FR2388784A1 - Procede de preparation du 1,2-dichlorethane - Google Patents

Procede de preparation du 1,2-dichlorethane

Info

Publication number
FR2388784A1
FR2388784A1 FR7812841A FR7812841A FR2388784A1 FR 2388784 A1 FR2388784 A1 FR 2388784A1 FR 7812841 A FR7812841 A FR 7812841A FR 7812841 A FR7812841 A FR 7812841A FR 2388784 A1 FR2388784 A1 FR 2388784A1
Authority
FR
France
Prior art keywords
dichloroethane
gases
gas
oxygen
volume
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7812841A
Other languages
English (en)
Other versions
FR2388784B1 (fr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19772718878 external-priority patent/DE2718878C3/de
Priority claimed from DE19772742409 external-priority patent/DE2742409C3/de
Application filed by Hoechst AG filed Critical Hoechst AG
Publication of FR2388784A1 publication Critical patent/FR2388784A1/fr
Application granted granted Critical
Publication of FR2388784B1 publication Critical patent/FR2388784B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/15—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination
    • C07C17/152—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons
    • C07C17/156—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons of unsaturated hydrocarbons
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

L'invention concerne un procédé de préparation du 1,2-dichloréthane par oxychloration de l'éthylène à l'aide de gaz chlorhydrique et d'un gaz contenant de l'oxygène moléculaire en phase gazeuse, à température élevée et en présence d'un catalyseur à lit fluidisé au chlorure de cuivre-II sur un support, dans lequel on refroidit sous pression les gaz de réaction en deux stades de condensation, on évacue ensuite le 1,2-dichloréthane condensé et on recycle la majeure partie des gaz de départ non convertis et des gaz inertes. Le procédé selon l'invention est plus particulièrement caractérisé en ce que, dans un troisième stade de condensation, on refroidit les gaz de réaction à une température comprise entre 5 et 18 degrés C dans une mesure juste suffisante pour retenir 0,5 à 3,0 % en volume de 1,2-dichloréthane et on mélange directement, en amont du réacteur, le gaz de recyclage avec la quantité d'oxygène pur nécessaire pour remplacer l'oxygène consommé et retablir une teneur en oxygène de 12 à 25 % en volume.
FR7812841A 1977-04-28 1978-04-28 Procede de preparation du 1,2-dichlorethane Granted FR2388784A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19772718878 DE2718878C3 (de) 1977-04-28 1977-04-28 Verfahren zur Herstellung von 1,2-Dichloräthan durch Oxychlorierung von Äthylen
DE19772742409 DE2742409C3 (de) 1977-09-21 1977-09-21 Verfahren zur Herstellung von 1,2 Dichloräthan

Publications (2)

Publication Number Publication Date
FR2388784A1 true FR2388784A1 (fr) 1978-11-24
FR2388784B1 FR2388784B1 (fr) 1985-03-01

Family

ID=25771929

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7812841A Granted FR2388784A1 (fr) 1977-04-28 1978-04-28 Procede de preparation du 1,2-dichlorethane

Country Status (14)

Country Link
US (1) US4310713A (fr)
JP (1) JPS549207A (fr)
BR (1) BR7802608A (fr)
CA (1) CA1114402A (fr)
CS (1) CS207608B2 (fr)
DD (1) DD136832A5 (fr)
ES (1) ES468300A1 (fr)
FR (1) FR2388784A1 (fr)
GB (1) GB1575883A (fr)
IT (1) IT1105401B (fr)
MX (1) MX147525A (fr)
NL (1) NL7804406A (fr)
NO (1) NO151821C (fr)
SE (1) SE442745B (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0013020A1 (fr) * 1978-12-26 1980-07-09 The B.F. GOODRICH Company Oxydation catalytique sélective de monoxyde de carbone en présence de monomères oléfiniques
EP0146925A2 (fr) * 1983-12-22 1985-07-03 Wacker-Chemie GmbH Procédé pour l'oxychloruration d'éthylène

