FR3071497B1 - Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur inorganique de deshydratation et d'une source de chlorure - Google Patents

Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur inorganique de deshydratation et d'une source de chlorure Download PDF

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Publication number
FR3071497B1
FR3071497B1 FR1759025A FR1759025A FR3071497B1 FR 3071497 B1 FR3071497 B1 FR 3071497B1 FR 1759025 A FR1759025 A FR 1759025A FR 1759025 A FR1759025 A FR 1759025A FR 3071497 B1 FR3071497 B1 FR 3071497B1
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FR
France
Prior art keywords
hydroxymethylfurfural
chloride
production
source
dehydration catalyst
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FR1759025A
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English (en)
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FR3071497A1 (fr
Inventor
Justine Denis
Marc Jacquin
Damien Delcroix
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IFP Energies Nouvelles IFPEN
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IFP Energies Nouvelles IFPEN
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Priority to FR1759025A priority Critical patent/FR3071497B1/fr
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to US16/651,381 priority patent/US11084797B2/en
Priority to BR112020004961-1A priority patent/BR112020004961A2/pt
Priority to CN201880063277.5A priority patent/CN111295377A/zh
Priority to JP2020516890A priority patent/JP2020535146A/ja
Priority to PCT/EP2018/075964 priority patent/WO2019063546A1/fr
Priority to EP18770055.4A priority patent/EP3687985A1/fr
Publication of FR3071497A1 publication Critical patent/FR3071497A1/fr
Application granted granted Critical
Publication of FR3071497B1 publication Critical patent/FR3071497B1/fr
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)

Abstract

L'invention concerne un nouveau procédé de transformation d'une charge comprenant au moins un sucre en 5-hydroxyméthylfurfural, dans lequel ladite charge est mise en contact avec un ou plusieurs catalyseurs inorganiques de déshydratation et une ou plusieurs sources de chlorure en présence d'au moins un solvant polaire aprotique pris seul ou en mélange, à une température comprise entre 30°C et 200°C, et à une pression comprise entre 0,1 MPa et 10 MPa.
FR1759025A 2017-09-28 2017-09-28 Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur inorganique de deshydratation et d'une source de chlorure Active FR3071497B1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR1759025A FR3071497B1 (fr) 2017-09-28 2017-09-28 Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur inorganique de deshydratation et d'une source de chlorure
BR112020004961-1A BR112020004961A2 (pt) 2017-09-28 2018-09-25 processo de produção de 5-hidroximetilfurfural na presença de um catalisador inorgânico de desidratação e de uma fonte de cloreto
CN201880063277.5A CN111295377A (zh) 2017-09-28 2018-09-25 在无机脱水催化剂和氯化物源的存在下生产5-羟甲基糠醛的方法
JP2020516890A JP2020535146A (ja) 2017-09-28 2018-09-25 無機脱水触媒およびクロリド源の存在中で５−ヒドロキシメチルフルフラールを製造する方法
US16/651,381 US11084797B2 (en) 2017-09-28 2018-09-25 Process for producing 5-hydroxymethylfurfural in the presence of an inorganic dehydration and a chloride source
PCT/EP2018/075964 WO2019063546A1 (fr) 2017-09-28 2018-09-25 Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur inorganique de deshydratation et d'une source de chlorure
EP18770055.4A EP3687985A1 (fr) 2017-09-28 2018-09-25 Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur inorganique de deshydratation et d'une source de chlorure

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1759025 2017-09-28
FR1759025A FR3071497B1 (fr) 2017-09-28 2017-09-28 Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur inorganique de deshydratation et d'une source de chlorure

Publications (2)

Publication Number Publication Date
FR3071497A1 FR3071497A1 (fr) 2019-03-29
FR3071497B1 true FR3071497B1 (fr) 2021-06-11

Family

ID=61187392

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1759025A Active FR3071497B1 (fr) 2017-09-28 2017-09-28 Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur inorganique de deshydratation et d'une source de chlorure

Country Status (7)

