition 0.000 abstract 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 3
- 238000006243 chemical reaction Methods 0.000 abstract 3
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 3
- 239000003999 initiator Substances 0.000 abstract 3
- 239000000047 product Substances 0.000 abstract 3
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 abstract 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- 238000005727 Friedel-Crafts reaction Methods 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 abstract 2
- 150000007513 acids Chemical class 0.000 abstract 2
- 230000001476 alcoholic effect Effects 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 2
- 229910052799 carbon Inorganic materials 0.000 abstract 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 abstract 2
- 125000000753 cycloalkyl group Chemical group 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 2
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- YDJZXHZRXDLCEH-UHFFFAOYSA-N methyl 6-hydroxyhexanoate Chemical compound COC(=O)CCCCCO YDJZXHZRXDLCEH-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 150000002894 organic compounds Chemical class 0.000 abstract 2
- 125000001424 substituent group Chemical group 0.000 abstract 2
- SHDLPQHFZRTKBH-UHFFFAOYSA-N 4,4,6-trimethyloxepan-2-one Chemical compound CC1COC(=O)CC(C)(C)C1 SHDLPQHFZRTKBH-UHFFFAOYSA-N 0.000 abstract 1
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical group CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 abstract 1
- 239000004952 Polyamide Substances 0.000 abstract 1
- AWMVMTVKBNGEAK-UHFFFAOYSA-N Styrene oxide Chemical class C1OC1C1=CC=CC=C1 AWMVMTVKBNGEAK-UHFFFAOYSA-N 0.000 abstract 1
- 229920002433 Vinyl chloride-vinyl acetate copolymer Polymers 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 1
- 125000003368 amide group Chemical group 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- PPQMBAHKDFJCGO-UHFFFAOYSA-N amino-oxo-(2-sulfanyl-2-sulfinosulfonylhydrazinyl)methane Chemical compound N(C(=O)N)N(S(=O)(=O)S(=O)O)S PPQMBAHKDFJCGO-UHFFFAOYSA-N 0.000 abstract 1
- 239000003957 anion exchange resin Substances 0.000 abstract 1
- 125000003710 aryl alkyl group Chemical group 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 125000000623 heterocyclic group Chemical group 0.000 abstract 1
- 125000000717 hydrazino group Chemical group [H]N([*])N([H])[H] 0.000 abstract 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 abstract 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- GRVDJDISBSALJP-UHFFFAOYSA-N methyloxidanyl Chemical compound [O]C GRVDJDISBSALJP-UHFFFAOYSA-N 0.000 abstract 1
- 238000006386 neutralization reaction Methods 0.000 abstract 1
- 239000004014 plasticizer Substances 0.000 abstract 1
- 229920002647 polyamide Polymers 0.000 abstract 1
- 238000006068 polycondensation reaction Methods 0.000 abstract 1
- 229920001228 polyisocyanate Polymers 0.000 abstract 1
- 239000005056 polyisocyanate Substances 0.000 abstract 1
- 239000004814 polyurethane Substances 0.000 abstract 1
- 229920002635 polyurethane Polymers 0.000 abstract 1
- 238000007086 side reaction Methods 0.000 abstract 1
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M3/00—Liquid compositions essentially based on lubricating components other than mineral lubricating oils or fatty oils and their use as lubricants; Use as lubricants of single liquid substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/50—Polyethers having heteroatoms other than oxygen
- C08G18/5021—Polyethers having heteroatoms other than oxygen having nitrogen
- C08G18/5033—Polyethers having heteroatoms other than oxygen having nitrogen containing carbocyclic groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/62—Alcohols or phenols
- C08G59/64—Amino alcohols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2101/00—Manufacture of cellular products
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant Compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant Compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/067—Polyaryl amine alkanes
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/02—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Polyurethanes Or Polyureas (AREA)
