GB391322A - Methods of producing active silicic acid or active mixed gels of silicic acid with metal hydroxides or metal oxides, or mixed gels of silicic acid with active carbon - Google Patents
Methods of producing active silicic acid or active mixed gels of silicic acid with metal hydroxides or metal oxides, or mixed gels of silicic acid with active carbonInfo
- Publication number
- GB391322A GB391322A GB14486/32A GB1448632A GB391322A GB 391322 A GB391322 A GB 391322A GB 14486/32 A GB14486/32 A GB 14486/32A GB 1448632 A GB1448632 A GB 1448632A GB 391322 A GB391322 A GB 391322A
- Authority
- GB
- United Kingdom
- Prior art keywords
- fibres
- silicic acid
- gel
- active
- capillaries
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/152—Preparation of hydrogels
- C01B33/154—Preparation of hydrogels by acidic treatment of aqueous silicate solutions
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Artificial Filaments (AREA)
Abstract
In the manufacture of active silicic acid or active mixed gels of silicic acid with metal oxides or hydroxides or mixed gels of silicic acid with active carbon by known processes, loose fibres of the kind possessing capillaries or leaving capillaries behind on heating are added to the components of the reaction or to the reaction mixture, at any stage before the drying of the gel, to the extent of 0,1 to 15 per cent by weight of the dry silicic acid. The artificially-produced capillaries facilitate the adsorption and the driving-off of substances or gases adsorbed. If fibres of the kind embodying capillaries are employed, for example, animal hair, the drying temperature need not be sufficient to char or to burn the fibres. If fibres such as cotton, artificial silk or wood are employed, the drying temperature should be sufficient to burn or char the fibres, or a hot current of air may be employed, either during or after drying p for this purpose. When the gel is prepared by precipitation from aqueous solutions the fibres may be added before, during or after precipitation, and can also be added to the gel after separation from the liquid or when the gel is partly dried. A portion of the fibres may be added at an earlier stage and the remainder at a later stage. When employing animal hair, it should preferably be boiled with water before admixture. According to an example, a water-glass solution, with which is admixed animal hair of a length depending on the required size of the dried gel, is stirred with a dilute hydrochloric acid solution. The weakly alkaline sol produced eventually coagulates to a gel which is filtered, washed, if desired, shaped, dried and heated.ALSO:In the manufacture of active silicic acid or active mixed gels of silicic acid with metal oxides or hydroxides or mixed gels of silicic acid with active carbon by known processes, loose fibres of the kind possessing capillaries or leaving capillaries behind on heating are added to the components of the reaction or to the reaction mixture, at any stage before the drying of the gel, to the extent of 0,1 to 15 per cent by weight of the dry silicic acid. The artificially produced capillaries facilitate the adsorption and the driving off of substances or gases absorbed. If fibres of the kind embodying capillaries are employed, for example animal hair, the drying temperature need not be sufficient to char or to burn the fibres. If fibres such as cotton, artificial silk or wood are employed, the drying temperature should be sufficient to burn or char the fibres, or a hot current of air may be employed either during or after drying for this purpose. When the gel is prepared by precipitation from aqueous solutions the fibres may be added before, during or after precipitation and can also be added to the gel after separation from the liquid or when the gel is partly dried. A portion of the fibres may be added at an earlier stage and the remainder at a later stage. When employing animal hair, it should preferably be boiled with water before admixture.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE391322X | 1931-05-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB391322A true GB391322A (en) | 1933-04-27 |
Family
ID=6379192
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB14486/32A Expired GB391322A (en) | 1931-05-21 | 1932-05-21 | Methods of producing active silicic acid or active mixed gels of silicic acid with metal hydroxides or metal oxides, or mixed gels of silicic acid with active carbon |
Country Status (2)
Country | Link |
---|---|
FR (1) | FR737316A (en) |
GB (1) | GB391322A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2844436A (en) * | 1952-11-28 | 1958-07-22 | Philadelphia Quartz Co | Manufacture of finely-divided compounds of certain elements |
-
1932
- 1932-05-19 FR FR737316D patent/FR737316A/en not_active Expired
- 1932-05-21 GB GB14486/32A patent/GB391322A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2844436A (en) * | 1952-11-28 | 1958-07-22 | Philadelphia Quartz Co | Manufacture of finely-divided compounds of certain elements |
Also Published As
Publication number | Publication date |
---|---|
FR737316A (en) | 1932-12-09 |
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