FR2467177A1 - Procede de fabrication de charbons actifs a surface specifique elevee a partir de brai de petrole - Google Patents
Procede de fabrication de charbons actifs a surface specifique elevee a partir de brai de petrole Download PDFInfo
- Publication number
- FR2467177A1 FR2467177A1 FR7925143A FR7925143A FR2467177A1 FR 2467177 A1 FR2467177 A1 FR 2467177A1 FR 7925143 A FR7925143 A FR 7925143A FR 7925143 A FR7925143 A FR 7925143A FR 2467177 A1 FR2467177 A1 FR 2467177A1
- Authority
- FR
- France
- Prior art keywords
- pitch
- temperature
- petroleum
- weight
- carbonization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 32
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 14
- 239000011301 petroleum pitch Substances 0.000 title claims abstract description 10
- 239000011295 pitch Substances 0.000 claims abstract description 104
- 238000000034 method Methods 0.000 claims abstract description 54
- 239000011347 resin Substances 0.000 claims abstract description 29
- 229920005989 resin Polymers 0.000 claims abstract description 29
- 239000003208 petroleum Substances 0.000 claims abstract description 14
- 230000003750 conditioning effect Effects 0.000 claims abstract description 3
- 238000011282 treatment Methods 0.000 claims description 38
- 238000003763 carbonization Methods 0.000 claims description 27
- 238000001994 activation Methods 0.000 claims description 22
- 230000004913 activation Effects 0.000 claims description 22
- 238000010438 heat treatment Methods 0.000 claims description 22
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 16
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 14
- 239000002904 solvent Substances 0.000 claims description 13
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 11
- 239000001301 oxygen Substances 0.000 claims description 11
- 229910052760 oxygen Inorganic materials 0.000 claims description 11
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims description 10
- 239000011261 inert gas Substances 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 239000006260 foam Substances 0.000 claims description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 8
- 238000005336 cracking Methods 0.000 claims description 7
- 239000008187 granular material Substances 0.000 claims description 7
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- 239000010426 asphalt Substances 0.000 claims description 6
- 239000000284 extract Substances 0.000 claims description 6
- 229920005610 lignin Polymers 0.000 claims description 6
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 5
- 239000010779 crude oil Substances 0.000 claims description 5
- 238000000354 decomposition reaction Methods 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- 230000001590 oxidative effect Effects 0.000 claims description 5
- 239000003209 petroleum derivative Substances 0.000 claims description 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
- 239000001569 carbon dioxide Substances 0.000 claims description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 4
- 238000004821 distillation Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 4
- 238000005292 vacuum distillation Methods 0.000 claims description 4
- 239000004604 Blowing Agent Substances 0.000 claims description 3
- 239000003570 air Substances 0.000 claims description 3
- 238000006356 dehydrogenation reaction Methods 0.000 claims description 3
- 239000007800 oxidant agent Substances 0.000 claims description 3
- 238000004230 steam cracking Methods 0.000 claims description 3
- 238000006277 sulfonation reaction Methods 0.000 claims description 3
- 238000004227 thermal cracking Methods 0.000 claims description 3
- 239000011592 zinc chloride Substances 0.000 claims description 3
- 235000005074 zinc chloride Nutrition 0.000 claims description 3
- 229910019142 PO4 Inorganic materials 0.000 claims description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
- 229910052786 argon Inorganic materials 0.000 claims description 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 2
- 238000004523 catalytic cracking Methods 0.000 claims description 2
- 239000003153 chemical reaction reagent Substances 0.000 claims description 2
- 150000001805 chlorine compounds Chemical class 0.000 claims description 2
- 230000000295 complement effect Effects 0.000 claims description 2
- 238000000227 grinding Methods 0.000 claims description 2
- 150000004679 hydroxides Chemical class 0.000 claims description 2
- 239000000155 melt Substances 0.000 claims description 2
- 235000021317 phosphate Nutrition 0.000 claims description 2
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 2
- 230000005070 ripening Effects 0.000 claims description 2
- 229930195734 saturated hydrocarbon Natural products 0.000 claims description 2
- 239000010902 straw Substances 0.000 claims description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 1
- 150000001342 alkaline earth metals Chemical class 0.000 claims 1
- 230000001143 conditioned effect Effects 0.000 claims 1
- 239000002274 desiccant Substances 0.000 claims 1
- 230000003213 activating effect Effects 0.000 abstract description 3
- 239000000047 product Substances 0.000 description 26
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 239000007789 gas Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 5
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 4
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 4
- 238000007664 blowing Methods 0.000 description 4
- 239000003245 coal Substances 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 239000012530 fluid Substances 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 229910052717 sulfur Inorganic materials 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- 238000004438 BET method Methods 0.000 description 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 239000003575 carbonaceous material Substances 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- TWXDDNPPQUTEOV-FVGYRXGTSA-N methamphetamine hydrochloride Chemical compound Cl.CN[C@@H](C)CC1=CC=CC=C1 TWXDDNPPQUTEOV-FVGYRXGTSA-N 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- XPFVYQJUAUNWIW-UHFFFAOYSA-N furfuryl alcohol Chemical compound OCC1=CC=CO1 XPFVYQJUAUNWIW-UHFFFAOYSA-N 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 238000001033 granulometry Methods 0.000 description 1
- -1 hard and soft coals Substances 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000002198 insoluble material Substances 0.000 description 1
- 239000003077 lignite Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 125000000896 monocarboxylic acid group Chemical group 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003415 peat Substances 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 239000011269 tar Substances 0.000 description 1
- 238000007725 thermal activation Methods 0.000 description 1
- 238000001029 thermal curing Methods 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10C—WORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
- C10C3/00—Working-up pitch, asphalt, bitumen
- C10C3/002—Working-up pitch, asphalt, bitumen by thermal means
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/318—Preparation characterised by the starting materials
- C01B32/33—Preparation characterised by the starting materials from distillation residues of coal or petroleum; from petroleum acid sludge
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/354—After-treatment
- C01B32/382—Making shaped products, e.g. fibres, spheres, membranes or foam
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/354—After-treatment
- C01B32/384—Granulation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Carbon And Carbon Compounds (AREA)
- Working-Up Tar And Pitch (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7925143A FR2467177A1 (fr) | 1979-10-09 | 1979-10-09 | Procede de fabrication de charbons actifs a surface specifique elevee a partir de brai de petrole |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7925143A FR2467177A1 (fr) | 1979-10-09 | 1979-10-09 | Procede de fabrication de charbons actifs a surface specifique elevee a partir de brai de petrole |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2467177A1 true FR2467177A1 (fr) | 1981-04-17 |
| FR2467177B1 FR2467177B1 (OSRAM) | 1981-10-30 |
Family
ID=9230501
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7925143A Granted FR2467177A1 (fr) | 1979-10-09 | 1979-10-09 | Procede de fabrication de charbons actifs a surface specifique elevee a partir de brai de petrole |
Country Status (1)
| Country | Link |
|---|---|
