FR2974582A1 - Procede de croissance de particules metalliques par electrodeposition avec inhibition in situ - Google Patents

Procede de croissance de particules metalliques par electrodeposition avec inhibition in situ Download PDF

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Publication number
FR2974582A1
FR2974582A1 FR1153606A FR1153606A FR2974582A1 FR 2974582 A1 FR2974582 A1 FR 2974582A1 FR 1153606 A FR1153606 A FR 1153606A FR 1153606 A FR1153606 A FR 1153606A FR 2974582 A1 FR2974582 A1 FR 2974582A1
Authority
FR
France
Prior art keywords
catalytic
conductive electrode
manufacturing
metal particles
metal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
FR1153606A
Other languages
English (en)
French (fr)
Inventor
Frederic Fouda-Onana
Nicolas Guillet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
King Saud University
Original Assignee
Commissariat a lEnergie Atomique CEA
Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
King Saud University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Commissariat a lEnergie Atomique CEA, Commissariat a lEnergie Atomique et aux Energies Alternatives CEA, King Saud University filed Critical Commissariat a lEnergie Atomique CEA
Priority to FR1153606A priority Critical patent/FR2974582A1/fr
Priority to US14/114,515 priority patent/US9391331B2/en
Priority to PCT/EP2012/057087 priority patent/WO2012146520A1/fr
Priority to EP12714335.2A priority patent/EP2702190B1/fr
Priority to JP2014506822A priority patent/JP6238889B2/ja
Priority to KR1020137028339A priority patent/KR102040338B1/ko
Priority to SA112330479A priority patent/SA112330479B1/ar
Publication of FR2974582A1 publication Critical patent/FR2974582A1/fr
Withdrawn legal-status Critical Current

Links

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/88—Processes of manufacture
    • H01M4/8825—Methods for deposition of the catalytic active composition
    • H01M4/8853—Electrodeposition
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D3/00—Electroplating: Baths therefor
    • C25D3/02—Electroplating: Baths therefor from solutions
    • C25D3/50—Electroplating: Baths therefor from solutions of platinum group metals
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D3/00—Electroplating: Baths therefor
    • C25D3/02—Electroplating: Baths therefor from solutions
    • C25D3/50—Electroplating: Baths therefor from solutions of platinum group metals
    • C25D3/52—Electroplating: Baths therefor from solutions of platinum group metals characterised by the organic bath constituents used
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/88—Processes of manufacture
    • H01M4/8803—Supports for the deposition of the catalytic active composition
    • H01M4/8807—Gas diffusion layers
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90—Selection of catalytic material
    • H01M4/92—Metals of platinum group
    • H01M4/921—Alloys or mixtures with metallic elements
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/10—Fuel cells with solid electrolytes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/10—Fuel cells with solid electrolytes
    • H01M2008/1095—Fuel cells with polymeric electrolytes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/50—Fuel cells

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Sustainable Energy (AREA)
  • Inert Electrodes (AREA)
  • Catalysts (AREA)
  • Electroplating Methods And Accessories (AREA)
  • Electrodes For Compound Or Non-Metal Manufacture (AREA)
  • Electroplating And Plating Baths Therefor (AREA)
FR1153606A 2011-04-27 2011-04-27 Procede de croissance de particules metalliques par electrodeposition avec inhibition in situ Withdrawn FR2974582A1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR1153606A FR2974582A1 (fr) 2011-04-27 2011-04-27 Procede de croissance de particules metalliques par electrodeposition avec inhibition in situ
US14/114,515 US9391331B2 (en) 2011-04-27 2012-04-18 Process for growing metal particles by electroplating with in situ inhibition
PCT/EP2012/057087 WO2012146520A1 (fr) 2011-04-27 2012-04-18 Procede de croissance de particules metalliques par electrodeposition avec inhibition in situ
EP12714335.2A EP2702190B1 (fr) 2011-04-27 2012-04-18 Procédé de croissance de particules métalliques par électrodéposition avec inhibition in situ
JP2014506822A JP6238889B2 (ja) 2011-04-27 2012-04-18 ｉｎｓｉｔｕ抑制を有する電気めっきによって金属粒子を成長させる方法
KR1020137028339A KR102040338B1 (ko) 2011-04-27 2012-04-18 인 시츄 억제를 갖는 전기도금에 의해 금속 입자들을 성장시키기 위한 프로세스
SA112330479A SA112330479B1 (ar) 2011-04-27 2012-04-25 عملية لزرع جسيمات معدنية بواسطة الطلاء بالكهرباء مع التثبيط في الموضع

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1153606A FR2974582A1 (fr) 2011-04-27 2011-04-27 Procede de croissance de particules metalliques par electrodeposition avec inhibition in situ

Publications (1)

Publication Number Publication Date
FR2974582A1 true FR2974582A1 (fr) 2012-11-02

Family

ID=45954687

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1153606A Withdrawn FR2974582A1 (fr) 2011-04-27 2011-04-27 Procede de croissance de particules metalliques par electrodeposition avec inhibition in situ

Country Status (7)

