FR3064262B1 - Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane - Google Patents

Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane Download PDF

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Publication number
FR3064262B1
FR3064262B1 FR1752473A FR1752473A FR3064262B1 FR 3064262 B1 FR3064262 B1 FR 3064262B1 FR 1752473 A FR1752473 A FR 1752473A FR 1752473 A FR1752473 A FR 1752473A FR 3064262 B1 FR3064262 B1 FR 3064262B1
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Prior art keywords
zeolite
izm
synthesis
methylpiperidinium
dibromide
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FR1752473A
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English (en)
French (fr)
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FR3064262A1 (fr
Inventor
Raquel MARTINEZ FRANCO
Nicolas Bats
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IFP Energies nouvelles
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IFP Energies nouvelles
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Priority to FR1752473A priority Critical patent/FR3064262B1/fr
Priority to ZA2018/01813A priority patent/ZA201801813B/en
Priority to JP2018050318A priority patent/JP7005399B2/ja
Priority to EP18305310.7A priority patent/EP3378830B1/fr
Priority to CN201810245524.5A priority patent/CN108622915B/zh
Priority to US15/935,946 priority patent/US10875778B2/en
Publication of FR3064262A1 publication Critical patent/FR3064262A1/fr
Application granted granted Critical
Publication of FR3064262B1 publication Critical patent/FR3064262B1/fr
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/305—Addition of material, later completely removed, e.g. as result of heat treatment, leaching or washing, e.g. for forming pores
    • B01J20/3057—Use of a templating or imprinting material ; filling pores of a substrate or matrix followed by the removal of the substrate or matrix
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Catalysts (AREA)
FR1752473A 2017-03-24 2017-03-24 Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane Active FR3064262B1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR1752473A FR3064262B1 (fr) 2017-03-24 2017-03-24 Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane
ZA2018/01813A ZA201801813B (en) 2017-03-24 2018-03-19 Process for the synthesis of izm-2 zeolite in the presence of a template, 1,6-bis(methylpiperidinium)hexane dibromide
JP2018050318A JP7005399B2 (ja) 2017-03-24 2018-03-19 テンプレートである１，６－ビス（メチルピペリジニウム）ヘキサンジブロミドの存在下でのｉｚｍ－２ゼオライトの合成方法
EP18305310.7A EP3378830B1 (fr) 2017-03-24 2018-03-21 Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane
CN201810245524.5A CN108622915B (zh) 2017-03-24 2018-03-23 在模板1,6-双(甲基哌啶鎓)己烷二溴化物的存在下合成izm-2沸石的方法
US15/935,946 US10875778B2 (en) 2017-03-24 2018-03-26 Process for the synthesis of IZM-2 zeolite in the presence of a template, 1,6-bis(methylpiperidinium)hexane dibromide

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1752473 2017-03-24
FR1752473A FR3064262B1 (fr) 2017-03-24 2017-03-24 Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane

Publications (2)

Publication Number Publication Date
FR3064262A1 FR3064262A1 (fr) 2018-09-28
FR3064262B1 true FR3064262B1 (fr) 2019-03-22

Family

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FR1752473A Active FR3064262B1 (fr) 2017-03-24 2017-03-24 Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane

Country Status (6)

