GB658616A - A process for the production of fine non-coherent powders containing surface-active substances - Google Patents
A process for the production of fine non-coherent powders containing surface-active substancesInfo
- Publication number
- GB658616A GB658616A GB8133/48A GB813348A GB658616A GB 658616 A GB658616 A GB 658616A GB 8133/48 A GB8133/48 A GB 8133/48A GB 813348 A GB813348 A GB 813348A GB 658616 A GB658616 A GB 658616A
- Authority
- GB
- United Kingdom
- Prior art keywords
- alkyl
- substances
- sodium sulphate
- bentonite
- talc
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000843 powder Substances 0.000 title abstract 9
- 238000000034 method Methods 0.000 title abstract 7
- 239000013543 active substance Substances 0.000 title abstract 6
- 230000001427 coherent effect Effects 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 18
- 239000000126 substance Substances 0.000 abstract 12
- 229910052938 sodium sulfate Inorganic materials 0.000 abstract 9
- 235000011152 sodium sulphate Nutrition 0.000 abstract 9
- -1 ester salt Chemical class 0.000 abstract 7
- 239000000440 bentonite Substances 0.000 abstract 6
- 229910000278 bentonite Inorganic materials 0.000 abstract 6
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 abstract 6
- 239000000203 mixture Substances 0.000 abstract 6
- 239000001117 sulphuric acid Substances 0.000 abstract 6
- 235000011149 sulphuric acid Nutrition 0.000 abstract 6
- 239000000454 talc Substances 0.000 abstract 6
- 229910052623 talc Inorganic materials 0.000 abstract 6
- 150000003839 salts Chemical class 0.000 abstract 5
- OXLXSOPFNVKUMU-UHFFFAOYSA-N 1,4-dioctoxy-1,4-dioxobutane-2-sulfonic acid Chemical compound CCCCCCCCOC(=O)CC(S(O)(=O)=O)C(=O)OCCCCCCCC OXLXSOPFNVKUMU-UHFFFAOYSA-N 0.000 abstract 3
- 239000005995 Aluminium silicate Substances 0.000 abstract 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 3
- 229910019142 PO4 Inorganic materials 0.000 abstract 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 3
- 229910052783 alkali metal Inorganic materials 0.000 abstract 3
- 150000001340 alkali metals Chemical class 0.000 abstract 3
- 125000000217 alkyl group Chemical group 0.000 abstract 3
- 235000012211 aluminium silicate Nutrition 0.000 abstract 3
- 235000019270 ammonium chloride Nutrition 0.000 abstract 3
- 235000019289 ammonium phosphates Nutrition 0.000 abstract 3
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical class N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 abstract 3
- 235000011130 ammonium sulphate Nutrition 0.000 abstract 3
- 235000012216 bentonite Nutrition 0.000 abstract 3
- 150000003841 chloride salts Chemical class 0.000 abstract 3
- 238000001035 drying Methods 0.000 abstract 3
- 238000007689 inspection Methods 0.000 abstract 3
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 abstract 3
- 239000002245 particle Substances 0.000 abstract 3
- 150000003013 phosphoric acid derivatives Chemical class 0.000 abstract 3
- 229910052708 sodium Inorganic materials 0.000 abstract 3
- 239000011734 sodium Substances 0.000 abstract 3
- 159000000000 sodium salts Chemical class 0.000 abstract 3
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 3
- 235000012222 talc Nutrition 0.000 abstract 3
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 abstract 2
- 239000011149 active material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21C—MANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
- B21C1/00—Manufacture of metal sheets, metal wire, metal rods, metal tubes by drawing
- B21C1/16—Metal drawing by machines or apparatus in which the drawing action is effected by other means than drums, e.g. by a longitudinally-moved carriage pulling or pushing the work or stock for making metal sheets, bars, or tubes
- B21C1/27—Carriages; Drives
- B21C1/30—Drives, e.g. carriage-traversing mechanisms; Driving elements, e.g. drawing chains; Controlling the drive
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B60—VEHICLES IN GENERAL
- B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
- B60C9/00—Reinforcements or ply arrangement of pneumatic tyres
- B60C9/02—Carcasses
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B60—VEHICLES IN GENERAL
- B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
- B60C9/00—Reinforcements or ply arrangement of pneumatic tyres
- B60C9/02—Carcasses
- B60C9/04—Carcasses the reinforcing cords of each carcass ply arranged in a substantially parallel relationship
- B60C9/08—Carcasses the reinforcing cords of each carcass ply arranged in a substantially parallel relationship the cords extend transversely from bead to bead, i.e. radial ply
- B60C9/09—Carcasses the reinforcing cords of each carcass ply arranged in a substantially parallel relationship the cords extend transversely from bead to bead, i.e. radial ply combined with other carcass plies having cords extending diagonally from bead to bead, i.e. combined radial ply and bias angle ply
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B60—VEHICLES IN GENERAL
- B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
- B60C9/00—Reinforcements or ply arrangement of pneumatic tyres
- B60C9/02—Carcasses
- B60C9/16—Carcasses built-up with metallic reinforcing inlays
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B60—VEHICLES IN GENERAL
- B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
- B60C9/00—Reinforcements or ply arrangement of pneumatic tyres
- B60C9/18—Structure or arrangement of belts or breakers, crown-reinforcing or cushioning layers
- B60C9/28—Structure or arrangement of belts or breakers, crown-reinforcing or cushioning layers characterised by the belt or breaker dimensions or curvature relative to carcass
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
- C11D3/126—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Paper (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
