GB1138750A - Preparation of oximes - Google Patents
Preparation of oximesInfo
- Publication number
- GB1138750A GB1138750A GB44743/66A GB4474366A GB1138750A GB 1138750 A GB1138750 A GB 1138750A GB 44743/66 A GB44743/66 A GB 44743/66A GB 4474366 A GB4474366 A GB 4474366A GB 1138750 A GB1138750 A GB 1138750A
- Authority
- GB
- United Kingdom
- Prior art keywords
- solvent
- reaction zone
- stream
- oxime
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000002923 oximes Chemical class 0.000 title abstract 5
- 239000002253 acid Substances 0.000 abstract 5
- 239000002904 solvent Substances 0.000 abstract 5
- 238000006243 chemical reaction Methods 0.000 abstract 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- 101100188555 Arabidopsis thaliana OCT6 gene Proteins 0.000 abstract 1
- -1 Cycloalkyl oximes Chemical class 0.000 abstract 1
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical class ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 1
- BIGPRXCJEDHCLP-UHFFFAOYSA-N ammonium bisulfate Chemical compound [NH4+].OS([O-])(=O)=O BIGPRXCJEDHCLP-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 150000003997 cyclic ketones Chemical class 0.000 abstract 1
- 238000010586 diagram Methods 0.000 abstract 1
- 238000010494 dissociation reaction Methods 0.000 abstract 1
- 230000005593 dissociations Effects 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
- 238000004064 recycling Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/32—Oximes
- C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C251/44—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL6513426A NL6513426A (xx) | 1965-10-16 | 1965-10-16 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1138750A true GB1138750A (en) | 1969-01-01 |
Family
ID=19794388
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB44743/66A Expired GB1138750A (en) | 1965-10-16 | 1966-10-06 | Preparation of oximes |
Country Status (12)
Country | Link |
---|---|
AT (1) | AT265240B (xx) |
BE (1) | BE688260A (xx) |
CH (1) | CH481888A (xx) |
DE (1) | DE1272288B (xx) |
DK (1) | DK117701B (xx) |
ES (1) | ES332252A1 (xx) |
FR (1) | FR1496435A (xx) |
GB (1) | GB1138750A (xx) |
IL (1) | IL26663A (xx) |
NL (1) | NL6513426A (xx) |
NO (1) | NO125629B (xx) |
SE (1) | SE338985B (xx) |
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3625835A (en) * | 1970-06-15 | 1971-12-07 | Stamicarbon | Process for the recovery of cyclohexanone oxime by plural stage, vacuum distillation per a |
US3720758A (en) * | 1969-09-20 | 1973-03-13 | Stamicarbon | Process for the continuous preparation of an aqueous solution of a hydroxylammonium salt |
US3862230A (en) * | 1969-09-20 | 1975-01-21 | Stamicarbon | Continuous preparation of cyclohexanone oxime |
US4031139A (en) * | 1975-02-26 | 1977-06-21 | Basf Aktiengesellschaft | Manufacture of cyclohexanone oxime |
US4104359A (en) * | 1977-02-28 | 1978-08-01 | Amax Inc. | Regeneration of organic extractants containing α-hydroxyoximes |
BE1005576A3 (fr) * | 1991-02-13 | 1993-11-09 | Mitsubishi Chem Ind | Procede de preparation d'une oxime. |
WO2001094296A1 (en) * | 2000-06-05 | 2001-12-13 | Dsm N.V. | Process for the production of cyclohexanone oxime |
WO2001094298A1 (en) * | 2000-06-05 | 2001-12-13 | Dsm N.V. | Process for the preparation of cyclohexanone oxime |
WO2002096861A2 (en) * | 2001-05-31 | 2002-12-05 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing phosphate, cyclohexanone and cycloexanone oxime |
