GB1354944A - Purification of aqueous magnesium chloride - Google Patents
Purification of aqueous magnesium chlorideInfo
- Publication number
- GB1354944A GB1354944A GB4521171A GB4521171A GB1354944A GB 1354944 A GB1354944 A GB 1354944A GB 4521171 A GB4521171 A GB 4521171A GB 4521171 A GB4521171 A GB 4521171A GB 1354944 A GB1354944 A GB 1354944A
- Authority
- GB
- United Kingdom
- Prior art keywords
- magnesium chloride
- alcohol
- chloride solution
- volume
- aqueous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 title abstract 10
- 229910001629 magnesium chloride Inorganic materials 0.000 title abstract 5
- 238000000746 purification Methods 0.000 title 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 239000002904 solvent Substances 0.000 abstract 3
- YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- 150000001639 boron compounds Chemical class 0.000 abstract 2
- IVSZLXZYQVIEFR-UHFFFAOYSA-N m-xylene Chemical group CC1=CC=CC(C)=C1 IVSZLXZYQVIEFR-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000012074 organic phase Substances 0.000 abstract 2
- JWZZKOKVBUJMES-UHFFFAOYSA-N (+-)-Isoprenaline Chemical compound CC(C)NCC(O)C1=CC=C(O)C(O)=C1 JWZZKOKVBUJMES-UHFFFAOYSA-N 0.000 abstract 1
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 1
- BODRLKRKPXBDBN-UHFFFAOYSA-N 3,5,5-Trimethyl-1-hexanol Chemical compound OCCC(C)CC(C)(C)C BODRLKRKPXBDBN-UHFFFAOYSA-N 0.000 abstract 1
- BWDBEAQIHAEVLV-UHFFFAOYSA-N 6-methylheptan-1-ol Chemical compound CC(C)CCCCCO BWDBEAQIHAEVLV-UHFFFAOYSA-N 0.000 abstract 1
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- 150000001298 alcohols Chemical class 0.000 abstract 1
- -1 aliphatic alcohols Chemical class 0.000 abstract 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 abstract 1
- 239000004327 boric acid Substances 0.000 abstract 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 abstract 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 abstract 1
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical class CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000000622 liquid--liquid extraction Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000000638 solvent extraction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/26—Magnesium halides
- C01F5/30—Chlorides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Electrolytic Production Of Metals (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NO3686/70A NO124026B (enExample) | 1970-09-29 | 1970-09-29 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1354944A true GB1354944A (en) | 1974-06-05 |
Family
ID=19879783
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB4521171A Expired GB1354944A (en) | 1970-09-29 | 1971-09-28 | Purification of aqueous magnesium chloride |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US3855392A (enExample) |
| JP (1) | JPS5422436B1 (enExample) |
| ES (1) | ES395503A1 (enExample) |
| FR (1) | FR2108640A5 (enExample) |
| GB (1) | GB1354944A (enExample) |
| NL (1) | NL153154B (enExample) |
| NO (1) | NO124026B (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1514927A (en) * | 1974-10-23 | 1978-06-21 | United States Borax Chem | Process for the production of boric acid |
| US4201758A (en) * | 1979-03-22 | 1980-05-06 | Nalco Chemical Co. | Boron removal from ethylene glycol-magnesium chloride solutions |
| US4208392A (en) * | 1979-03-23 | 1980-06-17 | Nalco Chemical Co. | Two-step process for removing boron compounds from aqueous solutions of magnesium chloride |
| US5219550A (en) * | 1989-03-31 | 1993-06-15 | Cyprus Foote Mineral Company | Production of low boron lithium carbonate from lithium-containing brine |
| US4980136A (en) * | 1989-07-14 | 1990-12-25 | Cyprus Foote Mineral Company | Production of lithium metal grade lithium chloride from lithium-containing brine |
| US5785868A (en) * | 1995-09-11 | 1998-07-28 | Board Of Regents, Univ. Of Texas System | Method for selective separation of products at hydrothermal conditions |
| AR001916A1 (es) * | 1996-02-20 | 1997-12-10 | Minera Salar De Atacama S A So | Proceso para extraer boro desde salmueras naturales o industriales empleando extración por solventes |
| AR001917A1 (es) * | 1996-03-28 | 1997-12-10 | Minera Salar De Atacama S A So | Producción de carbonato de litio de alta pureza desde salmueras naturales o industriales |
| EP3897927A4 (en) | 2018-12-21 | 2022-10-26 | Mangrove Water Technologies Ltd. | LI RECOVERY PROCESSES AND ON-SITE CHEMICAL PRODUCTION FOR LI RECOVERY PROCESSES |
| CN110422853B (zh) * | 2019-08-26 | 2021-09-21 | 东北大学 | 一种利用高镁低硼溶液制备高纯硼酸的方法 |
| AU2024314063A1 (en) * | 2023-06-22 | 2025-10-30 | Caremag | Method for the selective extraction of boron by means of an organic solvent from solutions derived from acid attack on permanent magnets comprising rare earths |
| FR3150199B1 (fr) | 2023-06-22 | 2025-10-03 | Caremag | Procede de recuperation d’un sel de bore a partir d’un solvant organique comprenant de l’acide borique |
| FR3150198B1 (fr) * | 2023-06-22 | 2025-10-03 | Caremag | Procede d’extraction selective du bore par un solvant organique a partir de solutions issues de l’attaque acide d’aimants permanents comprenant des terres rares |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1092284A (fr) * | 1953-06-18 | 1955-04-20 | Centre Nat Rech Scient | Procédé d'extraction et de purification d'acides forts en milieux aqueux. application particulière à l'acide perrhénique |
| US2969275A (en) * | 1958-11-14 | 1961-01-24 | American Potash & Chem Corp | Recovery of boron values |
| GB910541A (en) * | 1959-08-18 | 1962-11-14 | American Potash & Chem Corp | Improvements relating to the recovery of boron values from alkaline liquors |
| US3433604A (en) * | 1965-09-22 | 1969-03-18 | Dow Chemical Co | Calcium chloride and boric acid extraction from magnesium chloride brines using diols and catechols |
| US3424563A (en) * | 1966-02-03 | 1969-01-28 | Dow Chemical Co | Selective extraction of boron from aqueous solutions |
| US3493349A (en) * | 1966-09-28 | 1970-02-03 | Dow Chemical Co | Extraction of boron from brines having a ph of less than about 1.7 using beta-aliphatic diols |
-
1970
- 1970-09-29 NO NO3686/70A patent/NO124026B/no unknown
-
1971
- 1971-09-24 US US00183683A patent/US3855392A/en not_active Expired - Lifetime
- 1971-09-28 ES ES395503A patent/ES395503A1/es not_active Expired
- 1971-09-28 GB GB4521171A patent/GB1354944A/en not_active Expired
- 1971-09-28 JP JP7571771A patent/JPS5422436B1/ja active Pending
- 1971-09-28 NL NL717113299A patent/NL153154B/xx not_active IP Right Cessation
- 1971-09-28 FR FR7134848A patent/FR2108640A5/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2148464A1 (de) | 1972-03-30 |
| ES395503A1 (es) | 1973-12-16 |
| NL7113299A (enExample) | 1972-04-04 |
| FR2108640A5 (enExample) | 1972-05-19 |
| NO124026B (enExample) | 1972-02-21 |
| US3855392A (en) | 1974-12-17 |
| NL153154B (nl) | 1977-05-16 |
| JPS5422436B1 (enExample) | 1979-08-07 |
| DE2148464B2 (de) | 1976-03-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |