FR2398021A1 - Procede pour la preparation de bioxyde de silicium pur et poreux - Google Patents

Procede pour la preparation de bioxyde de silicium pur et poreux

Info

Publication number
FR2398021A1
FR2398021A1 FR7820656A FR7820656A FR2398021A1 FR 2398021 A1 FR2398021 A1 FR 2398021A1 FR 7820656 A FR7820656 A FR 7820656A FR 7820656 A FR7820656 A FR 7820656A FR 2398021 A1 FR2398021 A1 FR 2398021A1
Authority
FR
France
Prior art keywords
preparation
support
catalysts
pure
porous silicon
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7820656A
Other languages
English (en)
Other versions
FR2398021B1 (fr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stamicarbon BV
Original Assignee
Stamicarbon BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stamicarbon BV filed Critical Stamicarbon BV
Publication of FR2398021A1 publication Critical patent/FR2398021A1/fr
Application granted granted Critical
Publication of FR2398021B1 publication Critical patent/FR2398021B1/fr
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/16Preparation of silica xerogels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24Chromium, molybdenum or tungsten
    • B01J23/26Chromium
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F10/00Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S526/00Synthetic resins or natural rubbers -- part of the class 520 series
    • Y10S526/906Comminution of transition metal containing catalyst
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S526/00Synthetic resins or natural rubbers -- part of the class 520 series
    • Y10S526/908Containing catalyst of specified particle size

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Materials Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
  • Silicon Compounds (AREA)
  • Catalysts (AREA)
  • Polymerization Catalysts (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

L'invention concerne un procédé de préparation de bioxyde de silicium pur et poreux qui convient en particulier comme support de catalyseurs et elle concerne ensuite la préparation de catalyseurs du type oxyde chromique sur support Le bioxyde de silicium, qui est obtenu par la conversion d'un composé d'halogène de silicium avec un gaz combustible contenant de l'hydrogène est converti en un gel à l'aide d'eau, auquel on peut ajouter un agent de réticulation. Le gel est converti en le séchant par pulverisation en un xerogel, qui est utilisable comme support de catalyseurs. Les catalyseurs du type oxyde chromique - sur support pour la polymérisation d'oléfines - sont préparés en mettant un composé de chrome, par exemple, sous forme de solution sur le support, après quoi le support imprégné est activé par chauffage dans une atmosphère non réductrice.
FR7820656A 1977-07-18 1978-07-11 Procede pour la preparation de bioxyde de silicium pur et poreux Granted FR2398021A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL7707961A NL7707961A (nl) 1977-07-18 1977-07-18 Werkwijze ter bereiding van poreus, zuiver siliciumdioxyde.

Publications (2)

Publication Number Publication Date
FR2398021A1 true FR2398021A1 (fr) 1979-02-16
FR2398021B1 FR2398021B1 (fr) 1982-07-30

Family

ID=19828897

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7820656A Granted FR2398021A1 (fr) 1977-07-18 1978-07-11 Procede pour la preparation de bioxyde de silicium pur et poreux

Country Status (12)

Country Link
US (2) US4225464A (fr)
JP (1) JPS5421992A (fr)
AT (1) AT373853B (fr)
BE (1) BE868792A (fr)
CA (1) CA1126244A (fr)
DE (1) DE2831561A1 (fr)
ES (1) ES471789A1 (fr)
FR (1) FR2398021A1 (fr)
GB (1) GB2001044B (fr)
IT (1) IT1107453B (fr)
NL (2) NL7707961A (fr)
SE (1) SE7807949L (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003054089A1 (fr) * 2001-12-21 2003-07-03 Degussa Ag Granules a base de dioxyde de silicium obtenus par pyrogenese, fabrication et utilisation

