GB254402A - Improvements in the manufacture of naphthylamine sulpho acids - Google Patents

Improvements in the manufacture of naphthylamine sulpho acids

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Publication number
GB254402A
GB254402A GB904325A GB904325A GB254402A GB 254402 A GB254402 A GB 254402A GB 904325 A GB904325 A GB 904325A GB 904325 A GB904325 A GB 904325A GB 254402 A GB254402 A GB 254402A
Authority
GB
United Kingdom
Prior art keywords
ammonia
naphthalene
naphthylamine
manufacture
nitro
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB904325A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
RUTH MURIEL HEREWARD
Original Assignee
RUTH MURIEL HEREWARD
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by RUTH MURIEL HEREWARD filed Critical RUTH MURIEL HEREWARD
Priority to GB904325A priority Critical patent/GB254402A/en
Publication of GB254402A publication Critical patent/GB254402A/en
Expired legal-status Critical Current

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

254,402. Ehrhardt, E. F., and Hereward, R. M. April 4, 1925. Naphthylamine sulphonic acids are obtained by treating 1-nitro-naphthalene with an alkaline sulphite, or a mixture of alkaline sulphites, and ammonia under pressure in aqueous solution. Preferably a mixture of sodium and ammonium sulphites, obtained by neutralizing sodium bisulphite with ammonia, is used. This is heated with 1-nitro-naphthalene and ammonia in an autoclave and the product is poured into water, filtered, boiled to remove the excess of ammonia, and acidified with hydrochloric acid. Naphthionic acid separates out and is removed; 1 : 5 naphthalene sulphonic acid can be obtained from the mother liquor.
GB904325A 1925-04-04 1925-04-04 Improvements in the manufacture of naphthylamine sulpho acids Expired GB254402A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB904325A GB254402A (en) 1925-04-04 1925-04-04 Improvements in the manufacture of naphthylamine sulpho acids

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB904325A GB254402A (en) 1925-04-04 1925-04-04 Improvements in the manufacture of naphthylamine sulpho acids

Publications (1)

Publication Number Publication Date
GB254402A true GB254402A (en) 1926-07-05

Family

ID=9864279

Family Applications (1)

Application Number Title Priority Date Filing Date
GB904325A Expired GB254402A (en) 1925-04-04 1925-04-04 Improvements in the manufacture of naphthylamine sulpho acids

Country Status (1)

Country Link
GB (1) GB254402A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0214543A2 (en) * 1985-09-07 1987-03-18 Bayer Ag Process for the preparation of 1-aminonaphthalene-2,4,7-trisulfonic acid and 1-aminonaphthalene-7-sulfonic acid
CN110372547A (en) * 2018-04-12 2019-10-25 浙江龙盛化工研究有限公司 A method of preparing 1- amino -4- sodium naphthalene sulfonate

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0214543A2 (en) * 1985-09-07 1987-03-18 Bayer Ag Process for the preparation of 1-aminonaphthalene-2,4,7-trisulfonic acid and 1-aminonaphthalene-7-sulfonic acid
EP0214543A3 (en) * 1985-09-07 1989-01-25 Bayer Ag Process for the preparation of 1-aminonaphthalene-2,4,7-trisulfonic acid and 1-aminonaphthalene-7-sulfonic acid
CN110372547A (en) * 2018-04-12 2019-10-25 浙江龙盛化工研究有限公司 A method of preparing 1- amino -4- sodium naphthalene sulfonate
CN110372547B (en) * 2018-04-12 2021-12-21 浙江科永化工有限公司 Method for preparing 1-amino-4-sodium naphthalene sulfonate

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