A process for the production of surface-active compositions in the form of fine, non-coherent powders starting from dry or substantially dry surface-active substances which are secondary sulphuric acid alkyl ester salts, or mixtures thereof with inorganic salts, the particles of which substances display a tendency to stick together, comprises grinding these substances in the presence of a substance added to them which in finely-divided condition shows no or only little tendency to stick together. The substance to be added may be alkali metal or ammonium sulphates, phosphates or chlorides, or talc, kaolin or bentonite, but anhydrous sodium sulphate is preferred. In an example a dry powder containing 60 per cent of ester salt and 40 per cent of sodium sulphate, formed by atomization-drying of an aqueous secondary sodium alkyl sulphate solution, is ground with an equal quantity of sodium sulphate. The Specification as open to inspection under Sect. 91 comprises also the use of the process with other surface-active substances such as primary sulphuric acid ester salts, alkyl sulphonates, alkyl aryl sulphonates and sulpho-succinic acid ester salts. In an example, sodium salt of sulpho-succinic acid di-octyl ester is ground together with bentonite or talc. This subject-matter does not appear in the Specification as accepted.ALSO:A process for the production of surface-active compositions in the form of fine, non-coherent powders starting from dry or substantially dry surface-active substances which are secondary sulphuric acid alkyl ester salts, or mixtures thereof with inorganic salts, the particles of which substances display a tendency to stick together, comprises grinding these substances in the presence of a substance added to them which in finely-divided condition shows no or only little tendency to stick together. The substance to be added may be alkali metal or ammonium sulphates, phosphates or chlorides, or talc, kaolin or bentonite, but anhydrous sodium sulphate powder is preferred. In an example given, a dry powder containing 60 per cent of ester salt and 4 per cent of sodium sulphate, formed by atomization-drying of an aqueous secondary sodium alkyl sulphate solution, is ground with an equal quantity of sodium sulphate. The Specification as open to inspection under Sect. 91 comprises also the use of the process with other surface-active material such as primary sulphuric acid ester salts, alkyl sulphonates, alkyl aryl sulphonates and sulphosuccinic acid ester salts. A further example is given in which the sodium salt of sulphosuccinic acid di-octyl ester is ground with bentonite or talc. This subject-matter does not appear in the Specification as accepted.ALSO:A process for the production of surfaceactive compositions in the form of fine, non-coherent powders starting from dry or substantially dry surface-active substances which are secondary sulphuric acid alkyl ester salts, or mixtures thereof with inorganic salts, the particles of which substances display a tendency to stick together comprises grinding these substances in the presence of a substance added to them which in finely divided condition shows no or only little tendency to stick together. The substance to be added may be alkali metal or ammonium sulphates, phosphates or chlorides, or talc, kaolin or bentonite, but anhydrous sodium sulphate powder is preferred. In an example given, a dry powder containing 60 per cent of ester salt and 40 per cent of sodium sulphate, formed by atomization-drying of an aqueous secondary sodium alkyl sulphate solution, is ground with an equal quantity of sodium sulphate. The Specification as open to inspection under Sect. 91 comprises also the use of the process with other surface-active substances such as primary sulphuric acid ester salts, alkyl sulphonates, alkyl aryl sulphonates and sulpho-succinic acid ester salts. In an example, sodium salt of sulpho-succinic acid di-octyl ester is ground together with bentonite or talc. This subject-matter does not appear in the Specification as accepted.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL658616X | 1947-03-21 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB658616A true GB658616A (en) | 1951-10-10 |
Family
ID=19795314
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB8133/48A Expired GB658616A (en) | 1947-03-21 | 1948-03-18 | A process for the production of fine non-coherent powders containing surface-active substances |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US2617599A (en) |
| FR (1) | FR963737A (en) |
| GB (1) | GB658616A (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2749051A (en) * | 1953-02-26 | 1956-06-05 | Dow Chemical Co | Method of compacting light powders |
| US5066511A (en) * | 1989-05-19 | 1991-11-19 | Warner-Lambert Company | Method for preparing pulverized polydextrose which is substantially free of acids and compositions containing same |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US318044A (en) * | 1885-05-19 | Process of grinding caustic soda | ||
| US1546156A (en) * | 1920-08-13 | 1925-07-14 | Welter Adolf | Process for producing finely-granulated compounds |
| US1590795A (en) * | 1924-09-22 | 1926-06-29 | Pittsburgh Plate Glass Co | Process of increasing the density of finely-divided material |
| US1968628A (en) * | 1931-07-07 | 1934-07-31 | Vanderbilt Co R T | Powdered soap product and method of preparing the same |
| GB431682A (en) * | 1933-11-15 | 1935-07-08 | Henkel & Cie Gmbh | Improvements in or relating to wetting agents and the like |
| NL48762C (en) * | 1934-08-22 | |||
| GB485649A (en) * | 1936-11-23 | 1938-05-23 | Ig Farbenindustrie Ag | Washing preparations |
| US2358418A (en) * | 1941-11-12 | 1944-09-19 | Gehl Guernsey Farms Inc | Machine and a process for making sugared milk powder |
| US2400292A (en) * | 1941-12-23 | 1946-05-14 | Harold R Dalton | Crystalline pellets and method of preparation |
| US2423451A (en) * | 1943-09-28 | 1947-07-08 | Colgate Palmolive Peet Co | Soap product and method of making same |
| US2456437A (en) * | 1943-11-24 | 1948-12-14 | Colgate Palmolive Peet Co | Nondusting soap composition and method for making same |
| US2423452A (en) * | 1944-05-05 | 1947-07-08 | Colgate Palmolive Peet Co | Process for treating sprayed dried organic detergents |
-
0
- FR FR963737D patent/FR963737A/fr not_active Expired
-
1948
- 1948-03-15 US US15055A patent/US2617599A/en not_active Expired - Lifetime
- 1948-03-18 GB GB8133/48A patent/GB658616A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US2617599A (en) | 1952-11-11 |
| FR963737A (en) | 1950-07-19 |
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