WO2003048037A1 (en) * | 2001-12-04 | 2003-06-12 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing phosphate salt and organic compounds |
WO2004067497A1 (en) * | 2003-01-30 | 2004-08-12 | Dsm Ip Assets B.V. | Process for treating an organic solution comprising cyclohexanone oxime, cyclohexanone, and an organic solvent |
EP1942099A1 (en) * | 2007-01-05 | 2008-07-09 | China Petrochemical Development Corporation | Process for production of cyclohexanone oxime |
US7408081B2 (en) | 2001-12-04 | 2008-08-05 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing cyclohexanone oxime and cyclohexanone |
CN103193672A (zh) * | 2013-03-11 | 2013-07-10 | 浙江圣安化工有限公司 | 一种肟的蒸馏方法 |
CN105348145A (zh) * | 2015-10-23 | 2016-02-24 | 中石化南京工程有限公司 | 氨法烟气脱硫副产环己酮肟的方法 |
CN105384656A (zh) * | 2015-10-23 | 2016-03-09 | 中石化南京工程有限公司 | 一种环己酮肟化的方法 |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL135679C (xx) * | 1968-11-12 | 1900-01-01 | ||
DE2029114C2 (de) * | 1970-06-12 | 1982-07-01 | Stamicarbon B.V., 6160 Geleen | Verfahren zur Herstellung von Cyclohexanonoxim |
NL7008838A (xx) * | 1970-06-17 | 1971-12-21 | ||
DE3942334A1 (de) * | 1989-12-21 | 1991-06-27 | Basf Ag | Verfahren zur aufarbeitung von salzsaeure, schwefelsaeure und deren hydroxylammonium- und ammoniumsalze enthaltenden waessrigen mutterlaugen |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2270204A (en) * | 1938-11-28 | 1942-01-13 | Du Pont | Process of producing oximes |
DE1081884B (de) * | 1959-02-13 | 1960-05-19 | Basf Ag | Verfahren zur Herstellung von Cyclododecanonoxim |
GB972107A (en) * | 1962-09-01 | 1964-10-07 | Basf Ag | Production of oximes of cycloaliphatic ketones |
NL301053A (xx) * | 1963-11-27 |
-
1965
- 1965-10-16 NL NL6513426A patent/NL6513426A/xx unknown
-
1966
- 1966-10-06 GB GB44743/66A patent/GB1138750A/en not_active Expired
- 1966-10-07 AT AT942866A patent/AT265240B/de active
- 1966-10-07 DE DEP1272A patent/DE1272288B/de active Pending
- 1966-10-10 IL IL26663A patent/IL26663A/xx unknown
- 1966-10-10 CH CH1454566A patent/CH481888A/de not_active IP Right Cessation
- 1966-10-12 FR FR79609A patent/FR1496435A/fr not_active Expired
- 1966-10-14 NO NO165161A patent/NO125629B/no unknown
- 1966-10-14 ES ES0332252A patent/ES332252A1/es not_active Expired
- 1966-10-14 BE BE688260D patent/BE688260A/xx not_active IP Right Cessation
- 1966-10-14 SE SE14007/66A patent/SE338985B/xx unknown
- 1966-10-17 DK DK535566AA patent/DK117701B/da unknown
Cited By (32)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3720758A (en) * | 1969-09-20 | 1973-03-13 | Stamicarbon | Process for the continuous preparation of an aqueous solution of a hydroxylammonium salt |
US3862230A (en) * | 1969-09-20 | 1975-01-21 | Stamicarbon | Continuous preparation of cyclohexanone oxime |
US3625835A (en) * | 1970-06-15 | 1971-12-07 | Stamicarbon | Process for the recovery of cyclohexanone oxime by plural stage, vacuum distillation per a |
US4031139A (en) * | 1975-02-26 | 1977-06-21 | Basf Aktiengesellschaft | Manufacture of cyclohexanone oxime |
US4104359A (en) * | 1977-02-28 | 1978-08-01 | Amax Inc. | Regeneration of organic extractants containing α-hydroxyoximes |
BE1005576A3 (fr) * | 1991-02-13 | 1993-11-09 | Mitsubishi Chem Ind | Procede de preparation d'une oxime. |
US7005547B2 (en) | 2000-06-05 | 2006-02-28 | Dsm Ip Assets B.V. | Process for the preparation of cyclohexanone oxime |