- Polyesters Or Polycarbonates (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyethers (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US577953A US2914556A (en) | 1956-04-13 | 1956-04-13 | Preparation of lactone adducts |
| US85424459A | 1959-11-20 | 1959-11-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB859643A true GB859643A (en) | 1961-01-25 |
Family
ID=27077387
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1216357A Expired GB859643A (en) | 1956-04-13 | 1957-04-15 | Process for the preparation of lactone adducts and polyesters |
| GB3946160A Expired GB967359A (en) | 1956-04-13 | 1960-11-17 | Improvements in and relating to foamed polymers |
| GB3946060A Expired GB910333A (en) | 1956-04-13 | 1960-11-17 | Improvements in and relating to polymers |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3946160A Expired GB967359A (en) | 1956-04-13 | 1960-11-17 | Improvements in and relating to foamed polymers |
| GB3946060A Expired GB910333A (en) | 1956-04-13 | 1960-11-17 | Improvements in and relating to polymers |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE556560A (enrdf_load_stackoverflow) |
| DE (3) | DE1213995B (enrdf_load_stackoverflow) |
| GB (3) | GB859643A (enrdf_load_stackoverflow) |
| IT (1) | IT570070A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4393199A (en) | 1981-05-12 | 1983-07-12 | S R I International | Cationic polymerization |
| CN116284735A (zh) * | 2023-05-04 | 2023-06-23 | 辽宁奥克药业股份有限公司 | 一种制备嵌段聚醚的催化剂、嵌段聚醚的制备方法 |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3314995A (en) * | 1963-12-09 | 1967-04-18 | Mobay Chemical Corp | Alkylene oxide adducts of bis(2, 4-diamino-5-methyl phenyl)methane |
| NL133349C (enrdf_load_stackoverflow) * | 1963-12-30 | |||
| US3293297A (en) * | 1964-07-30 | 1966-12-20 | Universal Oil Prod Co | Nu-oxyalkylated-aminediphenyl-oxo-and amino-compounds |
| DE2015252C3 (de) * | 1969-04-01 | 1982-10-07 | Union Carbide Corp., 06817 Danbury, Conn. | Schwundarm aushärtbare Polyesterharzmasse |
| US3948825A (en) * | 1974-07-05 | 1976-04-06 | Basf Wyandotte Corporation | Curing agent for use in making cellular polyurethane compositions |
| US4379914A (en) * | 1981-12-21 | 1983-04-12 | Exxon Research And Engineering Co. | Polycaprolactone polymers |
| CN113015783B (zh) * | 2018-12-13 | 2024-07-05 | 陶氏环球技术有限责任公司 | 清洁助剂 |
| EP3894533B1 (en) * | 2018-12-13 | 2022-12-28 | Dow Global Technologies LLC | Liquid laundry detergent formulation |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR956245A (enrdf_load_stackoverflow) * | 1942-12-24 | 1950-01-27 | ||
| DE878857C (de) * | 1943-06-26 | 1953-06-08 | Basf Ag | Verfahren zur Herstellung von Kondensationsprodukten |
| DE861609C (de) * | 1943-07-14 | 1953-01-05 | Basf Ag | Verfahren zur Herstellung hochmolekularer Kondensationsprodukte |
| GB776661A (en) * | 1954-01-28 | 1957-06-12 | Wyandotte Chemical Corp | Improved polyoxypropylene-polyoxyalkylene surface-active agents |
| NL99836C (enrdf_load_stackoverflow) * | 1954-10-20 | |||
| DE961573C (de) * | 1954-11-16 | 1957-04-11 | Bayer Ag | Verfahren zur Herstellung von Schaumstoffen aus hydroxylgruppen- haltigen linearen oder verzweigten Polyaethern oder Polythioaethern und Polyisocyanaten |
-
0
- IT IT570070D patent/IT570070A/it unknown
- BE BE556560D patent/BE556560A/xx unknown
-
1957
- 1957-04-09 DE DEU4474A patent/DE1213995B/de active Pending
- 1957-04-15 GB GB1216357A patent/GB859643A/en not_active Expired
-
1960
- 1960-11-14 DE DEU7577A patent/DE1151938B/de active Pending
- 1960-11-16 DE DEU7586A patent/DE1191098B/de active Pending
- 1960-11-17 GB GB3946160A patent/GB967359A/en not_active Expired
- 1960-11-17 GB GB3946060A patent/GB910333A/en not_active Expired
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4393199A (en) | 1981-05-12 | 1983-07-12 | S R I International | Cationic polymerization |
| CN116284735A (zh) * | 2023-05-04 | 2023-06-23 | 辽宁奥克药业股份有限公司 | 一种制备嵌段聚醚的催化剂、嵌段聚醚的制备方法 |
| CN116284735B (zh) * | 2023-05-04 | 2023-12-29 | 辽宁奥克药业股份有限公司 | 一种制备嵌段聚醚的催化剂、嵌段聚醚的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1151938B (de) | 1963-07-25 |
| GB967359A (en) | 1964-08-19 |
| DE1191098B (de) | 1965-04-15 |
| GB910333A (en) | 1962-11-14 |
| IT570070A (enrdf_load_stackoverflow) | |
| DE1213995B (de) | 1966-04-07 |
| BE556560A (enrdf_load_stackoverflow) |
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