GB1008577A - Process for the production of stable alkyl sulphonic acid ester plasticisers of low inflammability - Google Patents

Process for the production of stable alkyl sulphonic acid ester plasticisers of low inflammability

Info

Publication number
GB1008577A
GB1008577A GB24123/62A GB2412362A GB1008577A GB 1008577 A GB1008577 A GB 1008577A GB 24123/62 A GB24123/62 A GB 24123/62A GB 2412362 A GB2412362 A GB 2412362A GB 1008577 A GB1008577 A GB 1008577A
Authority
GB
United Kingdom
Prior art keywords
alkyl sulphonic
production
acid ester
sulphonic acid
aliphatic hydrocarbon
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB24123/62A
Inventor
Kurt Spohn
Hans-Geor Rosenkranz
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Leuna Werke GmbH
Leuna Werke Walter Ulbright Germany VEB
Original Assignee
Leuna Werke GmbH
Leuna Werke Walter Ulbright Germany VEB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Leuna Werke GmbH, Leuna Werke Walter Ulbright Germany VEB filed Critical Leuna Werke GmbH
Priority to GB24123/62A priority Critical patent/GB1008577A/en
Publication of GB1008577A publication Critical patent/GB1008577A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/26—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids
    • C07C303/28—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids by reaction of hydroxy compounds with sulfonic acids or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
    • C08K5/41—Compounds containing sulfur bound to oxygen
    • C08K5/42—Sulfonic acids; Derivatives thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Alkyl sulphonic esters relatively free from unsaponifiable higher n-paraffins and of low volatility are prepared by subjecting saturated aliphatic hydrocarbon mixtures within the selected B.P. range of 235 DEG to 305 DEG C. to a partial sulphochlorination process until a hydrolysable chlorine content of up to 7% by weight based on the weight of the resulting product has been reached, and reacting the resulting product with phenols, chlorinated phenols or alcohols in the presence of a dilute solution of an alkali metal hydroxide, ammonia or amines at temperatures below 100 DEG C., and recovering the ester by known means. The preferred saturated aliphatic hydrocarbon mixtures used are those obtained from the catalytic hydrogenation of oxides of carbon or by appropriate fractionation of petroleum. The preferred reaction temperature is not higher than 20 DEG C.
GB24123/62A 1962-06-22 1962-06-22 Process for the production of stable alkyl sulphonic acid ester plasticisers of low inflammability Expired GB1008577A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB24123/62A GB1008577A (en) 1962-06-22 1962-06-22 Process for the production of stable alkyl sulphonic acid ester plasticisers of low inflammability

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB24123/62A GB1008577A (en) 1962-06-22 1962-06-22 Process for the production of stable alkyl sulphonic acid ester plasticisers of low inflammability

Publications (1)

Publication Number Publication Date
GB1008577A true GB1008577A (en) 1965-10-27

Family

ID=10206762

Family Applications (1)

Application Number Title Priority Date Filing Date
GB24123/62A Expired GB1008577A (en) 1962-06-22 1962-06-22 Process for the production of stable alkyl sulphonic acid ester plasticisers of low inflammability

Country Status (1)

Country Link
GB (1) GB1008577A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0220485A1 (en) * 1985-10-01 1987-05-06 Bayer Ag Polyhydroxylic compounds containing sulfonic ester groups and their use as polyol compounds in casting resins
US8480937B2 (en) 2004-11-17 2013-07-09 Dimplex North America Limited Method of forming a simulated combustible fuel element

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0220485A1 (en) * 1985-10-01 1987-05-06 Bayer Ag Polyhydroxylic compounds containing sulfonic ester groups and their use as polyol compounds in casting resins
US8480937B2 (en) 2004-11-17 2013-07-09 Dimplex North America Limited Method of forming a simulated combustible fuel element

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