GB603256A - Process of manufacture of glycol - Google Patents
Process of manufacture of glycolInfo
- Publication number
- GB603256A GB603256A GB26043/45A GB2604345A GB603256A GB 603256 A GB603256 A GB 603256A GB 26043/45 A GB26043/45 A GB 26043/45A GB 2604345 A GB2604345 A GB 2604345A GB 603256 A GB603256 A GB 603256A
- Authority
- GB
- United Kingdom
- Prior art keywords
- hydration
- ethylene oxide
- glycol
- decomposed
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
- C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
- C07C29/103—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers
- C07C29/106—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers of oxiranes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Ethylene glycol is prepared by the hydration of ethylene oxide in the presence of a trihalogenoacetic acid which is subsequently removed from the reaction product by thermal decomposition. In an example, ethylene oxide is hydrated at about 60 DEG C. in the presence of trichloroacetic acid which is subsequently decomposed into chloroform and carbon dioxide by heating at 100 DEG C., and p ethylene glycol is separated from di- and triethylene glycol by fractional distillation. The Specification as open to inspection under Sect. 91 states that the hydration may be effected in the presence of any organic acid which can be decomposed at a temperature above the hydration temperature of ethylene oxide. This subject-matter does not appear in the Specification as accepted.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BE603256X | 1942-12-24 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB603256A true GB603256A (en) | 1948-06-11 |
Family
ID=3874229
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB26043/45A Expired GB603256A (en) | 1942-12-24 | 1945-10-05 | Process of manufacture of glycol |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB603256A (en) |
-
1945
- 1945-10-05 GB GB26043/45A patent/GB603256A/en not_active Expired
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