ES8401990A1 - Un procedimiento para la preparacion de eteres de celulosa a partir de celulosa. - Google Patents
Un procedimiento para la preparacion de eteres de celulosa a partir de celulosa.Info
- Publication number
- ES8401990A1 ES8401990A1 ES517733A ES517733A ES8401990A1 ES 8401990 A1 ES8401990 A1 ES 8401990A1 ES 517733 A ES517733 A ES 517733A ES 517733 A ES517733 A ES 517733A ES 8401990 A1 ES8401990 A1 ES 8401990A1
- Authority
- ES
- Spain
- Prior art keywords
- dimethoxyethane
- cellulose ethers
- dispersing agent
- soluble cellulose
- preparing water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Immobilizing And Processing Of Enzymes And Microorganisms (AREA)
- Materials For Medical Uses (AREA)
Abstract
PROCEDIMIENTO PARA LA PREPARACION DE ETERES DE CELULOSA A PARTIR DE CELULOSA.CONSISTE EN DOS ETAPAS: A) ALCALINIZAR LA CELULOSA, EN UNA MEZCLA COMPUESTO POR DIMETOXIETANO, AGUA Y UN HIDROXIDO ALCALINO COMO HIDROXIDO SODICO. SE REALIZA CON AGITACION DE LA MEZCLA, A TEMPERATURA DE 0 A 30JC Y CON UN PESO DE DIMETOXIETANO DE 3 A 30 VECES MAYOR QUE EL PESO DE CELULOSA; B) A LA MEZCLA, SE LE AÑADE EL AGENTE ESTERIFICANTE, QUE PUEDE SER UN CLORURO DE ALQUILO DE C 1 A 3 O UN OXIDO DE ALQUILENO DE C 2 A 4. SE REALIZA CON AGITACION DE LA MEZCLA, A TEMPERATURA DE 30 A 120JC,CON DURACION DE 30 MINUTOS A 8 HORAS. SE NEUTRALIZA CON ACIDO PARA ELIMINAR LAS BASES QUE NO HAN REACCIONADO, SE CENTRIFUGA PARA ELIMINAR LOS COMPONENTES LIQUIDOS Y SE SOMETE LA MEZCLA A EXTRACCION, SE SECA Y SE TRITURA DESPUES DE SECADA, PARA MEZCLARSE CON OTROS COMPONENTES.SE UTILIZAN COMO ESPESANTES, ADHESIVOS O ADITIVOS PARA MATERIALES DE CONSTRUCCION.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19813147434 DE3147434A1 (de) | 1981-11-30 | 1981-11-30 | Verfahren zur herstellung von celluloseethern mit dimethoxyethan als dispergierhilfsmittel |
Publications (2)
Publication Number | Publication Date |
---|---|
ES517733A0 ES517733A0 (es) | 1984-01-01 |
ES8401990A1 true ES8401990A1 (es) | 1984-01-01 |
Family
ID=6147564
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES517733A Expired ES8401990A1 (es) | 1981-11-30 | 1982-11-26 | Un procedimiento para la preparacion de eteres de celulosa a partir de celulosa. |
Country Status (10)
Country | Link |
---|---|
US (1) | US4460766A (es) |
EP (1) | EP0080678B1 (es) |
JP (1) | JPS58103501A (es) |
AT (1) | ATE32081T1 (es) |
BR (1) | BR8206918A (es) |
CA (1) | CA1193250A (es) |
DE (2) | DE3147434A1 (es) |
ES (1) | ES8401990A1 (es) |
FI (1) | FI69632C (es) |
ZA (1) | ZA828552B (es) |
Families Citing this family (25)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3306621A1 (de) * | 1983-02-25 | 1984-08-30 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von celluloseethern mit einem dimethoxyethan enthaltenden dispergierhilfsmittel |
DE3316124A1 (de) * | 1983-05-03 | 1984-11-08 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von wasserloeslichen cellulosemischethern |
DE3417952A1 (de) * | 1984-05-15 | 1985-11-21 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von wasserloeslichen cellulosemischethern |
US4707189A (en) * | 1984-11-07 | 1987-11-17 | Hercules Incorporated | Biostable compositions and the aqueous solutions thereof as thickeners for aqueous-based systems |
US4855139A (en) * | 1987-01-20 | 1989-08-08 | Med. Fab (Lafayette), Inc. | Fungicidally active cellulosic textile compositions, or articles of manufacture |
