GB636399A - Manufacture of reducing agents derived from alkali sulphides and dyestuffs preparations containing them - Google Patents
Manufacture of reducing agents derived from alkali sulphides and dyestuffs preparations containing themInfo
- Publication number
- GB636399A GB636399A GB3036/47A GB303647A GB636399A GB 636399 A GB636399 A GB 636399A GB 3036/47 A GB3036/47 A GB 3036/47A GB 303647 A GB303647 A GB 303647A GB 636399 A GB636399 A GB 636399A
- Authority
- GB
- United Kingdom
- Prior art keywords
- drying
- product
- dry
- dextrin
- sulphide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/30—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using sulfur dyes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Molecular Biology (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Textile Engineering (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Detergent Compositions (AREA)
- Paper (AREA)
Abstract
Reducing agents are made by reacting a degradation product of a high molecular weight natural carbohydrate or a low molecular weight carbohydrate with an alkali sulphide in concentrated aqueous solution at a raised temperature not substantially above 108 DEG C., and drying at a temperature not substantially above 108 DEG C. A sulphur dye or its leuco-body may be incorporated dry in the dry product, or the leuco-body may be incorporated wet or dry, before or after drying of the reducing agent itself, followed by drying. The dye may be vatted with excess alkali sulphide and the carbohydrate product added, followed by drying. Carbohydrate products specified are dextrin, British gum, cane sugar, glucose, l vulose. The sulphide may be sodium sulphide or hydrosulphide. In examples: (1) dextrin, cane sugar, glucose, or l vulose is mixed with sodium sulphide fused in its own water of crystallization, followed by drying; (2) the dye obtained by sulphurizing N-p-hydroxyphenyl - N1 - o - carboxyphenyl - p - phenylene diamine is mixed dry with the product of (1), or converted to its leuco-body with sodium sulphide and the dry leuco-body mixed with the product of (1), or vatted with sodium sulphide in presence of dextrin, followed by drying only, and by drying and mixing with the product of (1). Also in examples: (3) Pyrogene Deep Black P is vatted with excess sodium sulphide and dextrin; followed by drying; (4) Pyrogene Yellow O is mixed dry with the product of (1) or vatted with sodium sulphide and dextrin. Specification 418,746 is referred to.ALSO:Reducing agents are made by reacting a degradation product of a high molecular weight natural carbohydrate or a low molecular weight carbohydrate with an alkali sulphide in concentrated aqueous solution at a raised temperature not substantially above 108 DEG C., and drying at a temperature not substantially above 108 DEG C. A sulphur dye or its leuco-body may be incorporated dry in the dry product, or the leuco-body may be incorporated wet or dry before or after drying of the reducing agent itself, followed by drying. The dye may be vatted with excess alkali sulphide and the carbohydrate product added, followed by drying. Carbohydrate products specified are dextrin, British gum, cane sugar, glucose, lacvulose. The sulphide may be sodium sulphide or hydrosulphide. In examples: (1) dextrin, cane sugar, glucose, or lacvulose is mixed with sodium sulphide fused in its own water of crystallization, followed by drying; (2) the dye obtained by sulphurizing N - p - hydroxyphenyl - N1 - o - carboxyphenyl-p-phenylene diamine is mixed dry with the product of (1), or converted to its leuco-body with sodium sulphide and the dry leuco-body mixed with the product of (1), or vatted with sodium sulphide in presence of dextrin, followed by drying only, and by drying and mixing with the product of (1). Also in examples: (3) Pyrogene Deep Black D is vatted with excess sodium sulphide and dextrin, followed by drying; (4) Pyrogene Yellow O is mixed dry with the product of (1) or vatted with sodium sulphide and dextrin. A dyeing example is also given. Specification 418,746 is referred to.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH636399X | 1946-02-01 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB636399A true GB636399A (en) | 1950-04-26 |
Family
ID=4525122
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3036/47A Expired GB636399A (en) | 1946-02-01 | 1947-01-31 | Manufacture of reducing agents derived from alkali sulphides and dyestuffs preparations containing them |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB636399A (en) |
-
1947
- 1947-01-31 GB GB3036/47A patent/GB636399A/en not_active Expired
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