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3626853A1 (de) * 1986-08-08 1988-02-11 Hoechst Ag Verfahren und vorrichtung zur rueckgewinnung von 1,2-dichlorethan aus abgasen
DE19837957C1 (de) * 1998-08-21 2000-01-05 Krupp Uhde Gmbh Verfahren zur Steuerung der Feinstaubpartikelmenge in einem Wirbelschichtreaktor, insbesondere zur Oxichlorierung von Ethylen
DE19851423A1 (de) * 1998-11-07 2000-05-11 Krupp Uhde Gmbh Vorrichtung zur Bereitstellung eines Blockflansches einer Mannlochöffnung o. dgl., insbesondere bei Wirbelschichtreaktoren
CN101242899B (zh) * 2005-08-18 2011-06-22 雅宝荷兰有限责任公司 催化氧氯化
JP5037536B2 (ja) * 2007-02-15 2012-09-26 日本発條株式会社 弁ばね装置と、それを用いたエンジンの動弁機構
JP5064138B2 (ja) 2007-08-15 2012-10-31 日本発條株式会社 弁ばね装置と、それを用いたエンジンの動弁機構

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1548259A (fr) * 1965-05-24 1968-12-06
DE2626133A1 (de) * 1975-06-17 1976-12-30 Allied Chem Zyklisches verfahren zur herstellung von aethylendichlorid

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2602021A (en) * 1948-06-30 1952-07-01 Kellogg M W Co Catalytic production of chlorine
US2846484A (en) * 1954-02-02 1958-08-05 Monsanto Chemicals Production of chlorinated aliphatic compounds
US2952714A (en) * 1957-12-30 1960-09-13 Columbia Southern Chem Corp Method of controlling alkane oxychlorination process
US3488398A (en) * 1964-04-23 1970-01-06 Goodrich Co B F Method of preparing 1,2-dichloroethane
JPS4932841A (fr) * 1972-07-26 1974-03-26

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1548259A (fr) * 1965-05-24 1968-12-06
DE1518931A1 (de) * 1965-05-24 1969-07-10 Goodrich Co B F Verfahren zur Herstellung von 1,2-Dichloraethan
DE2626133A1 (de) * 1975-06-17 1976-12-30 Allied Chem Zyklisches verfahren zur herstellung von aethylendichlorid
FR2314907A1 (fr) * 1975-06-17 1977-01-14 Allied Chem Procede cyclique d'oxychlorhydratation d'ethylene avec emissions d'hydrocarbures reduites et dichlorure d'ethylene ainsi obtenu

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0013020A1 (fr) * 1978-12-26 1980-07-09 The B.F. GOODRICH Company Oxydation catalytique sélective de monoxyde de carbone en présence de monomères oléfiniques
EP0146925A2 (fr) * 1983-12-22 1985-07-03 Wacker-Chemie GmbH Procédé pour l'oxychloruration d'éthylène
EP0146925A3 (en) * 1983-12-22 1985-09-25 Wacker-Chemie Gmbh Method for the oxychlorination of ethylene

Also Published As

Publication number Publication date
GB1575883A (en) 1980-10-01
SE7804878L (sv) 1978-10-29
FR2388784B1 (fr) 1985-03-01
ES468300A1 (es) 1978-11-16
NO781489L (no) 1978-10-31
NO151821C (no) 1985-06-12
CA1114402A (fr) 1981-12-15
SE442745B (sv) 1986-01-27
NO151821B (no) 1985-03-04
US4310713A (en) 1982-01-12
MX147525A (es) 1982-12-13
IT1105401B (it) 1985-11-04
JPS549207A (en) 1979-01-24
IT7849063A0 (it) 1978-04-26
JPS5715808B2 (fr) 1982-04-01
NL7804406A (nl) 1978-10-31
CS207608B2 (en) 1981-08-31
BR7802608A (pt) 1978-12-19
DD136832A5 (de) 1979-08-01

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Legal Events

Date Code Title Description
ST Notification of lapse