Country Link
US (1) US11084797B2 (fr)
EP (1) EP3687985A1 (fr)
JP (1) JP2020535146A (fr)
CN (1) CN111295377A (fr)
BR (1) BR112020004961A2 (fr)
FR (1) FR3071497B1 (fr)
WO (1) WO2019063546A1 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109970690B (zh) * 2019-04-23 2021-02-12 北京林业大学 一种利用固体酸催化生物质绿色高效制备糠醛的方法
CN116082278A (zh) * 2021-11-05 2023-05-09 中国科学院宁波材料技术与工程研究所 一种提高制备5-羟甲基-2-呋喃甲醛选择性的方法
CN115028609B (zh) * 2022-07-14 2024-04-30 中科国生(杭州)科技有限公司 一种连续化生产5-羟甲基糠醛的生产工艺及装置

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7939681B2 (en) * 2006-08-07 2011-05-10 Battelle Memorial Institute Methods for conversion of carbohydrates in ionic liquids to value-added chemicals
CN102066304A (zh) * 2008-06-17 2011-05-18 威斯康星校友研究基金会 木素纤维素生物质到燃料和化学品的化学转变方法
CN102050806B (zh) * 2010-11-24 2014-01-22 李韡 一种由木质纤维素制备含5-羟甲基糠醛产物的方法
CN102153527B (zh) * 2011-02-28 2013-01-30 浙江师范大学 一种由果糖制备5-羟甲基糠醛的方法
WO2013043131A1 (fr) 2011-09-23 2013-03-28 Agency For Science, Technology And Research Procédé de fabrication de 5-hydroxyméthylfurfural à partir de glucides
CN103842349B (zh) 2011-09-29 2015-09-30 韩国生产技术研究院 在有机溶剂的存在下、使用离子交换树脂生产5-羟甲基-2-呋喃甲醛或其烷基醚衍生物的方法
WO2013066776A1 (fr) * 2011-10-31 2013-05-10 E. I. Du Pont De Nemours And Company Procédés de production de 5-(hydroxyméthyl)furfural
CN104039772B (zh) * 2011-12-28 2016-06-29 纳幕尔杜邦公司 用于制备糠醛的方法
ITNO20130003A1 (it) * 2013-05-09 2014-11-10 Novamont Spa Processo di sintesi di 5-idrossimetilfurfurale da saccaridi
WO2015004273A1 (fr) * 2013-07-12 2015-01-15 Danmarks Tekniske Universitet Procédé de conversion efficace de saccharides en composés de furfural
US20150045576A1 (en) 2013-08-08 2015-02-12 Battelle Memorial Institute Methods of making alkyl lactates and alkyl levulinates from saccharides
CN104761519A (zh) * 2014-01-02 2015-07-08 湖南师范大学 一种在纯水中碳水化合物有效转化为5-羟甲基糠醛的方法
CN103788034B (zh) * 2014-01-27 2016-06-01 华东师范大学 一种5-羟甲基糠醛的制备方法
BR112017007656B1 (pt) * 2014-10-16 2021-09-08 Novamont S.P.A Processo para a produção e para o isolamento de 5-hidroximetilfurfural
FR3043082B1 (fr) * 2015-11-02 2019-07-26 IFP Energies Nouvelles Procede de production de 5-hydroxymethylfurfural en presence de catalyseurs de la famille des acides sulfoniques homogenes en presence d'au moins un solvant polaire aprotique
FR3043081B1 (fr) * 2015-11-02 2017-12-08 Ifp Energies Now Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur acide de lewis et/ou d'un catalyseur base heterogene et d'un catalyseur organique homogene acide de brønsted en presence d'au moins un solvant polaire aprotique
CN106995423A (zh) * 2017-06-01 2017-08-01 厦门大学 一种从果糖制备5‑甲酰氧基甲基糠醛的方法

Also Published As

Publication number Publication date
US20200299250A1 (en) 2020-09-24
EP3687985A1 (fr) 2020-08-05
WO2019063546A1 (fr) 2019-04-04
JP2020535146A (ja) 2020-12-03
BR112020004961A2 (pt) 2020-09-15
FR3071497A1 (fr) 2019-03-29
US11084797B2 (en) 2021-08-10
CN111295377A (zh) 2020-06-16

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