US4845206A (en) * | 1987-05-21 | 1989-07-04 | The Dow Chemical Company | Production of cellulose ethers using a premix of alkali and etherifying agent |
BR9000379A (pt) | 1989-01-31 | 1990-12-04 | Union Carbide Chem Plastic | Polissacarideo soluvel em agua,processo para producao de um polissacarideo soluvel em agua,composicao de latex e processo para producao de uma composicao de latex |
US5120838A (en) * | 1989-10-30 | 1992-06-09 | Aqualon Company | Alkylaryl hydrophobically modified cellulose ethers |
US5493013A (en) * | 1992-04-23 | 1996-02-20 | Hoechst Aktiengesellschaft | Process for preparing cellulose ethers with cyclic ethers as suspending agents |
DE4243281A1 (de) * | 1992-12-21 | 1994-06-23 | Wolff Walsrode Ag | Hochsubstituierte Sulfoalkylcellulosederivate, insbesondere Sulfoethylcelluloseether, Verfahren zu deren Herstellung und deren Verwendung als Verdickungsmittel für Textildruckfarbpasten |
US5504123A (en) * | 1994-12-20 | 1996-04-02 | Union Carbide Chemicals & Plastics Technology Corporation | Dual functional cellulosic additives for latex compositions |
DE19746264A1 (de) | 1997-10-20 | 1999-04-29 | Wolff Walsrode Ag | Verfahren zur Herstellung einer Carboxymethylcellulose mit verbesserter Wasserretention |
US6261218B1 (en) * | 1998-12-01 | 2001-07-17 | The Dow Chemical Company | Process and apparatus for making low molecular weight cellulose ethers |
EP1171471B2 (en) * | 1999-04-01 | 2009-07-08 | Dow Global Technologies Inc. | Enhanced gel strength methylcellulose |
US6686464B1 (en) * | 1999-04-26 | 2004-02-03 | Bki Holding Corporation | Cellulose ethers and method of preparing the same |
JP2001302701A (ja) * | 2000-02-15 | 2001-10-31 | Shin Etsu Chem Co Ltd | アルカリセルロース及びセルロースエーテルの製造方法 |
DE10018155A1 (de) * | 2000-04-12 | 2001-10-25 | Clariant Gmbh | Verfahren zur Herstellung von gut benetzbaren, wasserlöslichen, pulverförmigen, mindestens alkylierten, nicht-ionischen Celluloseethern |
JP4195289B2 (ja) * | 2000-11-01 | 2008-12-10 | ビーケイアイ・ホールディング・コーポレーション | セルロースエーテル及びその製造方法 |
DE10135464A1 (de) * | 2001-07-20 | 2003-02-06 | Wolff Walsrode Ag | Verfahren zur Herstellung von Alkylhydroxyalkylcellulose |
DE102004035870A1 (de) * | 2004-07-23 | 2006-02-09 | Wolff Cellulosics Gmbh & Co. Kg | Verfahren zur Herstellung aminoalkylgruppenhaltiger Polysaccharide und Polysaccharidderivate |
KR101321301B1 (ko) * | 2005-03-02 | 2013-10-30 | 허큘레스 인코포레이티드 | 수용성 저치환 히드록시에틸셀룰로스, 이의 유도체, 이의제조 방법, 및 용도 |
JP5377816B2 (ja) | 2005-06-16 | 2013-12-25 | 信越化学工業株式会社 | セルロースエーテルの製造方法 |
CN101583628B (zh) * | 2007-01-22 | 2014-09-24 | 阿克佐诺贝尔股份有限公司 | 制备纤维素醚的方法 |
JP2010031165A (ja) * | 2008-07-30 | 2010-02-12 | Sanyo Chem Ind Ltd | アルキルエーテル化カルボキシアルキルセルロース |
BRPI1006378B1 (pt) * | 2009-03-05 | 2019-09-17 | Dow Global Technologies Llc | Processo para a produção de celulose alcalina |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1980988A (en) * | 1933-05-03 | 1934-11-20 | Du Pont | Solvents for etherification of cellulose |
US2553695A (en) * | 1947-10-17 | 1951-05-22 | Celanese Corp | Manufacture of cellulose ethers |
US2618632A (en) * | 1949-04-05 | 1952-11-18 | Hercules Powder Co Ltd | Mixed cellulose ether and preparation thereof |
US2682535A (en) * | 1950-11-28 | 1954-06-29 | Union Carbide & Carbon Corp | Hydroxyalkylation of polysaccharides |
US2767170A (en) * | 1951-08-29 | 1956-10-16 | Hercules Powder Co Ltd | Preparation of alkali cellulose |