Country Link
US (1) US10875778B2 (cg-RX-API-DMAC7.html)
EP (1) EP3378830B1 (cg-RX-API-DMAC7.html)
JP (1) JP7005399B2 (cg-RX-API-DMAC7.html)
CN (1) CN108622915B (cg-RX-API-DMAC7.html)
FR (1) FR3064262B1 (cg-RX-API-DMAC7.html)
ZA (1) ZA201801813B (cg-RX-API-DMAC7.html)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3081347B1 (fr) 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
FR3095199B1 (fr) 2019-04-19 2021-10-29 Ifp Energies Now Procédé de synthèse rapide d'une zeolithe de type structural AFX avec une source de faujasite
FR3095967A1 (fr) * 2019-05-16 2020-11-20 IFP Energies Nouvelles Procédé de préparation d'une zéolithe de type structural MER
FR3101341B1 (fr) * 2019-09-26 2021-10-15 Ifp Energies Now Procede de preparation d’une zeolithe izm-2 en presence d’un structurant organique azote sous forme hydroxyde et d’un chlorure de metal alcalin, en milieu fluore ou non
FR3101342B1 (fr) 2019-09-26 2021-10-15 Ifp Energies Now Procede de preparation d’une zeolithe izm-2 en presence d’un melange de structurants organiques azotes sous forme hydroxyde et bromure et d’un chlorure de metal alcalin
CN110961148A (zh) * 2019-12-14 2020-04-07 中触媒新材料股份有限公司 一种aei/lev结构共生复合分子筛及其制备方法和scr应用
FR3109103A1 (fr) * 2020-04-08 2021-10-15 IFP Energies Nouvelles Méthode de synthèse de la zéolithe mordénite (MOR) de haut rapport Si/Al
FR3156130B1 (fr) * 2023-12-04 2025-11-14 Ifp Energies Now Synthese d’une zeolithe izm-2 en presence d’ethanol

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3222583A (en) * 1962-03-23 1965-12-07 Gen Electric Control systems
US5716593A (en) * 1996-07-31 1998-02-10 Chevron U.S.A. Inc. Preparation of Y-type faujasite using an organic template
ES2820232T3 (es) 2005-12-28 2021-04-20 Chevron Usa Inc Composición de materia de tamiz molecular SSZ-74
FR2918050B1 (fr) * 2007-06-29 2011-05-06 Inst Francais Du Petrole Solide cristallise izm-2 et son procede de preparation
FR2924110B1 (fr) * 2007-11-26 2010-02-26 Inst Francais Du Petrole Solide cristallise izm-3 et son procede de preparation
FR2934793B1 (fr) * 2008-08-08 2010-11-19 Inst Francais Du Petrole Catalyseur comprenant une zeolithe izm-2 et au moins un metal et son utilisation en transformation d'hydrocarbures
FR2934796B1 (fr) 2008-08-08 2010-09-03 Inst Francais Du Petrole Catalyseur a base de zeolithe izm-2 et procede d'hydroconversion/hydrocraquage de charges hydrocarbonees
FR2934795B1 (fr) 2008-08-08 2010-11-26 Inst Francais Du Petrole Catalyseur comprenant au moins une zeolithe izm-2 et son utilisation pour la transformation de charges hydrocarbonees
US9156706B2 (en) 2012-07-03 2015-10-13 Chevron U.S.A. Inc. Method for preparing high-silica LEV-type zeolites
CN104803396B (zh) * 2014-01-28 2017-09-26 中国石油化工股份有限公司 一种制备mww结构分子筛的方法
CN105271300B (zh) * 2014-07-02 2018-05-18 中国石油化工股份有限公司 一种分子筛催化剂、制备方法以及应用
US9802831B2 (en) 2014-07-23 2017-10-31 Chevron U.S.A. Inc. Synthesis of high silica zeolite via interzeolite transformation without OSDAs
US9938157B2 (en) * 2014-07-23 2018-04-10 Chevron U.S.A. Inc. Interzeolite transformation and metal encapsulation in the absence of an SDA
CN110540215B (zh) * 2014-11-21 2024-02-06 三菱化学株式会社 Aei型铝硅酸盐沸石、催化剂和废气处理方法

Also Published As

Publication number Publication date
CN108622915B (zh) 2023-03-10
EP3378830A1 (fr) 2018-09-26
JP7005399B2 (ja) 2022-01-21
US20180273393A1 (en) 2018-09-27
US10875778B2 (en) 2020-12-29
CN108622915A (zh) 2018-10-09
EP3378830B1 (fr) 2019-10-16
JP2018162206A (ja) 2018-10-18
FR3064262A1 (fr) 2018-09-28
ZA201801813B (en) 2019-01-30

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