FR2776293B1 - Nouveaux aminophosphonates et utilisation d'aminophosphonates comme marqueurs de ph et rmn du 31p - Google Patents

Nouveaux aminophosphonates et utilisation d'aminophosphonates comme marqueurs de ph et rmn du 31p

Info

Publication number
FR2776293B1
FR2776293B1 FR9803317A FR9803317A FR2776293B1 FR 2776293 B1 FR2776293 B1 FR 2776293B1 FR 9803317 A FR9803317 A FR 9803317A FR 9803317 A FR9803317 A FR 9803317A FR 2776293 B1 FR2776293 B1 FR 2776293B1
Authority
FR
France
Prior art keywords
aminophosphonates
markers
nmr
novel
novel aminophosphonates
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR9803317A
Other languages
English (en)
Other versions
FR2776293A1 (fr
Inventor
Sylvia Pietri
Moigne Francois Le
Malvina Miollan
Marcel Culcasi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Centre National de la Recherche Scientifique CNRS
Original Assignee
Centre National de la Recherche Scientifique CNRS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Centre National de la Recherche Scientifique CNRS filed Critical Centre National de la Recherche Scientifique CNRS
Priority to FR9803317A priority Critical patent/FR2776293B1/fr
Priority to US09/646,430 priority patent/US6528656B1/en
Priority to PCT/FR1999/000631 priority patent/WO1999047527A1/fr
Priority to JP2000536722A priority patent/JP2002506871A/ja
Priority to EP99909041A priority patent/EP1064287A1/fr
Publication of FR2776293A1 publication Critical patent/FR2776293A1/fr
Application granted granted Critical
Publication of FR2776293B1 publication Critical patent/FR2776293B1/fr
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic System
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids RP(=O)(OH)2; Thiophosphonic acids, i.e. RP(=X)(XH)2 (X = S, Se)
    • C07F9/40—Esters thereof
    • C07F9/4003—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
    • C07F9/4006—Esters of acyclic acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic System
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids RP(=O)(OH)2; Thiophosphonic acids, i.e. RP(=X)(XH)2 (X = S, Se)
    • C07F9/3804—Phosphonic acids RP(=O)(OH)2; Thiophosphonic acids, i.e. RP(=X)(XH)2 (X = S, Se) not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic System
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
    • C07F9/572—Five-membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/05—Isotopically modified compounds, e.g. labelled
FR9803317A 1998-03-18 1998-03-18 Nouveaux aminophosphonates et utilisation d'aminophosphonates comme marqueurs de ph et rmn du 31p Expired - Fee Related FR2776293B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR9803317A FR2776293B1 (fr) 1998-03-18 1998-03-18 Nouveaux aminophosphonates et utilisation d'aminophosphonates comme marqueurs de ph et rmn du 31p
US09/646,430 US6528656B1 (en) 1998-03-18 1999-03-18 Linear or cyclic aminophosphonates as pH markers in phosphorus 31 NMR spectroscopy
PCT/FR1999/000631 WO1999047527A1 (fr) 1998-03-18 1999-03-18 UTILISATION D'AMINOPHOSPHONATES COMME MARQUEURS DE pH EN RMN DU 31P
JP2000536722A JP2002506871A (ja) 1998-03-18 1999-03-18 ３１ＰＮＭＲにおけるｐＨマーカーとしてのアミノホスホネートの使用
EP99909041A EP1064287A1 (fr) 1998-03-18 1999-03-18 Utilisation d'aminophosphonates comme marqueurs de ph en rmn du 31 p

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9803317A FR2776293B1 (fr) 1998-03-18 1998-03-18 Nouveaux aminophosphonates et utilisation d'aminophosphonates comme marqueurs de ph et rmn du 31p

Publications (2)

Publication Number Publication Date
FR2776293A1 FR2776293A1 (fr) 1999-09-24
FR2776293B1 true FR2776293B1 (fr) 2002-10-04

Family

ID=9524189

Family Applications (1)

Application Number Title Priority Date Filing Date
FR9803317A Expired - Fee Related FR2776293B1 (fr) 1998-03-18 1998-03-18 Nouveaux aminophosphonates et utilisation d'aminophosphonates comme marqueurs de ph et rmn du 31p

Country Status (5)

Country Link
US (1) US6528656B1 (fr)
EP (1) EP1064287A1 (fr)
JP (1) JP2002506871A (fr)
FR (1) FR2776293B1 (fr)
WO (1) WO1999047527A1 (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9335285B2 (en) * 2013-10-18 2016-05-10 Exxonmobil Chemical Patents Inc. Method for measuring acid strength in reaction medium using trimethylphosphine oxide and 31P NMR

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2635112A (en) * 1949-07-28 1953-04-14 Research Corp Process for producing aminomethylphosphonic acid compounds
BE628184A (fr) * 1962-02-08
GB1354343A (en) * 1971-09-07 1974-06-05 Bitterfeld Chemie Herbicidal compositions
US3907652A (en) * 1974-10-30 1975-09-23 Monsanto Co Electrooxidation of phosphonomethyl amines
US4005160A (en) * 1975-05-05 1977-01-25 Petrolite Corporation Preparation of α-amino phosphonic acid derivatives
PL112289B2 (en) * 1978-11-30 1980-10-31 Process for preparing novel dipeptides of aminophosphonic acids
SE455259B (sv) * 1984-01-30 1988-07-04 Kenogard Ab Anvendning av vissa aminoalkanfosfonsyror for bekempning av svampsjukdomar hos vexter
DE3445300A1 (de) * 1984-12-12 1986-06-12 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von (alpha)-aminoalkylphosphon- und (alpha)-aminoalkylphosphinsaeuren
PL148859B1 (en) * 1987-04-23 1989-12-30 Method of obtaining aminophosphonic esters
FR2639350B1 (fr) * 1988-11-21 1990-12-21 Commissariat Energie Atomique Radical nitroxyde, son procede de fabrication et son application en magnetometrie
KR930005009B1 (ko) * 1990-03-27 1993-06-11 한국과학기술연구원 N-알킬치환아미노메틸포스폰산 유도체의 제조방법
FR2707990B1 (fr) * 1993-07-20 1995-10-20 Centre Nat Rech Scient Nouvelles nitrones utilisables pour le piégeage des radicaux libres.
US5508463A (en) * 1994-03-17 1996-04-16 Trustees Of The University Of Pennsylvania α-aminophosphonates

Also Published As

Publication number Publication date
FR2776293A1 (fr) 1999-09-24
WO1999047527A1 (fr) 1999-09-23
JP2002506871A (ja) 2002-03-05
US6528656B1 (en) 2003-03-04
EP1064287A1 (fr) 2001-01-03

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