GB1138750A - Preparation of oximes - Google Patents

Preparation of oximes

Info

Publication number
GB1138750A
GB1138750A GB44743/66A GB4474366A GB1138750A GB 1138750 A GB1138750 A GB 1138750A GB 44743/66 A GB44743/66 A GB 44743/66A GB 4474366 A GB4474366 A GB 4474366A GB 1138750 A GB1138750 A GB 1138750A
Authority
GB
United Kingdom
Prior art keywords
solvent
reaction zone
stream
oxime
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB44743/66A
Other languages
English (en)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stamicarbon BV
Original Assignee
Stamicarbon BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stamicarbon BV filed Critical Stamicarbon BV
Publication of GB1138750A publication Critical patent/GB1138750A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32Oximes
    • C07C251/34Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/44Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
GB44743/66A 1965-10-16 1966-10-06 Preparation of oximes Expired GB1138750A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL6513426A NL6513426A (de) 1965-10-16 1965-10-16

Publications (1)

Publication Number Publication Date
GB1138750A true GB1138750A (en) 1969-01-01

Family

ID=19794388

Family Applications (1)

Application Number Title Priority Date Filing Date
GB44743/66A Expired GB1138750A (en) 1965-10-16 1966-10-06 Preparation of oximes

Country Status (12)

Country Link
AT (1) AT265240B (de)
BE (1) BE688260A (de)
CH (1) CH481888A (de)
DE (1) DE1272288B (de)
DK (1) DK117701B (de)
ES (1) ES332252A1 (de)
FR (1) FR1496435A (de)
GB (1) GB1138750A (de)
IL (1) IL26663A (de)
NL (1) NL6513426A (de)
NO (1) NO125629B (de)
SE (1) SE338985B (de)

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3625835A (en) * 1970-06-15 1971-12-07 Stamicarbon Process for the recovery of cyclohexanone oxime by plural stage, vacuum distillation per a
US3720758A (en) * 1969-09-20 1973-03-13 Stamicarbon Process for the continuous preparation of an aqueous solution of a hydroxylammonium salt
US3862230A (en) * 1969-09-20 1975-01-21 Stamicarbon Continuous preparation of cyclohexanone oxime
US4031139A (en) * 1975-02-26 1977-06-21 Basf Aktiengesellschaft Manufacture of cyclohexanone oxime
US4104359A (en) * 1977-02-28 1978-08-01 Amax Inc. Regeneration of organic extractants containing α-hydroxyoximes
BE1005576A3 (fr) * 1991-02-13 1993-11-09 Mitsubishi Chem Ind Procede de preparation d'une oxime.
WO2001094298A1 (en) * 2000-06-05 2001-12-13 Dsm N.V. Process for the preparation of cyclohexanone oxime
WO2001094296A1 (en) * 2000-06-05 2001-12-13 Dsm N.V. Process for the production of cyclohexanone oxime
WO2002096861A2 (en) * 2001-05-31 2002-12-05 Dsm Ip Assets B.V. Process for treating an aqueous medium containing phosphate, cyclohexanone and cycloexanone oxime
WO2003048037A1 (en) * 2001-12-04 2003-06-12 Dsm Ip Assets B.V. Process for treating an aqueous medium containing phosphate salt and organic compounds
WO2004067497A1 (en) * 2003-01-30 2004-08-12 Dsm Ip Assets B.V. Process for treating an organic solution comprising cyclohexanone oxime, cyclohexanone, and an organic solvent
EP1942099A1 (de) * 2007-01-05 2008-07-09 China Petrochemical Development Corporation Verfahren zur Herstellung von Cyclohexanon-Oxim
US7408081B2 (en) 2001-12-04 2008-08-05 Dsm Ip Assets B.V. Process for treating an aqueous medium containing cyclohexanone oxime and cyclohexanone
CN103193672A (zh) * 2013-03-11 2013-07-10 浙江圣安化工有限公司 一种肟的蒸馏方法
CN105348145A (zh) * 2015-10-23 2016-02-24 中石化南京工程有限公司 氨法烟气脱硫副产环己酮肟的方法
CN105384656A (zh) * 2015-10-23 2016-03-09 中石化南京工程有限公司 一种环己酮肟化的方法