Country Link
US (1) US9391331B2 (https=)
EP (1) EP2702190B1 (https=)
JP (1) JP6238889B2 (https=)
KR (1) KR102040338B1 (https=)
FR (1) FR2974582A1 (https=)
SA (1) SA112330479B1 (https=)
WO (1) WO2012146520A1 (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6672210B2 (ja) 2017-03-21 2020-03-25 株式会社東芝 電気化学反応装置と電気化学反応方法
CN107188273A (zh) * 2017-04-27 2017-09-22 华中科技大学 一种三维碳基金属氧化物电催化电极的制备方法
CN113638017A (zh) * 2021-08-12 2021-11-12 深圳先进技术研究院 一种在金属导电图形上电镀Pt的方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4183790A (en) * 1977-07-22 1980-01-15 Noranda Mines Limited Electrolytic method of producing an active cobalt electrode for the evolution of hydrogen
US20060040157A1 (en) * 2004-07-28 2006-02-23 University Of South Carolina Development of a novel method for preparation of PEMFC electrodes
WO2007110246A2 (en) * 2006-03-29 2007-10-04 MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. Preparation of nanostructured metals and metal compounds and their uses
US20080251390A1 (en) * 2007-04-12 2008-10-16 Ming-Chi Tsai Process of electrodeposition platinum and platinum-based alloy nano-particles with addition of ethylene glycol
US20090202871A1 (en) * 2002-12-31 2009-08-13 Bose Rathindra N Metal-coated carbon surfaces for use in fuel cells

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB381932A (en) * 1931-07-11 1932-10-11 Mond Nickel Co Ltd Improvements relating to the electro-deposition of palladium
JPS5811000B2 (ja) * 1977-03-31 1983-02-28 新日本製鐵株式会社 水溶液の電解に用いる不溶性陽極の製造方法
US4401527A (en) * 1979-08-20 1983-08-30 Occidental Chemical Corporation Process for the electrodeposition of palladium
US4541905A (en) * 1983-12-13 1985-09-17 The Ohio State University Research Foundation Electrodes for use in electrocatalytic processes
US4778574A (en) * 1987-09-14 1988-10-18 American Chemical & Refining Company, Inc. Amine-containing bath for electroplating palladium
US5529680A (en) * 1990-06-29 1996-06-25 Electroplating Engineers Of Japan, Limited Platinum electroforming and platinum electroplating
US5084144A (en) 1990-07-31 1992-01-28 Physical Sciences Inc. High utilization supported catalytic metal-containing gas-diffusion electrode, process for making it, and cells utilizing it
EP0737760B1 (de) * 1995-04-15 2000-04-19 Degussa-Hüls Aktiengesellschaft Galvanisches Platinbad
US6863795B2 (en) * 2001-03-23 2005-03-08 Interuniversitair Microelektronica Centrum (Imec) Multi-step method for metal deposition
JP4894101B2 (ja) * 2001-07-19 2012-03-14 アイシン精機株式会社 色素増感型太陽電池の対極の製造方法、色素増感型太陽電池の製造方法
JP3949652B2 (ja) 2003-02-17 2007-07-25 Ｎｅｃエレクトロニクス株式会社 半導体装置の製造方法
JP4932370B2 (ja) * 2006-07-28 2012-05-16 日本マクダーミッド株式会社 電解めっき方法、プリント配線板及び半導体ウェハー
JP2009001846A (ja) * 2007-06-20 2009-01-08 Bridgestone Corp 貴金属の電気メッキ方法、貴金属担持導電性材料、固体高分子型燃料電池用電極及び固体高分子型燃料電池
WO2009076430A1 (en) * 2007-12-11 2009-06-18 Enthone Inc. Electrolytic deposition of metal-based composite coatings comprising nano-particles
US9034165B2 (en) * 2008-06-23 2015-05-19 Brookhaven Science Associates, Llc Underpotential deposition-mediated layer-by-layer growth of thin films
EP2261398B1 (en) * 2009-06-10 2018-12-05 Universität des Saarlandes Metal foams
CN101928979B (zh) * 2010-08-06 2012-07-04 厦门大学 金属纳米催化剂的表面结构调控和制备方法
FR2998814B1 (fr) * 2012-11-30 2015-05-08 Eurecat Sa Procede de preparation de catalyseurs metalliques supportes

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4183790A (en) * 1977-07-22 1980-01-15 Noranda Mines Limited Electrolytic method of producing an active cobalt electrode for the evolution of hydrogen
US20090202871A1 (en) * 2002-12-31 2009-08-13 Bose Rathindra N Metal-coated carbon surfaces for use in fuel cells
US20060040157A1 (en) * 2004-07-28 2006-02-23 University Of South Carolina Development of a novel method for preparation of PEMFC electrodes
WO2007110246A2 (en) * 2006-03-29 2007-10-04 MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. Preparation of nanostructured metals and metal compounds and their uses
US20080251390A1 (en) * 2007-04-12 2008-10-16 Ming-Chi Tsai Process of electrodeposition platinum and platinum-based alloy nano-particles with addition of ethylene glycol

Also Published As

Publication number Publication date
US20140048419A1 (en) 2014-02-20
JP2014516389A (ja) 2014-07-10
SA112330479B1 (ar) 2015-12-20
KR102040338B1 (ko) 2019-11-04
EP2702190B1 (fr) 2015-05-27
JP6238889B2 (ja) 2017-11-29
WO2012146520A1 (fr) 2012-11-01
KR20140029418A (ko) 2014-03-10
US9391331B2 (en) 2016-07-12
EP2702190A1 (fr) 2014-03-05

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