US2749336A (en) * | 1952-04-02 | 1956-06-05 | Hercules Powder Co Ltd | Process for producing cellulose derivatives |
US2744894A (en) * | 1952-09-08 | 1956-05-08 | Union Carbide & Carbon Corp | Hydroxyalkylation of polysaccharides |
DE1009173B (de) * | 1954-06-05 | 1957-05-29 | Du Pont | Verfahren zur Herstellung der Alkalisalze von Celluloseaethercarbonsaeuren |
US3085087A (en) * | 1956-09-13 | 1963-04-09 | Hercules Powder Co Ltd | Preparation of carboxyalkyl cellulose ethers |
US3131177A (en) * | 1960-04-13 | 1964-04-28 | Hercules Powder Co Ltd | Manufacture of water-soluble hydroxyalkyl cellulose ethers |
DE1196628B (de) * | 1962-05-18 | 1965-07-15 | Krempel August Soehne | Verfahren zur Herstellung von faserfoermigen Cyanalkylaethern der Cellulose |
US3351583A (en) * | 1964-07-06 | 1967-11-07 | Hercules Inc | Preparation of hydroxypropyl cellulose |
US3284441A (en) * | 1965-07-26 | 1966-11-08 | Hercules Inc | Process of preparing carboxymethyl-cellulose |
DE2000082A1 (de) * | 1970-01-02 | 1971-07-15 | Wolff Walsrode Ag | Verfahren zur Verhinderung des Abbaus von Alkalicellulose |
US4024335A (en) * | 1976-05-04 | 1977-05-17 | Union Carbide Corporation | Homogeneous hydroxy-alkylation of cellulose |
DE2644678A1 (de) * | 1976-10-02 | 1978-04-06 | Dynamit Nobel Ag | Verfahren zur herstellung funktionalisierter cellulosen |
US4129722A (en) * | 1977-12-15 | 1978-12-12 | National Starch And Chemical Corporation | Process for the preparation of high D. S. polysaccharides |
US4278790A (en) * | 1978-07-31 | 1981-07-14 | Hopkins Agricultural Chemical Co. | Novel cellulose solutions |
US4228277A (en) * | 1979-02-12 | 1980-10-14 | Hercules Incorporated | Modified nonionic cellulose ethers |
DE2929002A1 (de) * | 1979-07-18 | 1981-02-12 | Henkel Kgaa | Verfahren zur herstellung von cellulosederivaten mittels besonders reaktiver alkalicellulose |
DE3010464A1 (de) * | 1980-03-19 | 1981-10-01 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur herstellung von wasserarmer alkalicellulose |
-
1981
- 1981-11-30 DE DE19813147434 patent/DE3147434A1/de not_active Withdrawn
-
1982
- 1982-11-16 CA CA000415694A patent/CA1193250A/en not_active Expired
- 1982-11-19 US US06/443,104 patent/US4460766A/en not_active Expired - Lifetime
- 1982-11-19 ZA ZA828552A patent/ZA828552B/xx unknown
- 1982-11-22 AT AT82110764T patent/ATE32081T1/de active
- 1982-11-22 DE DE8282110764T patent/DE3278016D1/de not_active Expired
- 1982-11-22 EP EP82110764A patent/EP0080678B1/de not_active Expired
- 1982-11-26 ES ES517733A patent/ES8401990A1/es not_active Expired
- 1982-11-26 FI FI824090A patent/FI69632C/fi not_active IP Right Cessation
- 1982-11-29 BR BR8206918A patent/BR8206918A/pt unknown
- 1982-11-30 JP JP57208740A patent/JPS58103501A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
EP0080678A3 (en) | 1984-10-03 |
DE3147434A1 (de) | 1983-06-09 |
ATE32081T1 (de) | 1988-02-15 |
US4460766A (en) | 1984-07-17 |
FI824090L (fi) | 1983-05-31 |
JPS58103501A (ja) | 1983-06-20 |
FI69632B (fi) | 1985-11-29 |
DE3278016D1 (en) | 1988-02-25 |
ES517733A0 (es) | 1984-01-01 |
BR8206918A (pt) | 1983-10-04 |
FI824090A0 (fi) | 1982-11-26 |
CA1193250A (en) | 1985-09-10 |
EP0080678A2 (de) | 1983-06-08 |
EP0080678B1 (de) | 1988-01-20 |
ZA828552B (en) | 1983-09-28 |
FI69632C (fi) | 1986-03-10 |
JPH0242081B2 (es) | 1990-09-20 |
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