| FR (1) | FR2467177A1 (OSRAM) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3221367A1 (de) * | 1981-06-09 | 1983-01-13 | The British Petroleum Co. P.L.C., London | Verfahren zur herstellung von kohlenstoff-fasern aus erdoelpech |
| FR2801297A1 (fr) * | 1999-11-19 | 2001-05-25 | Centre Nat Rech Scient | Charbons actifs et leur procede d'obtention a partir d'un brai partiellement mesophase et partiellement mesogene |
| EP1518825A3 (en) * | 2003-09-25 | 2006-09-27 | Kureha Corporation | Process for producing spherical activated carbon |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2932619A (en) * | 1957-03-05 | 1960-04-12 | Sinclair Refining Co | Production of adsorptive charcoal from petroleum residual stocks containing asphaltenes |
| DE2202174A1 (de) * | 1971-08-27 | 1973-03-15 | Kureha Chemical Ind Co Ltd | Verfahren zur herstellung von mikrokugelfoermigem kohlenstoff und aktivkohle |
| FR2250571A1 (OSRAM) * | 1973-11-12 | 1975-06-06 | British Petroleum Co | |
| FR2250705A1 (en) * | 1973-11-09 | 1975-06-06 | Kureha Chemical Ind Co Ltd | Porous activated carbon prepn - by shaping pitch in aromatic hydrocarbon, extracting hydrocarbon, oxidising and calcining |
| GB1444732A (en) * | 1973-09-04 | 1976-08-04 | Shell Int Research | Production of active carbon |
| FR2325712A1 (fr) * | 1975-09-29 | 1977-04-22 | British Petroleum Co | Procede de fabrication en deux stades pour brai de petrole pour coke siderurgique |
| FR2411811A1 (fr) * | 1977-12-14 | 1979-07-13 | British Petroleum Co | Procede de fabrication de mousses de carbone et de graphite a partir de mousses de brais |
| FR2411875A1 (fr) * | 1977-12-14 | 1979-07-13 | British Petroleum Co | Mousses de brais et leur procede de preparation |
-
1979
- 1979-10-09 FR FR7925143A patent/FR2467177A1/fr active Granted
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2932619A (en) * | 1957-03-05 | 1960-04-12 | Sinclair Refining Co | Production of adsorptive charcoal from petroleum residual stocks containing asphaltenes |
| DE2202174A1 (de) * | 1971-08-27 | 1973-03-15 | Kureha Chemical Ind Co Ltd | Verfahren zur herstellung von mikrokugelfoermigem kohlenstoff und aktivkohle |
| GB1444732A (en) * | 1973-09-04 | 1976-08-04 | Shell Int Research | Production of active carbon |
| FR2250705A1 (en) * | 1973-11-09 | 1975-06-06 | Kureha Chemical Ind Co Ltd | Porous activated carbon prepn - by shaping pitch in aromatic hydrocarbon, extracting hydrocarbon, oxidising and calcining |
| FR2250571A1 (OSRAM) * | 1973-11-12 | 1975-06-06 | British Petroleum Co | |
| FR2325712A1 (fr) * | 1975-09-29 | 1977-04-22 | British Petroleum Co | Procede de fabrication en deux stades pour brai de petrole pour coke siderurgique |
| FR2411811A1 (fr) * | 1977-12-14 | 1979-07-13 | British Petroleum Co | Procede de fabrication de mousses de carbone et de graphite a partir de mousses de brais |
| FR2411875A1 (fr) * | 1977-12-14 | 1979-07-13 | British Petroleum Co | Mousses de brais et leur procede de preparation |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3221367A1 (de) * | 1981-06-09 | 1983-01-13 | The British Petroleum Co. P.L.C., London | Verfahren zur herstellung von kohlenstoff-fasern aus erdoelpech |
| FR2509331A1 (fr) * | 1981-06-09 | 1983-01-14 | British Petroleum Co | Procede de production de fibres de carbone ou de graphite a partir de brai de petrole |
| FR2801297A1 (fr) * | 1999-11-19 | 2001-05-25 | Centre Nat Rech Scient | Charbons actifs et leur procede d'obtention a partir d'un brai partiellement mesophase et partiellement mesogene |
| WO2001036326A1 (fr) * | 1999-11-19 | 2001-05-25 | Centre National De La Recherche Scientifique | Charbons actifs et leur procede d'obtention a partir d'un brai partiellement mesophase et partiellement mesogene |
| US7105083B1 (en) | 1999-11-19 | 2006-09-12 | Centre National De La Recherche Scientifique | Activated carbons and method for obtaining same from a partly mesophase and partly mesogenic pitch |
| EP1518825A3 (en) * | 2003-09-25 | 2006-09-27 | Kureha Corporation | Process for producing spherical activated carbon |
| US7781370B2 (en) | 2003-09-25 | 2010-08-24 | Kureha Corporation | Process for producing spherical activated carbon |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2467177B1 (OSRAM) | 1981-10-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |