FR2450818A1 - Procede de production de derives de pyridine comportant un groupe trifluoromethyle en position b, a partir de la b-picoline - Google Patents
Procede de production de derives de pyridine comportant un groupe trifluoromethyle en position b, a partir de la b-picolineInfo
- Publication number
- FR2450818A1 FR2450818A1 FR8004969A FR8004969A FR2450818A1 FR 2450818 A1 FR2450818 A1 FR 2450818A1 FR 8004969 A FR8004969 A FR 8004969A FR 8004969 A FR8004969 A FR 8004969A FR 2450818 A1 FR2450818 A1 FR 2450818A1
- Authority
- FR
- France
- Prior art keywords
- pyridine derivatives
- picoline
- production
- trifluoromethyl group
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical class C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 title abstract 3
- -1 TRIFLUOROMETHYL GROUP Chemical group 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 abstract 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 229940126601 medicinal product Drugs 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 239000012808 vapor phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/61—Halogen atoms or nitro radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D213/26—Radicals substituted by halogen atoms or nitro radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2736979A JPS55120564A (en) | 1979-03-09 | 1979-03-09 | Production of chloro-beta-trifluoromethylpyridines |
| JP4473379A JPS55147261A (en) | 1979-04-12 | 1979-04-12 | Preparation of chloro-beta-trifluoromethylpyridines |
| JP13605779A JPS5659757A (en) | 1979-10-22 | 1979-10-22 | Preparation of 2-chloro-5-trifluoromethylpyridine |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2450818A1 true FR2450818A1 (fr) | 1980-10-03 |
| FR2450818B1 FR2450818B1 (enExample) | 1984-03-02 |
Family
ID=27285760
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR8004969A Granted FR2450818A1 (fr) | 1979-03-09 | 1980-03-05 | Procede de production de derives de pyridine comportant un groupe trifluoromethyle en position b, a partir de la b-picoline |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US4288599A (enExample) |
| AU (1) | AU532020B2 (enExample) |
| BE (1) | BE882121A (enExample) |
| BR (1) | BR8001398A (enExample) |
| CA (1) | CA1125290A (enExample) |
| CH (1) | CH643543A5 (enExample) |
| DE (1) | DE3008081A1 (enExample) |
| FR (1) | FR2450818A1 (enExample) |
| GB (1) | GB2045245B (enExample) |
| IE (1) | IE49188B1 (enExample) |
| IT (1) | IT1129728B (enExample) |
| NL (1) | NL191149C (enExample) |
| NZ (1) | NZ192948A (enExample) |
| PL (1) | PL123917B1 (enExample) |
| SG (1) | SG83484G (enExample) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0107866B1 (en) * | 1977-08-12 | 1988-03-30 | Imperial Chemical Industries Plc | Trihalomethylpyridine compounds |
| JPS579762A (en) * | 1980-06-19 | 1982-01-19 | Ishihara Sangyo Kaisha Ltd | Production of trifluoromethylpyridine |
| JPS57159768A (en) * | 1981-03-27 | 1982-10-01 | Ishihara Sangyo Kaisha Ltd | Preparation of beta-trifluoromethylpyridine compound |
| AU548249B2 (en) | 1981-05-13 | 1985-12-05 | Imperial Chemical Industries Plc | Production of 3-trichloromethyl and 3-trifluoro methyl- pyridines |
| EP0078234B1 (de) * | 1981-10-20 | 1990-07-04 | Ciba-Geigy Ag | 5-Halogenalkyl-pyridine |
| JPS5877863A (ja) * | 1981-11-04 | 1983-05-11 | Ishihara Sangyo Kaisha Ltd | ３―クロロ―５―トリフルオロメチルピリジン系化合物の製造方法 |
| US4650875A (en) * | 1983-05-09 | 1987-03-17 | The Dow Chemical Company | Preparation of (trifluoromethyl)pyridines |
| US4590279A (en) * | 1982-11-26 | 1986-05-20 | The Dow Chemical Company | Preparation of (trifluoromethyl)pyridines under liquid phase conditions |
| FR2569191B1 (fr) * | 1984-08-20 | 1987-07-10 | Solvay | Procede pour la preparation de derives chlores de composes pyridiniques et initiateurs radicalaires utilises dans ce procede |
| DE3934957A1 (de) * | 1989-10-20 | 1991-04-25 | Bayer Ag | Verfahren zur herstellung von 3-trichlormethyl-pyridin |
| SE0200979D0 (sv) * | 2002-03-28 | 2002-03-28 | Astrazeneca Ab | New compounds |
| KR101196095B1 (ko) * | 2004-04-26 | 2012-11-01 | 다우 아그로사이언시즈 엘엘씨 | β-피콜린의 증기 상 촉매 염소화 반응 |
| CN103763923B (zh) * | 2011-06-30 | 2016-08-17 | 陶氏益农公司 | 3-烷氧基-4-氨基-6-(取代的)吡啶甲酸酯、3-硫代烷基-4-氨基-6-(取代的)吡啶甲酸酯和3-氨基-4-氨基-6-(取代的)吡啶甲酸酯以及它们作为除草剂的用途 |
| CN102875454B (zh) * | 2012-10-17 | 2014-10-22 | 山东绿霸化工股份有限公司 | 2-氯-5-三氟甲基吡啶和2-氯-3-三氟甲基吡啶的合成方法 |
| EP3608309B1 (en) * | 2017-04-04 | 2022-07-13 | Ishihara Sangyo Kaisha, Ltd. | Method for purifying trifluoromethylpyridine compound |
| CN109456257B (zh) * | 2017-09-06 | 2020-04-28 | 新发药业有限公司 | 一种高收率2-氯-5-硝基吡啶的制备方法 |
| CN110003097B (zh) * | 2018-01-05 | 2020-11-17 | 浙江省化工研究院有限公司 | 一种两段法制备2-氯-5-三氟甲基吡啶的方法 |
| CN110003096B (zh) * | 2018-01-05 | 2020-11-17 | 浙江省化工研究院有限公司 | 一种制备2-氯-5-三氟甲基吡啶的方法 |
| CN110003098B (zh) * | 2018-01-05 | 2020-11-17 | 浙江省化工研究院有限公司 | 一种3-三氟甲基吡啶气相催化氯化制备2-氯-5-三氟甲基吡啶的方法 |
| EP3620451B1 (en) | 2017-12-06 | 2022-09-21 | Zhejiang Lantian Environmental Protection Hi-Tech Co., Ltd. | Method for preparing 2,3-dichloro-5-trifluoromethylpyridine with high selectivity |
| EP3696168B1 (en) * | 2018-01-05 | 2022-09-21 | Zhejiang Lantian Environmental Protection Hi-Tech Co., Ltd. | Method for preparation of 2-chloro-5-trifluoromethylpyridine |
| CN108997203B (zh) * | 2018-06-26 | 2020-08-14 | 江苏扬农化工集团有限公司 | 一种2,3-二氯-5-三氟甲基吡啶的高效提纯方法 |
| US10815198B2 (en) | 2018-08-07 | 2020-10-27 | Ishihara Sangyo Kaisha, Ltd. | Method for separating and purifying 2-chloro-3-trifluoromethylpyridine |
| CN111170933B (zh) * | 2018-11-12 | 2021-07-20 | 新发药业有限公司 | 一种2-氯-5-硝基吡啶的制备方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2375168A1 (fr) * | 1976-12-27 | 1978-07-21 | Daikin Ind Ltd | Procede de preparation de l'a,a,a-trifluorotoluene et de ses derives |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2516402A (en) * | 1945-09-04 | 1950-07-25 | Purdue Research Foundation | Fluoromethylpyridines |
| NL132136C (enExample) * | 1964-08-05 | |||
| CA1247625A (en) * | 1977-07-22 | 1988-12-28 | Howard Johnston | Trifluoromethyl pyridinyloxyphenoxy propanoic acids and propanols and derivatives thereof and methods of herbicidal use |
| EP0107866B1 (en) * | 1977-08-12 | 1988-03-30 | Imperial Chemical Industries Plc | Trihalomethylpyridine compounds |
-
1980
- 1980-02-22 NZ NZ192948A patent/NZ192948A/xx unknown
- 1980-02-26 US US06/124,757 patent/US4288599A/en not_active Expired - Lifetime
- 1980-03-03 DE DE19803008081 patent/DE3008081A1/de active Granted
- 1980-03-05 FR FR8004969A patent/FR2450818A1/fr active Granted
- 1980-03-05 NL NL8001312A patent/NL191149C/xx not_active IP Right Cessation
- 1980-03-06 AU AU56191/80A patent/AU532020B2/en not_active Expired
- 1980-03-06 GB GB8007700A patent/GB2045245B/en not_active Expired
- 1980-03-07 IE IE475/80A patent/IE49188B1/en not_active IP Right Cessation
- 1980-03-07 CH CH184380A patent/CH643543A5/de not_active IP Right Cessation
- 1980-03-07 PL PL1980222533A patent/PL123917B1/pl unknown
- 1980-03-07 IT IT20423/80A patent/IT1129728B/it active
- 1980-03-07 CA CA347,229A patent/CA1125290A/en not_active Expired
- 1980-03-07 BE BE0/199706A patent/BE882121A/fr not_active IP Right Cessation
- 1980-03-10 BR BR8001398A patent/BR8001398A/pt not_active IP Right Cessation
-
1984
- 1984-11-23 SG SG834/84A patent/SG83484G/en unknown
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2375168A1 (fr) * | 1976-12-27 | 1978-07-21 | Daikin Ind Ltd | Procede de preparation de l'a,a,a-trifluorotoluene et de ses derives |
Also Published As
| Publication number | Publication date |
|---|---|
| AU532020B2 (en) | 1983-09-15 |
| IT1129728B (it) | 1986-06-11 |
| IE800475L (en) | 1981-09-09 |
| IT8020423A0 (it) | 1980-03-07 |
| US4288599A (en) | 1981-09-08 |
| GB2045245A (en) | 1980-10-29 |
| PL123917B1 (en) | 1982-12-31 |
| SG83484G (en) | 1985-09-13 |
| FR2450818B1 (enExample) | 1984-03-02 |
| GB2045245B (en) | 1983-03-30 |
| NL8001312A (nl) | 1980-09-11 |
| NL191149C (nl) | 1995-02-16 |
| PL222533A1 (enExample) | 1981-01-02 |
| IE49188B1 (en) | 1985-08-21 |
| DE3008081A1 (de) | 1980-09-11 |
| NZ192948A (en) | 1982-02-23 |
| NL191149B (nl) | 1994-09-16 |
| DE3008081C2 (enExample) | 1989-10-05 |
| BR8001398A (pt) | 1980-11-11 |
| BE882121A (fr) | 1980-09-08 |
| AU5619180A (en) | 1980-09-11 |
| CH643543A5 (de) | 1984-06-15 |
| CA1125290A (en) | 1982-06-08 |
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