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4301034A (en) * 1980-05-21 1981-11-17 Phillips Petroleum Company Silica from single phase controlled hydrolysis of silicate ester
NL8005856A (nl) * 1980-10-24 1982-05-17 Stamicarbon Bereiding van poreus, zuiver siliciumdioxyde en van chroomoxyde-op-siliciumdioxyde katalysatoren.
US4482635A (en) * 1982-03-29 1984-11-13 E. I. Du Pont De Nemours & Company Composition, indicator, process and device for detecting carbon monoxide
DE3525495C1 (de) * 1985-07-17 1987-01-02 Heraeus Schott Quarzschmelze Verfahren zur Herstellung von Gegenstaenden aus synthetischem Siliziumdioxid
NL8901893A (nl) * 1989-07-21 1991-02-18 Veg Gasinstituut Nv Katalysator voor de selectieve oxidatie van zwavelverbindingen tot elementaire zwavel, werkwijze voor de bereiding van een dergelijke katalysator en werkwijze voor de selectieve oxidatie van zwavelverbindingen tot elementaire zwavel.
IT1240673B (it) * 1990-04-24 1993-12-17 Tenav Microsfere di aerogels di ossidi inorganici a stretta distribuzione dei diametri dei pori e metodo per la loro preparazione
BE1005718A3 (fr) * 1992-03-10 1993-12-28 Solvay Procede pour la fabrication d'une poudre microspheroidale a faible dispersite, poudre microspheroidale a faible dispersite ainsi obtenue, catalyseurs pour la polymerisation d'alpha-olefines et procede de polymerisation d'alpha-olefines.
GB9210265D0 (en) * 1992-05-13 1992-07-01 Unilever Plc Catalysts and catalyst supports
BE1007148A3 (fr) * 1993-05-17 1995-04-11 Solvay Support pour catalyseurs, procede pour la fabrication d'un gel precurseur d'un support pour catalyseurs, procede de preparation d'un support pour catalyseurs, catalyseur pour la polymerisation d'olefines et procede pour la polymerisation d'olefines au moyen de ce catalyseur.
WO1995017347A1 (fr) * 1993-12-23 1995-06-29 Ppg Industries, Inc. Aerogel de silice produit dans des conditions sous-critiques
DE19516253A1 (de) * 1995-04-26 1996-10-31 Grace Gmbh Mattierungsmittel auf Basis von aggregiertem Siliciumdioxid mit verbesserter Effizienz
DE69717441T2 (de) 1996-06-21 2003-10-02 W.R. Grace & Co.-Conn., New York Zerbrechlicher sprühgetrockneter agglomeratträger, verfahren zur herstellung solcher träger und darauf angebrachte olefinpolymerisationskatalysatoren
US6841609B2 (en) 1998-07-09 2005-01-11 W. R. Grace & Co.-Conn. Formulation suitable for ink receptive coatings
US6313061B1 (en) 1998-12-22 2001-11-06 W. R. Grace & Co.-Conn. Method of making frangible spray dried agglomerated supports and olefin polymerization catalysts supported thereon
US6271325B1 (en) * 1999-05-17 2001-08-07 Univation Technologies, Llc Method of polymerization
GB2355711B (en) * 1999-10-27 2003-12-24 Agilent Technologies Inc Porous silica microsphere scavengers
US6638982B2 (en) * 2000-11-15 2003-10-28 Cabot Corporation Method of preparing a fumed metal oxide dispersion
DE10163154A1 (de) * 2001-12-20 2003-07-03 Basell Polyolefine Gmbh Pyrogene Kieselsäuren enthaltender Katalysatorfeststoff zur Olefinpolymerisation
TWI761649B (zh) * 2017-12-27 2022-04-21 日商日揮觸媒化成股份有限公司 多孔二氧化矽粒子及其製造方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2186431A1 (fr) * 1972-05-15 1974-01-11 Mo Gosud Rstvenny
GB1371440A (en) * 1972-05-31 1974-10-23 Mo G Uni Im Mv Lomonosova Process for preparing a wide-pore adsorbent for use in chromato graphy
FR2323706A1 (fr) * 1975-09-10 1977-04-08 Basf Ag Procede de preparation de polymeres d'olefines

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT636071A (fr) * 1959-09-22
US3095384A (en) * 1960-09-09 1963-06-25 Socony Mobil Oil Co Inc Hydrogel treatment
US3239498A (en) * 1961-07-20 1966-03-08 Phillips Petroleum Co Silica-containing catalysts
US3243262A (en) * 1963-02-18 1966-03-29 Grace W R & Co Process for preparing microspheroidal silica
GB1219877A (en) * 1968-05-22 1971-01-20 Grace W R & Co Process for making fine sized low density silica
US4067954A (en) * 1971-05-11 1978-01-10 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler Process for the production of finely divided silicon dioxide having a large specific surface
BE790704A (fr) * 1971-10-28 1973-02-15 Degussa Procede pour la fabrication d'oxydes finement
BE792365A (fr) * 1971-12-06 1973-03-30 Gulf Research Development Co Catalyseurs de polymerisation de 1-olefines
DE2414478C3 (de) * 1974-03-26 1978-07-13 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt Aerogelartige strukturierte Kieselsäure und Verfahren zu ihrer Herstellung

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2186431A1 (fr) * 1972-05-15 1974-01-11 Mo Gosud Rstvenny
GB1371440A (en) * 1972-05-31 1974-10-23 Mo G Uni Im Mv Lomonosova Process for preparing a wide-pore adsorbent for use in chromato graphy
FR2323706A1 (fr) * 1975-09-10 1977-04-08 Basf Ag Procede de preparation de polymeres d'olefines

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003054089A1 (fr) * 2001-12-21 2003-07-03 Degussa Ag Granules a base de dioxyde de silicium obtenus par pyrogenese, fabrication et utilisation

Also Published As

Publication number Publication date
AT373853B (de) 1984-02-27
DE2831561C2 (fr) 1989-03-30
US4228260A (en) 1980-10-14
ES471789A1 (es) 1979-10-01
NL7707961A (nl) 1979-01-22
IT7850321A0 (it) 1978-07-14
DE2831561A1 (de) 1979-02-01
NL7807220A (nl) 1979-01-22
GB2001044B (en) 1982-08-11
IT1107453B (it) 1985-11-25
ATA494178A (de) 1983-07-15
CA1126244A (fr) 1982-06-22
JPS5421992A (en) 1979-02-19
JPS6215485B2 (fr) 1987-04-08
BE868792A (nl) 1979-01-08
FR2398021B1 (fr) 1982-07-30
GB2001044A (en) 1979-01-24
US4225464A (en) 1980-09-30
SE7807949L (sv) 1979-03-21

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