GB465949A - Process of preparing purified glycyrrhizine (pale glycyrrhizine) - Google Patents
Process of preparing purified glycyrrhizine (pale glycyrrhizine)Info
- Publication number
- GB465949A GB465949A GB31151/35A GB3115135A GB465949A GB 465949 A GB465949 A GB 465949A GB 31151/35 A GB31151/35 A GB 31151/35A GB 3115135 A GB3115135 A GB 3115135A GB 465949 A GB465949 A GB 465949A
- Authority
- GB
- United Kingdom
- Prior art keywords
- glycyrrhizin
- glycyrrhizine
- purified
- treated
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
- C07H15/20—Carbocyclic rings
- C07H15/24—Condensed ring systems having three or more rings
- C07H15/256—Polyterpene radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Crude glycyrrhizin as it is obtained from liquorice, is purified by treatment with an alcohol or mixture of alcohols of limited solubility in water, such as pine oil. The mixture stratifies, the upper layer being the solution of purified glycyrrhizin. The solution is treated with an adsorbent to further purify it, and may then be treated with a reducing bleaching-agent such as sodium hydrosulphite and washed with water. Dilute ammonia or alkali hydroxide is then added and the precipitated glycyrrhizin salt is separated and dried.ALSO:Crude glycyrrhizin as it is obtained from liquorice is purified by treatment with an alcohol or mixture of alcohols of limited solubility in water, such as pine oil. The mixture stratifies, the upper layer being the solution of purified glycyrrhizin. The solution is treated with an adsorbent to further purify it, and may then be treated with a reducing bleaching agent such as sodium hydrosulphite, and washed with water. Dilute ammonia or alkali hydroxide is then added, and the precipitated glycyrrhizin salt is separated and dried.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE465949X | 1934-11-10 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB465949A true GB465949A (en) | 1937-05-11 |
Family
ID=3870073
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB31151/35A Expired GB465949A (en) | 1934-11-10 | 1935-11-11 | Process of preparing purified glycyrrhizine (pale glycyrrhizine) |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB465949A (en) |
-
1935
- 1935-11-11 GB GB31151/35A patent/GB465949A/en not_active Expired
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