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL135679C (de) * 1968-11-12 1900-01-01
DE2029114C2 (de) * 1970-06-12 1982-07-01 Stamicarbon B.V., 6160 Geleen Verfahren zur Herstellung von Cyclohexanonoxim
NL7008838A (de) * 1970-06-17 1971-12-21
DE3942334A1 (de) * 1989-12-21 1991-06-27 Basf Ag Verfahren zur aufarbeitung von salzsaeure, schwefelsaeure und deren hydroxylammonium- und ammoniumsalze enthaltenden waessrigen mutterlaugen

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2270204A (en) * 1938-11-28 1942-01-13 Du Pont Process of producing oximes
DE1081884B (de) * 1959-02-13 1960-05-19 Basf Ag Verfahren zur Herstellung von Cyclododecanonoxim
GB972107A (en) * 1962-09-01 1964-10-07 Basf Ag Production of oximes of cycloaliphatic ketones
NL301053A (de) * 1963-11-27

Cited By (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3720758A (en) * 1969-09-20 1973-03-13 Stamicarbon Process for the continuous preparation of an aqueous solution of a hydroxylammonium salt
US3862230A (en) * 1969-09-20 1975-01-21 Stamicarbon Continuous preparation of cyclohexanone oxime
US3625835A (en) * 1970-06-15 1971-12-07 Stamicarbon Process for the recovery of cyclohexanone oxime by plural stage, vacuum distillation per a
US4031139A (en) * 1975-02-26 1977-06-21 Basf Aktiengesellschaft Manufacture of cyclohexanone oxime
US4104359A (en) * 1977-02-28 1978-08-01 Amax Inc. Regeneration of organic extractants containing α-hydroxyoximes
BE1005576A3 (fr) * 1991-02-13 1993-11-09 Mitsubishi Chem Ind Procede de preparation d'une oxime.
US7005547B2 (en) 2000-06-05 2006-02-28 Dsm Ip Assets B.V. Process for the preparation of cyclohexanone oxime
WO2001094296A1 (en) * 2000-06-05 2001-12-13 Dsm N.V. Process for the production of cyclohexanone oxime
KR100843925B1 (ko) 2000-06-05 2008-07-03 디에스엠 아이피 어셋츠 비.브이. 시클로헥사논 옥심의 제조방법
KR100763111B1 (ko) 2000-06-05 2007-10-04 디에스엠 아이피 어셋츠 비.브이. 시클로헥사논 옥심의 제조방법
WO2001094298A1 (en) * 2000-06-05 2001-12-13 Dsm N.V. Process for the preparation of cyclohexanone oxime
US6844469B2 (en) 2000-06-05 2005-01-18 Dsm Ip Assets B.V. Process for the production of cyclohexanone oxime
JP2003535841A (ja) * 2000-06-05 2003-12-02 ディーエスエム エヌ.ブイ. シクロヘキサノンオキシムの製造法
KR100861858B1 (ko) 2001-05-31 2008-10-06 디에스엠 아이피 어셋츠 비.브이. 포스페이트, 시클로헥사논 및 시클로헥사논 옥심을함유하는 수성 매질의 처리 방법
CN1321976C (zh) * 2001-05-31 2007-06-20 Dsmip财产有限公司 处理含磷酸盐、环己酮和环己酮肟的水介质的方法
WO2002096861A3 (en) * 2001-05-31 2003-03-20 Dsm Nv Process for treating an aqueous medium containing phosphate, cyclohexanone and cycloexanone oxime
US7309801B2 (en) 2001-05-31 2007-12-18 Dsm Ip Assets B.V. Process for treating an aqueous medium containing phosphate, cyclohexanone and cyclohexanone oxime
WO2002096861A2 (en) * 2001-05-31 2002-12-05 Dsm Ip Assets B.V. Process for treating an aqueous medium containing phosphate, cyclohexanone and cycloexanone oxime
WO2003048037A1 (en) * 2001-12-04 2003-06-12 Dsm Ip Assets B.V. Process for treating an aqueous medium containing phosphate salt and organic compounds
US7408081B2 (en) 2001-12-04 2008-08-05 Dsm Ip Assets B.V. Process for treating an aqueous medium containing cyclohexanone oxime and cyclohexanone
EP1318141A1 (de) * 2001-12-04 2003-06-11 Dsm Nv Verfahren zur Behandlung eines Phosphat, Cyclohexanon, Cyclohexanonoxim enthaltenden wässrigen Mediums
US7161037B2 (en) 2001-12-04 2007-01-09 Dsm Ip Assets B.V. Process for treating an aqueous medium containing phosphate salt and organic compounds
JP2006516612A (ja) * 2003-01-30 2006-07-06 デーエスエム アイピー アセッツ ベー. ヴェー. シクロヘキサノンオキシム、シクロヘキサノン、および有機溶媒を含む有機溶液の処理方法
US7423178B2 (en) 2003-01-30 2008-09-09 Dsm Ip Assets B.V. Process for treating an organic solution comprising cyclohexanone oxime, cyclohexanone, and an organic solvent
WO2004067497A1 (en) * 2003-01-30 2004-08-12 Dsm Ip Assets B.V. Process for treating an organic solution comprising cyclohexanone oxime, cyclohexanone, and an organic solvent
KR101078927B1 (ko) * 2003-01-30 2011-11-01 디에스엠 아이피 어셋츠 비.브이. 사이클로헥산온 옥심, 사이클로헥산온 및 유기 용매를포함하는 유기 용액을 처리하는 방법
EP1942099A1 (de) * 2007-01-05 2008-07-09 China Petrochemical Development Corporation Verfahren zur Herstellung von Cyclohexanon-Oxim
CN103193672A (zh) * 2013-03-11 2013-07-10 浙江圣安化工有限公司 一种肟的蒸馏方法
CN103193672B (zh) * 2013-03-11 2014-09-17 浙江圣安化工有限公司 一种肟的蒸馏方法
CN105348145A (zh) * 2015-10-23 2016-02-24 中石化南京工程有限公司 氨法烟气脱硫副产环己酮肟的方法
CN105384656A (zh) * 2015-10-23 2016-03-09 中石化南京工程有限公司 一种环己酮肟化的方法
CN105348145B (zh) * 2015-10-23 2018-02-06 中石化南京工程有限公司 氨法烟气脱硫副产环己酮肟的方法

Also Published As

Publication number Publication date
AT265240B (de) 1968-10-10
FR1496435A (fr) 1967-09-29
NL6513426A (de) 1967-04-17
CH481888A (de) 1969-11-30
DK117701B (da) 1970-05-25
DE1272288B (de) 1968-07-11
ES332252A1 (es) 1967-07-16
BE688260A (de) 1967-04-14
IL26663A (en) 1970-09-17
SE338985B (de) 1971-09-27
NO125629B (de) 1972-10-09

Similar Documents

Publication Publication Date Title
GB1138750A (en) Preparation of oximes
GB1447575A (en) Process for the recovery of alkali or ammonium citrates
US3336298A (en) Separation of lactams from a strong sulphuric acid medium
GB1081760A (en) Preparation of oximes
GB1287303A (en) Preparation of oxime
GB1399000A (en) Process for the recovery of pure epsilon-caprolactam
ES402472A1 (es) Procedimiento para la preparacion de lactamas.
GB1279527A (en) Continuous preparation of cyclohexanone oxime
GB1479900A (en) Process for the separation and recovery of ammonia and acid gases
GB1528513A (en) Manufacture of cyclohexanone oxime
GB1259747A (en) Process for the preparation of aliphatic tertiary amides
GB1083085A (en) Process for the recovery of free sulfuric acid from ammonium bisulfate
GB1174601A (en) Process for the Purification of Adiponitrile
GB1508942A (en) Process for producing lactams
GB1158998A (en) Process for the Recovery of Ammonium Sulfate from Aqueous Ammonium Sulfate Solutions Containing Organic Components.
GB1283280A (en) Recycle process for the preparation and processing of a hydroxylammonium salt solution in a cyclohexanone oxime synthesis
GB1409522A (en) Process for recovery of epsilon-caprolactam
ES223348A1 (es) Un método para recuperar oxima de ciclohexanona
GB1283894A (en) Cyclic process for preparing and working up a hydroxylammonium salt solution
GB1106740A (en) Process for the preparation of lactams
GB1103351A (en) Method of preparing urea
GB1284515A (en) Improved cyclic process for preparing and working up a hydroxylammonium salt solution
GB1435894A (en) Production of isocyanates
GB1165597A (en) Synthesis of 1,12-Dodecanedioic Acids
GB1129215A (en) Process for the preparation of isomalic acid through hydrolysis of the 1-acetoxy-1,1-dicyanoethane with strong mineral acids