GB452868A - Manufacture of salts of cyclic nitrogen bases - Google Patents

Manufacture of salts of cyclic nitrogen bases

Info

Publication number
GB452868A
GB452868A GB6742/35A GB674235A GB452868A GB 452868 A GB452868 A GB 452868A GB 6742/35 A GB6742/35 A GB 6742/35A GB 674235 A GB674235 A GB 674235A GB 452868 A GB452868 A GB 452868A
Authority
GB
United Kingdom
Prior art keywords
pyrazolone
dimethyl
acid
methylamino
phenyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB6742/35A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IG Farbenindustrie AG
Original Assignee
IG Farbenindustrie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IG Farbenindustrie AG filed Critical IG Farbenindustrie AG
Publication of GB452868A publication Critical patent/GB452868A/en
Expired legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/04—Carriers or supports for textile materials to be treated
    • D06B23/042—Perforated supports
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D219/00—Heterocyclic compounds containing acridine or hydrogenated acridine ring systems
    • C07D219/04—Heterocyclic compounds containing acridine or hydrogenated acridine ring systems with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to carbon atoms of the ring system
    • C07D219/08—Nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms
    • C07D231/46—Oxygen atom in position 3 or 5 and nitrogen atom in position 4
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D453/00—Heterocyclic compounds containing quinuclidine or iso-quinuclidine ring systems, e.g. quinine alkaloids
    • C07D453/02—Heterocyclic compounds containing quinuclidine or iso-quinuclidine ring systems, e.g. quinine alkaloids containing not further condensed quinuclidine ring systems
    • C07D453/04—Heterocyclic compounds containing quinuclidine or iso-quinuclidine ring systems, e.g. quinine alkaloids containing not further condensed quinuclidine ring systems having a quinolyl-4, a substituted quinolyl-4 or a alkylenedioxy-quinolyl-4 radical linked through only one carbon atom, attached in position 2, e.g. quinine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D489/00—Heterocyclic compounds containing 4aH-8, 9 c- Iminoethano-phenanthro [4, 5-b, c, d] furan ring systems, e.g. derivatives of [4, 5-epoxy]-morphinan of the formula:
    • C07D489/02—Heterocyclic compounds containing 4aH-8, 9 c- Iminoethano-phenanthro [4, 5-b, c, d] furan ring systems, e.g. derivatives of [4, 5-epoxy]-morphinan of the formula: with oxygen atoms attached in positions 3 and 6, e.g. morphine, morphinone
    • C07D489/04—Salts; Organic complexes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatment Of Fiber Materials (AREA)
  • Springs (AREA)
  • Storage Of Web-Like Or Filamentary Materials (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)

Abstract

Salts of cyclic nitrogenous bases with w-methanesulphonic acids of pyrazolone-amines are prepared by interaction of the sulphonic acid with the base or with a salt thereof of a weak acid. The methanesulphonic acids, which are described in Specification 452,363, may be used as such or may be formed in situ. The products possess therapeutic properties. The examples describe the interaction of (1) quinine with 1 - phenyl - 2 3 - dimethyl - 4 - methylamino - 5 - pyrazolone - 4 - methanesulphonic acid in alcoholic or aqueous solution; the same product is formed when sulphur dioxide is passed into an alcoholic solution of 1-phenyl-2 : 3-dimethyl - 4 - methylamino - 5 - pyrazolone, aqueous formaldehyde and quinine; (2) morphine with 1 - phenyl - 2 : 3 - dimethyl - 4 - methylamino - 5 - pyrazolone - 4 - methanesulphonic acid in water; (3) quinine with 1 - cyclohexyl - 2 3 - dimethyl - 4 - methylamino - 5 - pyrazolone - 4 - methanesulphonic acid in acetone and ether, and with 1-phenyl-2 : 3 - dimethyl - 4 - cyclohexenylamino - 5 - pyrazolone - 4 - methanesulphonic acid in alcohol and acetone; (4) the acid carbonate of 3 : 6 - diamino - 10 - methylacridinium hydroxide, prepared by treating the corresponding acridinium chloride with sodium bicarbonate, with 1 - phenyl - 2 : 3 - dimethyl - 4 - methylamino - 5 - pyrazolone - 4 - methanesulphonic acid in alcohol. The products are recovered by crystallization or evaporation of the solvent.
GB6742/35A 1934-03-03 1935-03-04 Manufacture of salts of cyclic nitrogen bases Expired GB452868A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE452868X 1934-03-03

Publications (1)

Publication Number Publication Date
GB452868A true GB452868A (en) 1936-09-01

Family

ID=6538715

Family Applications (2)

Application Number Title Priority Date Filing Date
GB35368/34A Expired GB427953A (en) 1934-03-03 1934-12-08 Improvements in and relating to spool or cop cores for dyeing yarns on spools or cops and piece goods
GB6742/35A Expired GB452868A (en) 1934-03-03 1935-03-04 Manufacture of salts of cyclic nitrogen bases

Family Applications Before (1)

Application Number Title Priority Date Filing Date
GB35368/34A Expired GB427953A (en) 1934-03-03 1934-12-08 Improvements in and relating to spool or cop cores for dyeing yarns on spools or cops and piece goods

Country Status (4)

Country Link
BE (1) BE406692A (en)
DE (1) DE644645C (en)
FR (1) FR800070A (en)
GB (2) GB427953A (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2818222A (en) * 1953-12-08 1957-12-31 Scholl Werner Axially compressible reel for filamentary coils
DE944306C (en) * 1953-12-08 1956-06-14 Scholl A G Zofingen In the axial direction resiliently compressible lap carrier
CN109281098A (en) * 2018-08-30 2019-01-29 嘉兴奥斯卡染整有限公司 Palm sample special effect yarn hand sample dyeing creel

Also Published As

Publication number Publication date
BE406692A (en) 1935-01-31
DE644645C (en) 1937-05-10
GB427953A (en) 1935-05-02
FR800070A (en) 1936-06-26

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