WO2001094298A1 (en) * | 2000-06-05 | 2001-12-13 | Dsm N.V. | Process for the preparation of cyclohexanone oxime |
KR100843925B1 (ko) | 2000-06-05 | 2008-07-03 | 디에스엠 아이피 어셋츠 비.브이. | 시클로헥사논 옥심의 제조방법 |
KR100763111B1 (ko) | 2000-06-05 | 2007-10-04 | 디에스엠 아이피 어셋츠 비.브이. | 시클로헥사논 옥심의 제조방법 |
WO2001094296A1 (en) * | 2000-06-05 | 2001-12-13 | Dsm N.V. | Process for the production of cyclohexanone oxime |
US6844469B2 (en) | 2000-06-05 | 2005-01-18 | Dsm Ip Assets B.V. | Process for the production of cyclohexanone oxime |
JP2003535841A (ja) * | 2000-06-05 | 2003-12-02 | ディーエスエム エヌ.ブイ. | シクロヘキサノンオキシムの製造法 |
KR100861858B1 (ko) | 2001-05-31 | 2008-10-06 | 디에스엠 아이피 어셋츠 비.브이. | 포스페이트, 시클로헥사논 및 시클로헥사논 옥심을함유하는 수성 매질의 처리 방법 |
CN1321976C (zh) * | 2001-05-31 | 2007-06-20 | Dsmip财产有限公司 | 处理含磷酸盐、环己酮和环己酮肟的水介质的方法 |
WO2002096861A3 (en) * | 2001-05-31 | 2003-03-20 | Dsm Nv | Process for treating an aqueous medium containing phosphate, cyclohexanone and cycloexanone oxime |
US7309801B2 (en) | 2001-05-31 | 2007-12-18 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing phosphate, cyclohexanone and cyclohexanone oxime |
WO2002096861A2 (en) * | 2001-05-31 | 2002-12-05 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing phosphate, cyclohexanone and cycloexanone oxime |
WO2003048037A1 (en) * | 2001-12-04 | 2003-06-12 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing phosphate salt and organic compounds |
US7408081B2 (en) | 2001-12-04 | 2008-08-05 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing cyclohexanone oxime and cyclohexanone |
EP1318141A1 (en) * | 2001-12-04 | 2003-06-11 | Dsm Nv | Process for treating an aqueous medium containing phosphate, cyclohexanone and cyclohexanone oxime |
US7161037B2 (en) | 2001-12-04 | 2007-01-09 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing phosphate salt and organic compounds |
JP2006516612A (ja) * | 2003-01-30 | 2006-07-06 | デーエスエム アイピー アセッツ ベー. ヴェー. | シクロヘキサノンオキシム、シクロヘキサノン、および有機溶媒を含む有機溶液の処理方法 |
US7423178B2 (en) | 2003-01-30 | 2008-09-09 | Dsm Ip Assets B.V. | Process for treating an organic solution comprising cyclohexanone oxime, cyclohexanone, and an organic solvent |
WO2004067497A1 (en) * | 2003-01-30 | 2004-08-12 | Dsm Ip Assets B.V. | Process for treating an organic solution comprising cyclohexanone oxime, cyclohexanone, and an organic solvent |
KR101078927B1 (ko) * | 2003-01-30 | 2011-11-01 | 디에스엠 아이피 어셋츠 비.브이. | 사이클로헥산온 옥심, 사이클로헥산온 및 유기 용매를포함하는 유기 용액을 처리하는 방법 |
EP1942099A1 (en) * | 2007-01-05 | 2008-07-09 | China Petrochemical Development Corporation | Process for production of cyclohexanone oxime |
CN103193672A (zh) * | 2013-03-11 | 2013-07-10 | 浙江圣安化工有限公司 | 一种肟的蒸馏方法 |
CN103193672B (zh) * | 2013-03-11 | 2014-09-17 | 浙江圣安化工有限公司 | 一种肟的蒸馏方法 |
CN105348145A (zh) * | 2015-10-23 | 2016-02-24 | 中石化南京工程有限公司 | 氨法烟气脱硫副产环己酮肟的方法 |
CN105384656A (zh) * | 2015-10-23 | 2016-03-09 | 中石化南京工程有限公司 | 一种环己酮肟化的方法 |
CN105348145B (zh) * | 2015-10-23 | 2018-02-06 | 中石化南京工程有限公司 | 氨法烟气脱硫副产环己酮肟的方法 |
Also Published As
Publication number | Publication date |
---|---|
ES332252A1 (es) | 1967-07-16 |
BE688260A (xx) | 1967-04-14 |
CH481888A (de) | 1969-11-30 |
DE1272288B (de) | 1968-07-11 |
SE338985B (xx) | 1971-09-27 |
FR1496435A (fr) | 1967-09-29 |
IL26663A (en) | 1970-09-17 |
NO125629B (xx) | 1972-10-09 |
AT265240B (de) | 1968-10-10 |
DK117701B (da) | 1970-05-25 |
NL6513426A (xx) | 1967-04-17 |
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